International Journal of Adhesion and Adhesives最新文献

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Development of acrylic acid–agar-based adhesive hydrogel: Influence of tannic acid concentration on adhesion performance 丙烯酸-琼脂基黏附水凝胶的研制:单宁酸浓度对黏附性能的影响
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-06-16 DOI: 10.1016/j.ijadhadh.2025.104088
Muhammad Tahir Khan , Tanzil Ur Rehman , Luqman Ali Shah , Hyeongmin Yoo
{"title":"Development of acrylic acid–agar-based adhesive hydrogel: Influence of tannic acid concentration on adhesion performance","authors":"Muhammad Tahir Khan ,&nbsp;Tanzil Ur Rehman ,&nbsp;Luqman Ali Shah ,&nbsp;Hyeongmin Yoo","doi":"10.1016/j.ijadhadh.2025.104088","DOIUrl":"10.1016/j.ijadhadh.2025.104088","url":null,"abstract":"<div><div>The present study aimed to develop a mechanically enhanced and biocompatible adhesive hydrogel utilizing acrylic acid and agar. N, N-methylene bisacrylamide (MBA) and tannic acid (TA) were employed as chemical and physical crosslinkers, respectively. The structural and chemical characteristics of the hydrogel were confirmed through scanning electron microscopy (SEM) and Fourier transform infrared (FTIR) spectroscopy, verifying its successful Synthesis via free radical polymerization. Rheological analyses, including frequency sweep, amplitude sweep, and creep recovery tests, were conducted to assess the viscoelastic and adhesive properties of the hydrogel. The findings revealed that specific polymeric chain interaction governed the adhesive behavior of the hydrogel. Furthermore, varying concentrations of tannic acid were investigated to determine their influence on adhesive performance, with results indicating that increasing TA concentration significantly enhanced adhesive properties. The adhesion strength followed the order: 36.8 &gt; 21.06 &gt; 13.04 &gt; 7.75 &gt; 4.31 kPa for TA ranging from 0.025 to 0 g, respectively. The synthesized hydrogel demonstrate superior approach, cost-effectiveness, high efficiency, and biodegradable nature which highlights their potential as an advanced adhesive material for future applications.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"142 ","pages":"Article 104088"},"PeriodicalIF":3.2,"publicationDate":"2025-06-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144312675","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of graphene nanoparticles (GNP) on adhesively bonded patch repaired composite under tensile static and fatigue loading 石墨烯纳米颗粒(GNP)对粘接贴片修复复合材料在拉伸静态和疲劳载荷下的影响
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-06-11 DOI: 10.1016/j.ijadhadh.2025.104072
Banamali Sahu , Chinmaya Kumar Sahoo , Ramadas Chennamsetti , A. Arockiarajan
{"title":"Effect of graphene nanoparticles (GNP) on adhesively bonded patch repaired composite under tensile static and fatigue loading","authors":"Banamali Sahu ,&nbsp;Chinmaya Kumar Sahoo ,&nbsp;Ramadas Chennamsetti ,&nbsp;A. Arockiarajan","doi":"10.1016/j.ijadhadh.2025.104072","DOIUrl":"10.1016/j.ijadhadh.2025.104072","url":null,"abstract":"<div><div>Composite materials are prone to damage during their operation and service condition. In these circumstances, composite patch repair is a promising alternative to the damaged part as it enhances the properties of the damaged material. This work performed static and fatigue tensile tests on pristine, drill, and two external patch-repaired samples (15 and 30 mm square patches). Both the 15 mm and 30 mm patch-repaired samples showed 8% and 31% improvement in fatigue life compared to the drill sample, respectively. Furthermore, to understand the effect of graphene nanoparticles (GNP), the 30 mm patch was preferred due to its superiority in improving mechanical properties. In order to enhance fatigue life, GNP of different weight percentages (0.3, 0.5, 0.7, and 0.9) were added to the patch-parent interface. A 0.5 wt% GNP provided approximately 157% and 96% improvement in fatigue life compared to drilled and repaired specimens, respectively. A thorough understanding of GNP addition in repaired composites with the help of failure pattern, DIC, and AE has been elaborated.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"142 ","pages":"Article 104072"},"PeriodicalIF":3.2,"publicationDate":"2025-06-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144290634","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Mechanical performance and bond-slip model of adhesively bonded joints between Fe-SMA and concrete Fe-SMA与混凝土粘结接头力学性能及粘结滑移模型
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-06-07 DOI: 10.1016/j.ijadhadh.2025.104085
Xu Jiang , Chengxiu Jia , Xueqiang Ma , Xuhong Qiang
