Xuedong Chen , Guoqiang Chen , Mengjiao Li , Zixiang Liu , Wenxue Dai , Fan Wang , Haibo Zhang , Fei Liu , Youshuang Zhu
{"title":"Structural characterization, biological activities, and rheological behavior of an exopolysaccharide from tea-bacteria Herbaspirillum sp. S-1","authors":"Xuedong Chen , Guoqiang Chen , Mengjiao Li , Zixiang Liu , Wenxue Dai , Fan Wang , Haibo Zhang , Fei Liu , Youshuang Zhu","doi":"10.1016/j.carpta.2025.100842","DOIUrl":"10.1016/j.carpta.2025.100842","url":null,"abstract":"<div><div>The investigation of polysaccharides derived from microorganisms is significant due to the exceptional advantages offered by microbial exopolysaccharides (EPSs). We explored the isolation, purification, preliminary structure characterization, and potential applications of an exopolysaccharide (HS, 6.68 g/L) produced by <em>Herbaspirillum</em> sp. S-1. Through DEAE Sepharose fast flow column chromatography and Sephacryl S-200, we obtained a single fraction of the exopolysaccharide (S-1). Monosaccharide composition analysis revealed that S-1 mainly consisted of D-mannose, D-glucose, and D-galactose, with an average molecular weight of 4.995 × 10<sup>3</sup> g/mol, respectively. Further analyzes indicated that the main chain repeating unit of S-1 was →4)-α-D- Manp-(1→6)-β-D-Galp-(1→3)-α-D-Glcp-(1→6)-β-D-Galp-(1→3)-α-D-Glcp-(1→6)-β-D-Galp-(1→. Moreover, the <em>in vitro</em> determination of antioxidant activities demonstrated that S-1 exhibited notable antioxidant properties, with ∼85.6 %. S-1 has high activity in inhibiting α-glucosidase (∼52.79 %) and α-amylase (∼46.26 %). HS and S-1 exhibited anti-proliferative effects on HT-29 and BEL-7402 cells, whereas S-1 had higher anti-proliferative activity than HS. Furthermore, it exhibited good synergistic thickening performance with sclerotium gum. Consequently, the S-1 exopolysaccharide has potential for application as a natural antioxidant and additive in functional food and related industries.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100842"},"PeriodicalIF":6.2,"publicationDate":"2025-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144071576","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Cold plasma-enhanced polylactic acid/chitosan films incorporating zein nanoparticles: a promising strategy for developing food packaging materials","authors":"Mahdi Norozi , Seyed Hadi Peighambardoust , Sirous Khorram , Hamed Hamishehkar","doi":"10.1016/j.carpta.2025.100852","DOIUrl":"10.1016/j.carpta.2025.100852","url":null,"abstract":"<div><div>This study developed packaging films using polylactic acid (PLA) and chitosan incorporated with zein nanoparticles (Z-NPs) for active packaging applications. Dielectric barrier discharge (DBD) air plasma treatment was applied to improve adhesion between PLA and the nanocomposite film, resulting in a bilayer film. The plasma treatment reduced the water contact angle from 98.2° to 42.6° and increased surface roughness from 19.75 nm to 31.5 nm, as confirmed by atomic force microscopy. The optimally plasma-treated PLA showed an 80 % increase in tensile strength, while the bilayer film exhibited improved water vapor permeability of 0.64 × 10<sup>−7</sup> g/m.h.Pa. The incorporation of 15 % Z-NPs into the chitosan matrix enhanced the mechanical properties, with a 20 % increase in tensile strength and a 15 % decrease in water vapor permeability. The bilayer film demonstrated a 40 % increase in tensile strength and a 30 % decrease in water vapor permeability compared to the neat PLA film. Additionally, the bilayer film showed enhanced antibacterial activity against <em>S. aureus</em>, with a 6 mm inhibition zone. The results demonstrate that the combination of plasma treatment and Z-NPs incorporation significantly enhances the properties of biodegradable packaging materials, offering a sustainable alternative for the food industry with improved mechanical and barrier properties.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100852"},"PeriodicalIF":6.2,"publicationDate":"2025-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144089601","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Hurong Ge , Peipei Ma , Qing Huang , Shijie Wei , Zhizhong Wang
