Fibers and Polymers最新文献

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Mechanical, Viscoelastic and Soil Degradation Performance of Hemp Fiber Reinforced Bio-PBS Composites Developed via Microwave Processing 微波法制备麻纤维增强生物pbs复合材料的力学、粘弹性和土壤降解性能
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-17 DOI: 10.1007/s12221-025-00944-x
Aatish Sharma, Sunny Zafar, Chandrakant K. Nirala
{"title":"Mechanical, Viscoelastic and Soil Degradation Performance of Hemp Fiber Reinforced Bio-PBS Composites Developed via Microwave Processing","authors":"Aatish Sharma,&nbsp;Sunny Zafar,&nbsp;Chandrakant K. Nirala","doi":"10.1007/s12221-025-00944-x","DOIUrl":"10.1007/s12221-025-00944-x","url":null,"abstract":"<div><p>This study focuses on bio-based natural fiber-reinforced polymer composites (NFRPCs). In this work, bio-polybutylene succinate (bio-PBS) reinforced with hemp fibers (HF) varying at 10 wt%, 20 wt%, and 30 wt% were developed via microwave-assisted compression moulding (MACM) technique. The mechanical properties, crystalline properties, dynamic mechanical analysis, and soil degradation behaviour of these composites were analysed. The study demonstrated that composites with 30 wt% hemp fiber content exhibited the most optimal mechanical properties, with crystallinity increasing by 22%. These composites achieved the highest storage modulus of 13,349 MPa, while their loss modulus was found to be 110% higher compared to neat bio-PBS. Additionally, soil burial experiments revealed that the 30 wt% HF/bio-PBS composites underwent the greatest weight loss after 60 days of soil exposure, indicating superior biodegradability compared to the pure bio-PBS matrix. The work further concluded that hemp fiber-reinforced bio-PBS composites showcased improved mechanical performance, crystallinity, biodegradability, and processing characteristics, surpassing other bio-composite alternatives.</p><h3>Graphical Abstract</h3><div><figure><div><div><picture><source><img></source></picture></div></div></figure></div></div>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"2175 - 2188"},"PeriodicalIF":2.2,"publicationDate":"2025-04-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879615","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Enhancement of Antifouling and Antibacterial Properties of Biosynthesis Silver Nanoparticles from Parkia speciosa (Stink Bean) Polysulfone Mixed Matrix Membrane 臭豆聚砜混合基质膜生物合成纳米银的防污抑菌性能
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-17 DOI: 10.1007/s12221-025-00925-0
Faiz Hafeez Azhar, Zawati Harun, Khairul Nazri Yusof, Siti Aida Ibrahim, Rosniza Hussin, Hatijah Basri, Siti Salwa Alias, Nur Hanis Hayati Hairom
{"title":"Enhancement of Antifouling and Antibacterial Properties of Biosynthesis Silver Nanoparticles from Parkia speciosa (Stink Bean) Polysulfone Mixed Matrix Membrane","authors":"Faiz Hafeez Azhar,&nbsp;Zawati Harun,&nbsp;Khairul Nazri Yusof,&nbsp;Siti Aida Ibrahim,&nbsp;Rosniza Hussin,&nbsp;Hatijah Basri,&nbsp;Siti Salwa Alias,&nbsp;Nur Hanis Hayati Hairom","doi":"10.1007/s12221-025-00925-0","DOIUrl":"10.1007/s12221-025-00925-0","url":null,"abstract":"<p>Green biosynthesis of silver nanoparticles (bio-AgNPs) provides an eco-friendly and effective approach to enhance the antibacterial performance and biofouling resistance of mixed-matrix membranes (MMMs). In this study, bio-AgNPs were synthesized using <i>Parkia speciosa</i> (Stink Bean) leaf extract as a reducing agent for silver nitrate and were incorporated into polysulfone (PSf) MMM to create bio-AgNP/PSf MMM. The antibacterial and antifouling properties of the bio-AgNP/PSF MMMs were compared with those of pristine PSf membranes and commercial AgNP/PSF MMMs. As a result, bio-AgNPs significantly increased hydrophilicity with contact angles of 65°, compared to 67° for AgNP/PSF MMM and 88° for the pristine PSf membrane. Surface roughness increased to 26.09 nm (bio-AgNP/PSf MMM) and 25.27 nm (AgNP/PSf MMM) from 3.73 nm (pristine). Meanwhile, pure water flux (PWF) results showed that bio-AgNP/PSf MMM achieved 248.7 L (m<sup>2</sup> h)<sup>−1</sup>, compared to 239.5 