{"title":"Mechanical performance and bond-slip model of adhesively bonded joints between Fe-SMA and concrete","authors":"Xu Jiang ,&nbsp;Chengxiu Jia ,&nbsp;Xueqiang Ma ,&nbsp;Xuhong Qiang","doi":"10.1016/j.ijadhadh.2025.104085","DOIUrl":"10.1016/j.ijadhadh.2025.104085","url":null,"abstract":"<div><div>The vast scale of reinforced concrete structures in civil engineering, combined with their ongoing aging and damage, has led engineers and researchers to propose numerous reinforcement and repair solutions. In recent years, iron-based shape memory alloy (Fe-SMA), as a low-cost, self-prestressing intelligent material, has been demonstrated as a competitive alternative to traditional reinforcement materials such as steel and carbon fiber reinforced polymer (CFRP), exhibiting significant potential in structural strengthening applications. When using Fe-SMA to reinforce concrete structures, it is crucial to ensure a reliable connection between the two materials for effective load transfer, but research in this area, both experimental and theoretical, remains limited. To investigate the load transfer mechanism and failure criteria of Fe-SMA/concrete adhesively bonded joints (BoJs) under shear forces, shear tests are conducted on 20 sets of bonded joint specimens composed of Fe-SMA plates (FSPs) and concrete blocks. The effects of adhesive layer thickness (ALT), bond length (BL), and structural adhesive type on the mechanical performance of these joints are analyzed. Besides, this study proposes the bond-slip model of bonded joints between Fe-SMA and concrete in structural reinforcements, laying a experimental and theoretical foundation for promoting the reinforcement utilization of Fe-SMA in civil engineering, especially for concrete structures.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"142 ","pages":"Article 104085"},"PeriodicalIF":3.2,"publicationDate":"2025-06-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144272208","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Enhancing bond strength and sealer penetration of resin-based Sealers: The impact of chitosan/genipin solution in root canal final irrigation 壳聚糖/吉尼平溶液对根管末灌的影响
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-06-07 DOI: 10.1016/j.ijadhadh.2025.104073
Fillipe Mendes Silva, Rafael Verardino de Camargo, Débora Fernandes Costa Guedes, Helena Cristina de Assis, Fabiane Carneiro Lopes-Olhê, Antonio Miranda da Cruz Filho
{"title":"Enhancing bond strength and sealer penetration of resin-based Sealers: The impact of chitosan/genipin solution in root canal final irrigation","authors":"Fillipe Mendes Silva,&nbsp;Rafael Verardino de Camargo,&nbsp;Débora Fernandes Costa Guedes,&nbsp;Helena Cristina de Assis,&nbsp;Fabiane Carneiro Lopes-Olhê,&nbsp;Antonio Miranda da Cruz Filho","doi":"10.1016/j.ijadhadh.2025.104073","DOIUrl":"10.1016/j.ijadhadh.2025.104073","url":null,"abstract":"<div><div>This study aimed to evaluate the effect of final irrigation of the root canal with a chitosan/genipin solution on bond strength (BS) and the penetration of AH Plus sealer into root dentin. Thirty maxillary canines were sectioned to a standardized length of 16 mm. The roots were instrumented using the ProTaper Universal system (F5 file) and divided into three groups based on the final irrigation protocol: distilled water (control), 17 % EDTA, and 1 % chitosan diluted in 5 % EDTA with 0.06 % genipin. After irrigation, the canals were dried and filled with AH Plus sealer using the lateral condensation technique. Three dentin slices were obtained from each root third. The first slice from each third was used for the push-out test and failure analysis (n = 10), while the third slice was analyzed for sealer penetration using scanning electron microscopy (n = 10). BS data were analyzed using two-way ANOVA, followed by Tukey's test (p &lt; 0.05). The treatments with chitosan/genipin and EDTA showed significantly higher BS compared to distilled water (p &lt; 0.05). However, no significant difference in BS was observed between the chitosan/genipin and EDTA groups (p = 0.132). Failure analysis showed a homogeneous distribution of failure types across all treatments and root thirds. Sealer tubular penetration was observed in the chitosan/genipin and EDTA groups, while the distilled water group exhibited no sealer penetration or resin tags within the dentinal tubules, particularly in the apical third. Final irrigation with chitosan/genipin and EDTA resulted in higher BS and enhanced sealer penetration into dentinal tubules compared to distilled water.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"142 ","pages":"Article 104073"},"PeriodicalIF":3.2,"publicationDate":"2025-06-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144231621","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Laser treatment design for CFRP bonding: an innovative approach to reduce process time CFRP粘合的激光处理设计:一种减少加工时间的创新方法
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-06-06 DOI: 10.1016/j.ijadhadh.2025.104075
Gianluca Parodo , Luca Sorrentino , Sandro Turchetta , Giuseppe Moffa