{"title":"Cyclodextrin host-guest complexes-derived exosomal miRNAs for enhancing the antifatigue effects of resveratrol","authors":"Hurong Ge , Peipei Ma , Qing Huang , Shijie Wei , Zhizhong Wang","doi":"10.1016/j.carpta.2025.100832","DOIUrl":"10.1016/j.carpta.2025.100832","url":null,"abstract":"<div><div>Objectives: To study the encapsulation of resveratrol by three cyclodextrin derivatives, investigate the impact of encapsulation technology on its anti-fatigue effect, and explore the anti-fatigue mechanism of the encapsulated resveratrol via transcriptomics analysis of exosomal miRNAs. Methods (1) UV spectroscopy and nuclear magnetic resonance (NMR) were used to investigate the encapsulation and encapsulation modes of resveratrol by <em>β</em>-CD, HP-<em>β</em>-CD and CM-<em>β</em>-CD; and the phase solubility method was used to calculate the solubilisation multiplicity of resveratrol by the three cyclodextrin derivatives. (2) Male C57BL/6 J mice were randomly divided into: fatigue model group (FM), FM+resveratrol group (SF+Res), FM+<em>β</em>-CD, FM+HP-<em>β</em>-CD, FM+CM-<em>β</em>-CD, FM+<em>β</em>-CD+Res, FM+HP-<em>β</em>-CD+Res, FM+CM-<em>β</em>-CD +Res, and after 30 days of rearing, the mice were subjected to exhaustion swimming experiment to detect fatigue-related indexes and observe the effects of the three cyclodextrin derivatives on the anti-fatigue effects of resveratrol. (3) Male C57BL/6 J mice were randomly divided into Control, FM, and FM+HP-<em>β</em>-CD+Res. After 30 days of rearing, except for the Control group, the remaining mice were subjected to exhaustion swimming experiments, and exosomes were extracted from cardiac tissue, skeletal muscle tissue, and liver tissue of the three groups of mice, and the transcriptomics technology was applied to sequence the exosomal miRNAs and to explore the mechanism of the effect of the HP-<em>β</em>-CD+Res envelope on fatigue. Results (1) The inclusion ratios of <em>β</em>-CD, HP-<em>β</em>-CD, and CM-<em>β</em>-CD encapsulated resveratrol were 1:1, 1:2, and 1:1, and the solubilisation multiplicities of resveratrol were 23, 39, and 21 fold, respectively; <em>β</em>-CD and CM-<em>β</em>-CD encapsulated Res, which was the benzene ring with two hydroxyl‑terminal ends of Res entered the cavity from the small-ported end of the cyclodextrins; HP-<em>β</em>-CD encapsulated Res, which was the Res containing one hydroxyl‑terminated benzene ring enters the cavity from the wide-mouth end of HP-β-CD. (2) Compared with the FM+Res group, all three inclusions were able to prolong the exhaustion swimming time of mice, with HP-<em>β</em>-CD+Res being the most effective. (3) After HP-<em>β</em>-CD+Res acted on the fatigued mouse model, cardiac tissue showed 1726 differentially expressed exosomal miRNAs, of which 840 were up-regulated and 886 were down-regulated, reversing the fatigue-induced changes in 64.96 % of the exosomal miRNAs (1170 shared differential exosomal miRNAs); Skeletal muscle tissue showed 1948 differentially expressed exosomal miRNAs, of which 718 were up-regulated and 1230 were down-regulated, reversing 80.57 % of the fatigue-induced changes in exosomal miRNAs (1576 shared differential exosomal miRNAs); Liver tissue showed 1442 differentially expressed exosomal miRNAs, of which 4","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100832"},"PeriodicalIF":6.2,"publicationDate":"2025-05-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144089600","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Evmorfia Athanasopoulou , Enrico Maurizzi , Francesco Bigi , Andrea Quartieri , Andrea Pulvirenti , Theofania Tsironi
{"title":"Comparative effect of different plasticizers on physicochemical properties of hydroxypropyl methyl cellulose (HPMC)- based films appropriate for gilthead seabream packaging","authors":"Evmorfia Athanasopoulou , Enrico Maurizzi , Francesco Bigi , Andrea Quartieri , Andrea Pulvirenti , Theofania Tsironi","doi":"10.1016/j.carpta.2025.100839","DOIUrl":"10.1016/j.carpta.2025.100839","url":null,"abstract":"<div><div>The selection of adequate plasticizers to synthesize biopolymer biodegradable and edible films for food packaging is crucial to develop materials with appropriate barriers, mechanical and physicochemical properties. The aim of the study was to develop hydroxypropyl methyl cellulose (HPMC) based films with hydrophilic and hydrophobic plasticizers and evaluate their effectiveness as green packaging materials for gilthead seabream fillets. Mechanical properties, water barrier, surface hydrophobicity, optical and UV–visible barrier properties were determined. The films produced were transparent with excellent optical appearance and good preventive ability against UV radiation. HPMC based films with glycerol as plasticizer were more compact and had lower thickness (45.43±3.33 μm) and higher young’s modulus, indicating stiffer, less flexible films (1613.22±492.88 MPa). In contrast, films plasticized with oleic acid had the highest elongation at break (30.35±4.21 %), indicating greater flexibility. The films with glycerol were hydrophilic (contact angle equal to 81.47±6.65°) while the films with fatty acids (oleic and linoleic acid) were hydrophobic (contact angle > 90°). The hydrophobic films had also better water barriers compared to films with glycerol. All tested packaging materials resulted in similar preservative effect on packed gilthead seabream fillets, leading in shelf life 7–8 days at 2 °C. The results of the study show the potential of the developed biodegradable films to replace the conventional synthetic petroleum based materials in fresh fish packaging.