L (m<sup>2</sup> h)<sup>−1</sup> for AgNP/PSf MMM and 84.2 L (m<sup>2</sup> h)<sup>−1</sup> for pristine PSf membrane. The rejection rates were 98% for the bio-AgNP/PSF MMM and 97% for the AgNP/PSF MMM. The bio-AgNPs/PSf MMM produced a larger inhibition zone (&gt; 6 nm) against <i>Escherichia coli</i> (<i>E. coli</i>) than AgNPs/PSf MMM (&lt; 6 nm), which was attributed to flavonoids enhancing the antibacterial properties. Both MMMs showed a flux recovery ratio (FRR) exceeding 80% after physical cleaning and 98% after chemical cleaning, indicating that bio-AgNP incorporation significantly improved the antibacterial and antifouling properties of MMMs.</p>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"1851 - 1866"},"PeriodicalIF":2.2,"publicationDate":"2025-04-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879614","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Erratum: Magnetic Biochar Production from Agricultural Waste and Reactive Blue 19 Removal by Peroxymonosulfate Activation 更正:从农业废弃物中生产磁性生物炭和通过过氧单硫酸盐活化去除活性蓝19
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-16 DOI: 10.1007/s12221-025-00947-8
Neslihan Kader, Gökçe Didar Değermenci
{"title":"Erratum: Magnetic Biochar Production from Agricultural Waste and Reactive Blue 19 Removal by Peroxymonosulfate Activation","authors":"Neslihan Kader,&nbsp;Gökçe Didar Değermenci","doi":"10.1007/s12221-025-00947-8","DOIUrl":"10.1007/s12221-025-00947-8","url":null,"abstract":"","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"2259 - 2262"},"PeriodicalIF":2.2,"publicationDate":"2025-04-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879610","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of Glycolic Acid and Ethanolamine on Preparation of Hemp Fibers in a Cascade Organosolv Degumming Process 乙醇酸和乙醇胺对级联有机溶剂脱胶法制备大麻纤维的影响
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-16 DOI: 10.1007/s12221-025-00935-y
Lingyu Wang, Wenying Xia, Boya Li, Kai Nie, Chengfeng Zhou, Yuanming Zhang, Guangting Han, Wei Jiang, Haoxi Ben, Tao Zhao
{"title":"Effect of Glycolic Acid and Ethanolamine on Preparation of Hemp Fibers in a Cascade Organosolv Degumming Process","authors":"Lingyu Wang,&nbsp;Wenying Xia,&nbsp;Boya Li,&nbsp;Kai Nie,&nbsp;Chengfeng Zhou,&nbsp;Yuanming Zhang,&nbsp;Guangting Han,&nbsp;Wei Jiang,&nbsp;Haoxi Ben,&nbsp;Tao Zhao","doi":"10.1007/s12221-025-00935-y","DOIUrl":"10.1007/s12221-025-00935-y","url":null,"abstract":"<div><p>In an attempt to implement eco-friendly degumming for preparation of hemp fibers, this study developed a cascade organosolv degumming method employing the advantages of both organic acids and organic bases without using any inorganic alkaline reagents. The cascade degumming improved the hemicellulose and lignin removal rates by 20.1% and 139.8%, respectively, under low temperature (≤ 110 °C) and short reaction time (≤ 3 h). The different mechanism of lignin removal by GA and ETA was verified. The FTIR result showed that GA mainly acted on removal of G-type lignin, while ETA mostly removed S-type lignin. In addition, the FTIR and solid-state <sup>13</sup>C NMR results revealed that the esterification induced by GA was eliminated by ETA in the cascade degumming process. The HSQC NMR result confirmed that the cascade degumming process mainly acted on β-β bond, while β-O-4 bond was relatively preserved. Although the hemp fibers of the cascade degumming exhibited slightly lower tensile strength, the cascade degumming contributed to finer hemp fiber diameter (10.09 dtex) than the alkaline degummed fibers (12.66 dtex). Thus, the cascade degumming has favorable effects in removing gum components and achieving better fiber separation.</p></div>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"1993 - 2005"},"PeriodicalIF":2.2,"publicationDate":"2025-04-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879609","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
How do Printing Parameters Influence the Tensile Performance of 3D-Printed Lightweight Structures: A Comprehensive Analysis and Optimization Approach? 打印参数如何影响3d打印轻量化结构的拉伸性能:综合分析和优化方法?