{"title":"Laser treatment design for CFRP bonding: an innovative approach to reduce process time","authors":"Gianluca Parodo ,&nbsp;Luca Sorrentino ,&nbsp;Sandro Turchetta ,&nbsp;Giuseppe Moffa","doi":"10.1016/j.ijadhadh.2025.104075","DOIUrl":"10.1016/j.ijadhadh.2025.104075","url":null,"abstract":"<div><div>Generally, the production of structural parts in fiber-reinforced polymer with complex shape or big dimensions can be difficult to achieve. Therefore, it could be preferable to produce simpler parts, which are often assembled through fastening systems or bonding with structural adhesives. In the latter case, polymer composites should be pretreated before bonding to obtain a reliable structure. For this, laser systems can represent a repeatable and very attractive solution for pretreating polymer composites. However, often the time required for realizing the pre-treatment could lead to the choice of other technologies by the manufacturer. In this article, an innovative approach to design the laser texturing for bonding CFRP is presented. Based on the assumption that only the interfaces subjected to higher stress values should be pretreated, it allows a reduction in process time. In fact, the developed method allows to design the pretreatment process as a function of the stress field on which the joint is subjected. Experimental results demonstrate a 63 % increase in shear strength for fully treated specimens compared to untreated controls, with optimized treatment yielding equivalent performance at a normalized treated area of 0.4. Numerical predictions showed strong agreement with experimental results, with a discrepancy of only 3 ÷ 4 %, validating the model's accuracy. Additionally, the treatment time was reduced by approximately 60 % without a significant loss in joint strength. This approach, transferable to complex joint geometries, enhances the efficiency and viability of laser pretreatment for CFRP bonding.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"142 ","pages":"Article 104075"},"PeriodicalIF":3.2,"publicationDate":"2025-06-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144242674","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Analysis of the interface properties of multi-material fused filament fabricated (FFF) printed polymer composite structures 多材料熔丝制备(FFF)打印聚合物复合结构界面性能分析
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-06-05 DOI: 10.1016/j.ijadhadh.2025.104074
Shauvik Pahari, Garrett W. Melenka
{"title":"Analysis of the interface properties of multi-material fused filament fabricated (FFF) printed polymer composite structures","authors":"Shauvik Pahari,&nbsp;Garrett W. Melenka","doi":"10.1016/j.ijadhadh.2025.104074","DOIUrl":"10.1016/j.ijadhadh.2025.104074","url":null,"abstract":"<div><div>Interface characteristics in multi-material 3D-printed (MM3DP) structures are a critical factor in determining the strength of the structures and predicting failure. This study investigated the shear behavior of multi-material single-lap joints fabricated entirely in a single process using Fused Filament Fabrication without the use of adhesives or post-processing techniques such as welding. The joints, comprising various combinations of PLA, PETG, and carbon-fiber reinforced PETG (PETC) were fabricated. The lap joints were subjected to shear testing, with strain fields and failure locations analyzed using two-dimensional digital image correlation (2D DIC) from synchronized front and side camera views. Results show that certain multi-material joints, particularly PETG-PETC, achieved a shear strength of 2.701 MPa, comparable to the 2.923 MPa strength of the strongest homogenous joint (PLA-PLA), and exceeding that of other homogenous joints. The presence of short carbon-fibers in PETC enhances adhesion, likely due to mechanical interlocking taking place at the interface region. These findings demonstrate that multi-material FFF, when optimized for interface compatibility and process parameters, can yield composite structures with superior mechanical properties compared to single-material prints. The successful fabrication of lap joints in a single print process highlights the feasibility of producing robust, functional multi-material components for advanced engineering applications.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"142 ","pages":"Article 104074"},"PeriodicalIF":3.2,"publicationDate":"2025-06-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144263079","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Development and characterization of self-etch adhesive system containing curcumin anchored to nanosilica on the bond strength to sound and caries-affected dentin 含姜黄素的纳米二氧化硅自蚀刻粘接体系的研制与表征
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-06-03 DOI: 10.1016/j.ijadhadh.2025.104070
