Journal of The Chemical Society, Chemical Communications最新文献

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Erratum: Intercalation of nitric oxide into double-layered cuprate superstructure (Journal of the Chemical Society, Chemical Communications (1995) (485)) 勘误:将一氧化氮插入双层铜上层结构(化学学会杂志,化学通讯(1995)(485))
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-12-01 DOI: 10.1039/C39950001309
M. Machida, Hirotaka Murakami, Takeshi Kitsubayashi, T. Kijima
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引用次数: 0
Novel naphthoquinone methide dyes for second-order nonlinear optical materials 用于二阶非线性光学材料的新型萘醌染料
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-09-12 DOI: 10.1039/C39950000969
Y. Kubo, S. Aramaki, Okamoto Yuko, T. Murayama
{"title":"Novel naphthoquinone methide dyes for second-order nonlinear optical materials","authors":"Y. Kubo, S. Aramaki, Okamoto Yuko, T. Murayama","doi":"10.1039/C39950000969","DOIUrl":"https://doi.org/10.1039/C39950000969","url":null,"abstract":"Naphthoquinone methide dyes show a large Pockels coefficient at 1.3 µm when poled in a polymer matrix: the second-order nonlinear hyperpolarizability (µβ) values obtained from Pockels coefficients that appear after poling in a constant electric field are (5700–7400)× 10–48 esu, being much higher than that of commonly used Disperse Red 1 (DR1).","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"124 1","pages":"969-970"},"PeriodicalIF":0.0,"publicationDate":"1995-09-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86902660","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Optically active diazacyclophosphamides: novel efficient reagents for the determination of the absolute configuration of amines and alcohols 光活性重氮环磷酰胺:一种测定胺和醇绝对构型的新型高效试剂
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-08-08 DOI: 10.1039/C39950000435
T. Oshikawa,, M. Yamashita,, Sadaaki Kumagai, K. Seo, J. Kobayashi
{"title":"Optically active diazacyclophosphamides: novel efficient reagents for the determination of the absolute configuration of amines and alcohols","authors":"T. Oshikawa,, M. Yamashita,, Sadaaki Kumagai, K. Seo, J. Kobayashi","doi":"10.1039/C39950000435","DOIUrl":"https://doi.org/10.1039/C39950000435","url":null,"abstract":"Various amines and alcohols are converted into the corresponding phosphamides by the action of optically active diazacyclophosphamidic chlorides and absolute configurations of amines and alcohols are readily determined by proton and phosphorus NMR of the cyclophosphamides that are formed.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"49 1","pages":"435-436"},"PeriodicalIF":0.0,"publicationDate":"1995-08-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75330667","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 12
Remote asymmetric induction in reactions between 4- and 5-benzyloxypent-2-enyl(tributyl)stannanes and chiral imines prepared from butyl glyoxylate 4-和5-苄基氧基-2-烯基(三丁基)锡烷与乙氧基丁酸酯制备的手性亚胺的远程不对称诱导反应
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-08-01 DOI: 10.1039/C39950000657
D. Hallett, E. Thomas
{"title":"Remote asymmetric induction in reactions between 4- and 5-benzyloxypent-2-enyl(tributyl)stannanes and chiral imines prepared from butyl glyoxylate","authors":"D. Hallett, E. Thomas","doi":"10.1039/C39950000657","DOIUrl":"https://doi.org/10.1039/C39950000657","url":null,"abstract":"Transmetallation of 4- and 5-benzyloxypent-2-enyl(tributyl)stannanes 13 and 18 with tin(IV) chloride generates intermediate allyltin trichlorides which react with imines 9 and ent-9, prepared from butyl glyoxylate and either (R)- or (S)-1-phenylethylamine, with effective 1,5-asymmetric induction.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"12 1","pages":"657-658"},"PeriodicalIF":0.0,"publicationDate":"1995-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91185479","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 23
A SIMPLE IN SITU 31P NMR METHOD FOR THE DETERMINATION OF THE ENANTIOMERIC PURITY OF AROMATIC SUBSTRATES 一种简单的原位31p核磁共振测定芳香底物对映体纯度的方法
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-08-01 DOI: 10.1039/C39950000689
J. Buriak, J. Osborn
{"title":"A SIMPLE IN SITU 31P NMR METHOD FOR THE DETERMINATION OF THE ENANTIOMERIC PURITY OF AROMATIC SUBSTRATES","authors":"J. Buriak, J. Osborn","doi":"10.1039/C39950000689","DOIUrl":"https://doi.org/10.1039/C39950000689","url":null,"abstract":"The enantiomeric purity of aromatic substrates can be determined using 31P NMR with chiral rhodium complexes in situ.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"121 10 1","pages":"689-690"},"PeriodicalIF":0.0,"publicationDate":"1995-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84090097","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
A new telogen for telechelic oligomers of chlorotrifluoroethylene 三氟氯乙烯远旋低聚物的一种新止动素
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-07-01 DOI: 10.1039/C39910001323
R. Chambers, M. Greenhall, A. Wright, G. Caporiccio