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100839"},"PeriodicalIF":6.2,"publicationDate":"2025-05-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144068116","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Xueyi Jing , Weiyue Li , Yang Gao , Xin Qiao , Yufei Cheng , Wenjuan Zhang , Lei Pu , Hua Yang , Jianbin Zhang , Liang Hong
{"title":"Propyl inulin nanoprebiotics as a synbiotic partner of Lactiplantibacillus plantarum for Inhibiting pathogenic infection in a mouse model","authors":"Xueyi Jing , Weiyue Li , Yang Gao , Xin Qiao , Yufei Cheng , Wenjuan Zhang , Lei Pu , Hua Yang , Jianbin Zhang , Liang Hong","doi":"10.1016/j.carpta.2025.100837","DOIUrl":"10.1016/j.carpta.2025.100837","url":null,"abstract":"<div><div><em>Listeria monocytogenes</em> (LM) can proliferate significantly under refrigeration conditions, impacting food storage and safety for humans. This study investigated the effects of different forms of inulin on the antibacterial properties of lactic acid bacteria. Initially, propionylated inulin (IPr) and propyl-inulin nanoparticles (PIN) were synthesized and characterized. Characterization revealed that IPr had an irregular shape, while PIN exhibited a regular spherical structure, with a particle size of 949.7 and 434.4 nm, respectively. The zeta potential of PIN was measured at -51.16 mV. Subsequently, the effects of IPr and PIN on <em>Lactiplantibacillus plantarum</em> (LP) were studied, demonstrating that neither compound negatively affected LP's growth, but both significantly enhanced its antimicrobial activity. Animal studies indicated that LP and PIN had a considerable <em>in vivo</em> antimicrobial impact. They effectively repaired intestinal barrier damage caused by pathogens, alleviated liver injury, regulated immune responses, and restored gut microbiota composition. This study highlights the potent antimicrobial properties of enhanced nanoprebiotics and LP-based synbiotics, which inhibit the growth of psychrotrophic bacteria and promote animal gut health. The study innovatively develops nanoprebiotic-enhanced synbiotics, effectively combating infections, restoring gut health, and offering novel insights for creating additives to improve livestock product quality and shelf life.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100837"},"PeriodicalIF":6.2,"publicationDate":"2025-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143942457","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Glutaraldehyde crosslinked chitosan-β-cyclodextrin/ZnO composite for the effective adsorption of Congo red anionic dye: A glimpse into adsorption performance and ANN modeling","authors":"Ruksana Sirach, Pragnesh N Dave","doi":"10.1016/j.carpta.2025.100835","DOIUrl":"10.1016/j.carpta.2025.100835","url":null,"abstract":"<div><div>Removal of azo dyes is of great concern because of their large contribution in dye industry and persistent toxic nature. Congo red (CR), an anionic azo dye, poses significant environmental hazards to aquatic and terrestrial ecosystems. This study explores the use of a positively charged adsorbent composite for the effective removal of CR via adsorption. Chitosan (CS) based composite, CS-GA-<em>β</em>-CD/ZnO, was synthesized by grafting <em>β</em>-cyclodextrin (<em>β</em>-CD) onto cationic CS using glutaraldehyde (GA) in the presence of ZnO nanoparticles. The composite’s physicochemical characteristics were evaluated using various analytical techniques. The effects of pH, contact time, temperature, initial CR concentration, and adsorbent dosage on CR removal were systematically investigated through isotherm, kinetic, and thermodynamic analyses. The composite demonstrated high adsorption efficiency, particularly at adsorbent dosages ≥30 mg, with optimal performance under acidic conditions due to its enhanced surface positivity. The presence of salts had minimal impact on adsorption efficiency, confirming the robustness of the material. Thermodynamic studies indicated spontaneous adsorption within 300 minutes. The adsorption behavior was best described by Liu, Dubinin-Radushkevich (D-R), and Langmuir isotherm models, with a maximum capacity (i.e., Langmuir qₘ) of 337 ± 13 mg g⁻¹ at <em>T</em> = 30 °C. The composite retained over 93% of its adsorption efficiency after five regeneration cycles, highlighting its reusability. Moreover, an artificial neural network (ANN) model provided accurate predictive capability with an R² > 0.995. These findings underscore the potential of CS-GA-<em>β</em>-CD/ZnO as a cost-effective, environmentally friendly, and scalable adsorbent for CR removal from wastewater. CS-GA-<em>β</em>-CD/ZnO is not explored for its adsorption potential and therefore, the outcome of the present work can advance the knowledge in the field of achieving good dye removal from the aqueous solution using composite materials. The study also highlights leaching of composite adsorbent after prolonged contact period under highly acidic and basic conditions.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100835"},"PeriodicalIF":6.2,"publicationDate":"2025-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144068552","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Huy Vu Duc Nguyen, Angus C.L.A. Crampton, Daniel F. Schmidt, Tim Huber
{"title":"Evaluating ultra-fine friction grinding for the continuous production of nanofibrillated cellulose","authors":"Huy Vu Duc Nguyen, Angus C.L.A. Crampton, Daniel F. Schmidt, Tim Huber","doi":"10.1016/j.carpta.2025.100838","DOIUrl":"10.1016/j.carpta.2025.100838","url":null,"abstract":"<div><div>Nanofibrillated cellulose (NFC) has diverse applications, but economical large-scale production with minimized ecological footprint remains challenging. A Masuko Supermasscolloider was modified for continuous processing using a pump-controlled circulating system, an in-line viscosimeter, and power consumption meters. Utilizing the upgraded system, we investigated NFC production from <em>Miscanthus</em> biomass under various conditions: different initial cellulose concentrations (1, 1.5, and 2 wt%), process volumes (15 and 25 L) and different grinding times (15–120 min, 15 min intervals). Particle size analysis showed equivalent hydrodynamic diameters of 200–300 nm regardless of processing conditions. Notably, our approach demonstrated 70 % reduction in specific energy consumption by simultaneously increasing process volume from 15 L to 25 L and initial cellulose concentration from 1 wt% to 2 wt%. Additionally, NFC produced at different grinding times was used to prepare carboxymethyl cellulose nanocomposites. Tensile testing demonstrated the same level of mechanical reinforcement regardless of NFC grinding time, highlighting a clear opportunity to reduce the footprint of NFC production while maintaining performance.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100838"},"PeriodicalIF":6.2,"publicationDate":"2025-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"144068117","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Fabrication of functional edible packaging materials based on carboxymethyl cellulose and pomelo peel powder supplemented with Nisin as active compound","authors":"Andra-Gabriela Zorcă , Nicoleta Chira , Gabriela Olimpia Isopencu , Cristina Busuioc , Ovidiu-Cristian Oprea , Cristina-Ileana Covaliu-Mierlă , Alexandru Cîrîc , Gabriela Toader , Iuliana Mihaela Deleanu","doi":"10.1016/j.carpta.2025.100836","DOIUrl":"10.1016/j.carpta.2025.100836","url":null,"abstract":"<div><div>In this study, functional edible materials were prepared based on citric acid (CA) crosslinked carboxymethylcellulose (CMC), pomelo peel powder (PP), and Nisin. To benefit from agri-food waste that are available, two basic materials have been developed, both containing considerable amounts of PP. The formulations with a CMC:PP ratio of 1:2 (w/w) proved homogenous and compact, having suitable characteristics for edible packaging (EP): film thickness (below 0.2 mm), oxygen permeability (OP) (less than 1.3 meq<sup>.</sup>kg<sup>-1</sup>), reduced water solubility (approximately 40 %), good water vapor transmission rate (WVTR) (between 21.7 and 22.9 g<sup>.</sup>m<sup>2.</sup>h<sup>-1</sup>), and acceptable mechanical strength (3.4 MPa). Due to its complex composition, PP also contributes to antioxidant activity of films (approx. 130 µmol Trolox<sup>.</sup>g<sup>-1</sup>). A comparative analysis showed that increasing PP content (CMC:PP 1:4) has negative effects on morphological characteristics and on films’ properties because of pores formation and particle agglomeration. Nisin, used for its bio-preservation ability, had little effect on physico-chemical properties of films, being added in low concentration in all formulations. Due to Nisin and PP content the antibacterial activity of the composite packaging materials proved successful against <em>B. subtilis</em>, a Gram-positive bacterium and <em>Escherichia coli</em>, a Gram-negative bacterium.