Júlia Correa Raffaini , Rocio Geng Vivanco , Viviane de Cássia Oliveira , Eduardo José Soares , Mario Alexandre Coelho Sinhoreti , Fernanda de Carvalho Panzeri
{"title":"Development and characterization of self-etch adhesive system containing curcumin anchored to nanosilica on the bond strength to sound and caries-affected dentin","authors":"Júlia Correa Raffaini ,&nbsp;Rocio Geng Vivanco ,&nbsp;Viviane de Cássia Oliveira ,&nbsp;Eduardo José Soares ,&nbsp;Mario Alexandre Coelho Sinhoreti ,&nbsp;Fernanda de Carvalho Panzeri","doi":"10.1016/j.ijadhadh.2025.104070","DOIUrl":"10.1016/j.ijadhadh.2025.104070","url":null,"abstract":"<div><div>To evaluate the effects of incorporating curcumin anchored to nanosilica (CAN) into an experimental adhesive (EXP) on flexural strength, antimicrobial potential, bacterial collagenase activity, and bond strength (BS) to dentin. A commercial adhesive and EXPs containing 0 %, 1 %, 2.5 %, and 5 % CAN were tested. Cavities were prepared in 160 M (n = 20), half with induced caries. After adhesive application, cavities were restored with composite, sectioned into sticks, and stored at 37 °C for 24 h, 6 months, and 1 year before BS testing. Fracture patterns were analyzed using scanning electron microscopy, and bacterial collagenase resistance was assessed. EXPs exhibited similar flexural strength and antimicrobial activity (p &gt; 0.05), both higher than commercial (p &lt; 0.05). In caries-affected dentin, CAN0 % and CAN1 % had the lowest BS (p &lt; 0.05) after 24 h, while CAN1 % and CAN2.5 % exhibited the lowest BS (p &lt; 0.05) after 6 months. In sound dentin, CAN2.5 % showed the lowest BS (p &lt; 0.05) after 6 months and remained the lowest after 1 year in both substrates. In sound dentin, adhesive fractures were more common in commercial and CAN2.5 % after 24 h, whereas mixed fractures predominated in CAN0 % and CAN1 %. With aging, mixed fractures became more frequent. In caries-affected dentin, adhesive fractures increased over time. Aging caused hybrid layer degradation, with Whitlockite crystals in Exps. All adhesives showed biodegradation. Incorporating CAN into EXP did not flexural strength but also did not enhance antimicrobial potential or BS. High CAN concentrations may have compromised BS over time. EXP showed no effect against bacterial collagenase.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"142 ","pages":"Article 104070"},"PeriodicalIF":3.2,"publicationDate":"2025-06-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144205279","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Rheological characterization of optically clear adhesives using an in situ UV-rheometer: Insights from UV intensities and acrylate monomers 使用原位紫外线流变仪的光学透明胶粘剂的流变特性:来自紫外线强度和丙烯酸酯单体的见解
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-05-24 DOI: 10.1016/j.ijadhadh.2025.104069
Mingeun Kim , Ahran Kim , Minseon Byeon , Jin Suk Myung , Jae Heung Lee , Kyu Hyun , Woo Jin Choi
{"title":"Rheological characterization of optically clear adhesives using an in situ UV-rheometer: Insights from UV intensities and acrylate monomers","authors":"Mingeun Kim ,&nbsp;Ahran Kim ,&nbsp;Minseon Byeon ,&nbsp;Jin Suk Myung ,&nbsp;Jae Heung Lee ,&nbsp;Kyu Hyun ,&nbsp;Woo Jin Choi","doi":"10.1016/j.ijadhadh.2025.104069","DOIUrl":"10.1016/j.ijadhadh.2025.104069","url":null,"abstract":"<div><div>This study investigates the rheological properties of optically clear adhesives (OCAs) commonly used in the display industry, with a focus on the effects of ultraviolet (UV) curing intensity and acrylate monomer composition. Using an <em>in situ</em> UV-rheometer, the research particularly explores the role of isobornyl acrylate (IBOA) in influencing the internal crosslinking structure of OCAs. Results from temperature ramp, creep-recovery, and oscillatory shear tests (SAOS and LAOS) revealed that the incorporation of IBOA leads to higher glass transition temperatures (<em>T</em><sub><em>g</em></sub>) of about 30 °C and increased storage modulus (<em>G</em>′) of about 1.1 times, attributed to its bulky molecular structure that limits chain mobility. While I-0 (without IBOA) formed a robust, chemically crosslinked network with solid-like behavior, I-40 (with IBOA) exhibited viscoelastic properties indicative of linear or branched chain structures. These differences were traced to pre-curing chain formation dynamics, where the presence of IBOA and its propagation rate resulted in early crosslinking with shorter chains. The findings provide valuable insights into optimizing UV-curing processes and monomer formulations to tailor OCA performance for advanced display applications.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"141 ","pages":"Article 104069"},"PeriodicalIF":3.2,"publicationDate":"2025-05-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144170246","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Optimizing adhesion in aluminum alloys: A cross-disciplinary approach to surface treatment and bond strength 优化铝合金的附着力:表面处理和结合强度的跨学科方法