{"title":"A new telogen for telechelic oligomers of chlorotrifluoroethylene","authors":"R. Chambers, M. Greenhall, A. Wright, G. Caporiccio","doi":"10.1039/C39910001323","DOIUrl":"https://doi.org/10.1039/C39910001323","url":null,"abstract":"A new telogen, I(CF2CFCl)nl (n= 1) and its telomers (n= average 6) are obtained by irradiation of mixtures of iodine and Chlorotrifluoroethylene.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"29 1","pages":"1323-1324"},"PeriodicalIF":0.0,"publicationDate":"1995-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78798308","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 13
Structural order in MCM-41 controlled by shifting silicate polymerization equilibrium 转移硅酸盐聚合平衡控制MCM-41的结构顺序
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-04-01 DOI: 10.1039/C39950000711
R. Ryoo, Ji Man Kim
{"title":"Structural order in MCM-41 controlled by shifting silicate polymerization equilibrium","authors":"R. Ryoo, Ji Man Kim","doi":"10.1039/C39950000711","DOIUrl":"https://doi.org/10.1039/C39950000711","url":null,"abstract":"Powder X-ray diffraction, 29Si and 129Xe NMR spectroscopy of MCM-41 show that the long-range structural order and textural uniformity of the mesoporous molecular sieve are markedly improved due to a shift in the reaction equilibrium when acetic acid is repeatedly added during the conversion of sodium silicate and NMe3(C16H33)Cl to a MCM-41 phase.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"148 1","pages":"711-712"},"PeriodicalIF":0.0,"publicationDate":"1995-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76623204","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 169
The construction of 1,3-dienes containing an E-double bond and an exo-methylene group 含有e -双键和外亚甲基的1,3-二烯的构造
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-01-01 DOI: 10.1039/C39950001497
J. Eshelby, P. Parsons, N. C. Sillars, P. Crowley
{"title":"The construction of 1,3-dienes containing an E-double bond and an exo-methylene group","authors":"J. Eshelby, P. Parsons, N. C. Sillars, P. Crowley","doi":"10.1039/C39950001497","DOIUrl":"https://doi.org/10.1039/C39950001497","url":null,"abstract":"The use of a tandem Ireland Claisen rearrangement followed by an in situ silicon mediated epoxide fragmentation provides an efficient entry into 1,3-dienes containing an E-double bond and an exo-methylene group; initial results regarding remote chirality control are reported.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"20 1","pages":"1497-1498"},"PeriodicalIF":0.0,"publicationDate":"1995-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73662484","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
Iodination and Heck alkynylation of 5,15-diphenylporphyrin. A convenient entry to asymmetrically meso-substituted porphyrins 5,15-二苯基卟啉的碘化和Heck炔基化。不对称中位取代卟啉的方便入口
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-01-01 DOI: 10.1039/C39950000527
R. Boyle, Claire K. Johnson, D. Dolphin
{"title":"Iodination and Heck alkynylation of 5,15-diphenylporphyrin. A convenient entry to asymmetrically meso-substituted porphyrins","authors":"R. Boyle, Claire K. Johnson, D. Dolphin","doi":"10.1039/C39950000527","DOIUrl":"https://doi.org/10.1039/C39950000527","url":null,"abstract":"Iodination of 5,15-diphenylporphyrin followed by metallation and palladium(0) catalysed coupling with monosubstituted acetylenes gives zinc(II)-10-(2-substituted-alkynyl)-5,15-diphenylporphyrins.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"31 1","pages":"527-528"},"PeriodicalIF":0.0,"publicationDate":"1995-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73793733","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 58
Activation and functionalisation of the C–H bonds of methane and higher alkanes by a silica-supported tantalum hydride complex 二氧化硅负载的氢化钽配合物对甲烷和高级烷烃碳氢键的活化和功能化
Journal of The Chemical Society, Chemical Communications Pub Date : 1995-01-01 DOI: 10.1039/C39950000991
V. Vidal, A. Théolier, J. Thivolle-cazat, J. Basset
{"title":"Activation and functionalisation of the C–H bonds of methane and higher alkanes by a silica-supported tantalum hydride complex","authors":"V. Vidal, A. Théolier, J. Thivolle-cazat, J. Basset","doi":"10.1039/C39950000991","DOIUrl":"https://doi.org/10.1039/C39950000991","url":null,"abstract":"Silica-supported tantalum hydride activates at low temperature the C–H and the C–D bonds of cyclooctane and CD4, respectively, to form the corresponding cyclooctyl and perdeuteriomethyl-tantalum surface complexes; these complexes are transformed under molecular oxygen into the corresponding tantalum-alkoxy derivatives which with acetic acid give rise to the corresponding alkylacetates.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"6 1","pages":"991-992"},"PeriodicalIF":0.0,"publicationDate":"1995-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74002108","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 23
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