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-14 DOI: 10.1007/s12221-025-00940-1
Mahmoud F. Abd El-Halim, Mahmoud M. Awd Allah, Ahmed Ibrahim, Adel Fathy
{"title":"How do Printing Parameters Influence the Tensile Performance of 3D-Printed Lightweight Structures: A Comprehensive Analysis and Optimization Approach?","authors":"Mahmoud F. Abd El-Halim,&nbsp;Mahmoud M. Awd Allah,&nbsp;Ahmed Ibrahim,&nbsp;Adel Fathy","doi":"10.1007/s12221-025-00940-1","DOIUrl":"10.1007/s12221-025-00940-1","url":null,"abstract":"<div><p>3D printing enables the creation of lightweight cellular structures, balancing high strength and stiffness, enabling complex shapes that are challenging to achieve with conventional manufacturing methods. Subsequently, this study seeks to optimize the printing parameters of advanced polylactic acid (PLA+) structures to maximize their mechanical performance under tensile loading. For this reason, four key design parameters, the layer height, the infill pattern structure, the infill density, and the nozzle temperature, each at three levels, were selected. The design of experiments framework has employed the Taguchi approach to determine the ideal parameters for attaining the optimum tensile performance. A number of experiments were carried out using the L9 orthogonal array. Through the largest ultimate tensile strength (<span>(sigma_{{{text{ult}}}})</span>), failure strain (<span>(varepsilon_{{text{f}}})</span>), tensile modulus (<span>(E)</span>), and toughness modulus (<span>(U_{{text{T}}})</span>), the optimal parameters were established. The analysis demonstrated that the studied parameters significantly impact the tensile performance of PLA+. According to the accomplished analysis, infill density has the largest influence on the value of <span>(sigma_{{{text{ult}}}})</span>, <span>(E)</span>, and <span>(U_{{text{T}}} )</span> with an influence percent of 76.072, 85.062, and 55.116%, respectively. However, nozzle temperature has the most significant influence on <span>(varepsilon_{{text{f}}})</span> with 48.668% influence percent. Moreover, the error percentages for <span>(sigma_{{{text{ult}}}})</span>, <span>(varepsilon_{{text{f}}})</span>, <span>(E)</span>, and <span>(U_{{text{T}}})</span> based on the confirmation tests are 2.945, 13.051, 6.480, and 10.520%, respectively.</p></div>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"1879 - 1895"},"PeriodicalIF":2.2,"publicationDate":"2025-04-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879672","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Optimizing Melt-Blowing Nozzles for Small-Diameter Fibers: An Artificial Neural Network Framework 小直径纤维熔喷喷嘴优化:人工神经网络框架
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-10 DOI: 10.1007/s12221-025-00919-y
Ignacio Formoso
{"title":"Optimizing Melt-Blowing Nozzles for Small-Diameter Fibers: An Artificial Neural Network Framework","authors":"Ignacio Formoso","doi":"10.1007/s12221-025-00919-y","DOIUrl":"10.1007/s12221-025-00919-y","url":null,"abstract":"<p>In this study, two feedforward artificial neural networks (ANNs) were trained on experimental data to predict the melt-blowing (MB) fiber diameter of hot-melt adhesive and polypropylene fibers based on process operating conditions and nozzle geometry. These ANNs enabled a sensitivity analysis to investigate the effects of input parameters on the fiber drawing ratio. The results indicate that higher air–polymer flux ratios and extrusion temperatures, along with nozzles having an air impact point close to the nozzle exit and a low polymer-to-air area ratio, facilitate the production of small-diameter fibers. Furthermore, the ANNs incorporated a comprehensive set of input parameters characterizing the melt-blowing process and were trained using cross-validation and regularization techniques to enhance their generalization. This enabled the design of optimized nozzles for small-fiber production. Additionally, a nozzle design optimization framework based on ANNs is proposed to optimize new MB nozzles and enhance existing designs according to established industrial objectives and fiber compositions.</p>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"1933 - 1953"},"PeriodicalIF":2.2,"publicationDate":"2025-04-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879666","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Development of Special Reactive Disperse Dyes for the Coloration of Wool and Nylon-6 Fabrics in Supercritical CO2 羊毛及锦纶6织物超临界CO2染色专用活性分散染料的研制