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-05-23 DOI: 10.1016/j.ijadhadh.2025.104068
F. Tajti , M. Berczeli , Z. Weltsch
{"title":"Optimizing adhesion in aluminum alloys: A cross-disciplinary approach to surface treatment and bond strength","authors":"F. Tajti ,&nbsp;M. Berczeli ,&nbsp;Z. Weltsch","doi":"10.1016/j.ijadhadh.2025.104068","DOIUrl":"10.1016/j.ijadhadh.2025.104068","url":null,"abstract":"<div><div>As the use of aluminum structures grows due to their lightweight properties and sustainability advantages, optimizing bonding technologies is essential for ensuring strong and durable joints. This study systematically evaluates fourteen surface treatment methods applied to aluminum sheets and L-section joints, assessing their influence on adhesion performance.</div><div>Surface preparation significantly impacted bond strength. Veil sanding combined with Sika® Primer-207 led to an 82 % increase in tensile strength and a 258 % increase in shear strength compared to untreated surfaces. Laser and hot deionized water treatments resulted in the highest measured surface energy (88 mN/m), improving wettability and adhesive-substrate interaction.</div><div>To analyze bonding performance, a flexible polyurethane adhesive was applied to structural joints, which were tested under tensile and shear stress conditions. The results demonstrated that surface roughness, free energy, and chemical modification strongly influence failure modes. While untreated surfaces predominantly exhibited adhesive failure, optimized treatments shifted failure toward cohesive failure, indicating a stronger interfacial bond.</div><div>Additionally, the correlation between surface free energy, surface roughness, and adhesive strength was examined to understand their combined effects on joint performance. The findings highlight the importance of selecting appropriate surface modification techniques to maximize adhesion and joint durability.</div><div>This research provides practical insights for industries relying on aluminum bonding, offering guidance on optimizing surface treatment protocols to enhance structural integrity and long-term reliability in demanding applications.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"142 ","pages":"Article 104068"},"PeriodicalIF":3.2,"publicationDate":"2025-05-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144205388","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Enhancing interfacial bonding and mechanical properties of CF/EP composites through low-temperature jet plasma treatment 低温喷射等离子体处理增强CF/EP复合材料的界面结合和力学性能
IF 3.2 3区 材料科学
International Journal of Adhesion and Adhesives Pub Date : 2025-05-20 DOI: 10.1016/j.ijadhadh.2025.104067
Shiyun Lin , Bei Ye , Chenyun Peng , Menghao Ran , Donghang Jie , Yuhuan Du , Dagang Yin
{"title":"Enhancing interfacial bonding and mechanical properties of CF/EP composites through low-temperature jet plasma treatment","authors":"Shiyun Lin ,&nbsp;Bei Ye ,&nbsp;Chenyun Peng ,&nbsp;Menghao Ran ,&nbsp;Donghang Jie ,&nbsp;Yuhuan Du ,&nbsp;Dagang Yin","doi":"10.1016/j.ijadhadh.2025.104067","DOIUrl":"10.1016/j.ijadhadh.2025.104067","url":null,"abstract":"<div><div>Carbon fiber reinforced epoxy (CF/EP) composites are widely employed in aerospace, automotive, and maritime industries. However, the inherently smooth surface and low chemical reactivity of carbon fibers compromise the interfacial bonding with epoxy resin. This study examines the effect of low-temperature jet plasma treatment at various processing speeds (25, 50, 100, and 200 mm/s) on the surface characteristics of carbon fibers and the mechanical performance of CF/EP composites. A treatment rate of 50 mm/s was found to optimally enhance fiber surface roughness and promote the formation of -C=O functional groups—evidenced by a decrease in carbon content from 75.51 % to 73.27 % and an increase in oxygen content from 24.49 % to 26.73 %. Consequently, composites fabricated under these conditions exhibited notable improvements in bending strength (522.28 MPa, +19.23 %), bending modulus (33.22 GPa, +50.38 %), tensile strength (610.62 MPa, +40.35 %), and tensile modulus (27.94 GPa, +38.59 %). Scanning electron microscopy further confirmed enhanced interfacial bonding through a reduction in voids. This concise study provides experimental evidence for optimizing carbon fiber surface treatments to achieve superior composite performance.</div></div>","PeriodicalId":13732,"journal":{"name":"International Journal of Adhesion and Adhesives","volume":"141 ","pages":"Article 104067"},"PeriodicalIF":3.2,"publicationDate":"2025-05-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144116698","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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