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100836"},"PeriodicalIF":6.2,"publicationDate":"2025-05-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143942347","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Minocycline Hydrochloride-infused Polyvinyl alcohol/ pectin-based bio-nanocomposite antibacterial hydrogel films reinforced with nanofibrillar cellulose from biomass for preventing bactericidal infections in wound dressings","authors":"Jijo Thomas Koshy, D Sangeetha","doi":"10.1016/j.carpta.2025.100831","DOIUrl":"10.1016/j.carpta.2025.100831","url":null,"abstract":"<div><div>The wound healing process is typically susceptible to a variety of bacterial infections as a result of the challenging physiological environment, which significantly impedes wound healing. Topical antibiotic use is not recommended for wound healing, as excessive use can lead to bacterial resistance, posing serious risks to human health. Antibiotic-infused wound dressings offer a promising approach to address the limitations of conventional wound care. Cellulose nanofibrils (CNF) are biocompatible, renewable, and naturally occurring materials that have been extensively used as innovative, sustainable reinforcing nanofillers in polymer composites. In this article, we extracted CNF from a plant-based source, <em>Sida rhombifolia</em>. The CNF extracted were characterized using XRD, FTIR and TEM. Using CNF-based nanofillers in Polyvinyl alcohol and Pectin bio nanocomposites exhibit enhanced physical and mechanical characteristics (6.85 ± 0.84 MPa). The nanofiller-reinforced polymer films were non-cytotoxic, showed excellent cell proliferation (105.21 ± 1.71 at 72 h), and effectively inhibited biofilm formation by <em>S. aureus</em> and <em>P. aeruginosa</em>, outperforming the GTR membrane. The biodegradability of all film formulations was assessed, showing an average enzymatic degradation of 55.2 ± 2.3 % and environmental degradation of 60.1 ± 1.8 % over the testing period. The overall results confirm that the developed PVA/PEC<img>CNF-Min hydrogel films show excellent potential as wound dressing materials, with strong antibacterial and wound healing properties.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100831"},"PeriodicalIF":6.2,"publicationDate":"2025-05-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143931444","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Jinhua Zhang , Jichen Su , Xinyi Liu , Min Chen , Baoqing Bai , Yukun Yang , Sanhong Fan , Tao Bo
{"title":"Preparation and characterization of carboxymethyl cellulose-based edible thin films loaded with rosmarinic acid and citral nanoparticles","authors":"Jinhua Zhang , Jichen Su , Xinyi Liu , Min Chen , Baoqing Bai , Yukun Yang , Sanhong Fan , Tao Bo","doi":"10.1016/j.carpta.2025.100821","DOIUrl":"10.1016/j.carpta.2025.100821","url":null,"abstract":"<div><div>This study aimed to prepare a CS-TPP nanoparticle loaded with rosmarinic acid and citral and to evaluate the overall performance of the novel antimicrobial film prepared by the addition of the nanoparticles to the CMC film. The structure of the nanoparticles was determined by particle size potentiometry, SEM, and FTIR, and it was demonstrated that rosemarinic acid and citral were successfully combined with CS-TPP nanoparticles with a particle size of 446.2 nm. The surface morphology and mechanical properties of the films were determined by texture instrumentation, SEM, FTIR, and XRD.The CMC-XT showed a tensile strength of 9.30 N/mm² (49 % higher than the blank film, 6.23 N/mm²) and an elongation at break of 175 %, surpassing the CMC-RA (6.58 N/mm²). The antibacterial performance experiment showed that the inhibition rates of CMC-XT on E.coli and S.aureus were 69.4 % and 61.9 %, respectively, which were significantly better than the blank membrane (9.2 %).The experiment provides a new type of film that combines mechanical strength, antibacterial performance, and environmental friendliness for food preservation, solving the safety issues of traditional chemical preservatives and the cost limitations of physical preservation technology.As well as it utilizes natural antimicrobial agents and biodegradable polymers, reducing reliance on traditional chemical preservatives that may pose health risks or environmental concerns.</div></div>","PeriodicalId":100213,"journal":{"name":"Carbohydrate Polymer Technologies and Applications","volume":"10 ","pages":"Article 100821"},"PeriodicalIF":6.2,"publicationDate":"2025-05-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143942455","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}