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-10 DOI: 10.1007/s12221-025-00924-1
Hanan Elsisi, Elham Negm, Tarek Abou Elmaaty, Mayada Shaban, Heba Sorour
{"title":"Development of Special Reactive Disperse Dyes for the Coloration of Wool and Nylon-6 Fabrics in Supercritical CO2","authors":"Hanan Elsisi,&nbsp;Elham Negm,&nbsp;Tarek Abou Elmaaty,&nbsp;Mayada Shaban,&nbsp;Heba Sorour","doi":"10.1007/s12221-025-00924-1","DOIUrl":"10.1007/s12221-025-00924-1","url":null,"abstract":"<div><p>The global textile industry pollutes water significantly, primarily due to the harmful impact of dyeing processes. Researchers have explored different techniques to address this issue, such as utilizing supercritical fluid for dyeing. A new type of reactive disperse dyes has been developed by incorporating a transient anionic sulfatoethylsulfone group. The chemical structure was identified using spectral analysis, encompassing FT-IR, NMR, and elemental analysis. The dyeing process was performed on wool and nylon-6 using supercritical carbon dioxide. The dyed fabrics displayed deep hues and exceptional dye fixation. In the fastness experiments, significant findings were recorded for washing fastness (fading and staining grade of 4–5), rubbing fastness (wet and dry grade of 4–5), sweat (acidic and alkaline), and acceptable light fastness results for all the dyes. A significant improvement in antibacterial activity has been observed for both new dyes and dyed fabrics. The findings demonstrated that the suggested dyeing procedure is highly resistant to washing after five cycles.</p></div>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"2017 - 2029"},"PeriodicalIF":2.2,"publicationDate":"2025-04-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://link.springer.com/content/pdf/10.1007/s12221-025-00924-1.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879665","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Self-Supervised Algorithm for Predicting Data Based on Knitting Direction in Capacitive Strain Stitch Sensors 电容式应变针式传感器中基于编织方向的自监督预测算法
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-09 DOI: 10.1007/s12221-025-00942-z
Ji-seon Kim, Jooyong Kim
{"title":"Self-Supervised Algorithm for Predicting Data Based on Knitting Direction in Capacitive Strain Stitch Sensors","authors":"Ji-seon Kim,&nbsp;Jooyong Kim","doi":"10.1007/s12221-025-00942-z","DOIUrl":"10.1007/s12221-025-00942-z","url":null,"abstract":"<div><p>In this study, the characteristics of knit-based stitch sensors were compared using capacitance and stress values based on the knit direction. The restored predicted data were analyzed using a masked autoencoder algorithm. First, changes in capacitance with respect to strain were compared, followed by a comparison of stress values with respect to strain. The capacitance <span>((C))</span> values reflected differences in the distance between electrodes <span>((d))</span> and the area of the electrodes <span>((A))</span>, with the course direction showing a larger variation. Although the stress values <span>((sigma ))</span> exhibited similar trends in the graph, the comparison using the elastic modulus <span>((E))</span> and Poisson's ratio <span>((nu ))</span> confirmed that the course direction had greater deformation under the same tensile strain. Finally, using the masked autoencoder algorithm, the restoration rate of the original data was measured under 10%, 30%, 50%, and 100% noise levels, showing nearly perfect consistency. These results demonstrate the analysis of knit stitch sensor characteristics and the performance evaluation of the masked autoencoder algorithm.</p></div>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"2221 - 2231"},"PeriodicalIF":2.2,"publicationDate":"2025-04-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879649","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Investigating the Impact of Different Loading Modes on the Mechanical Behavior of a Semi-crystalline Polymer 研究不同加载模式对半结晶聚合物力学行为的影响
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-09 DOI: 10.1007/s12221-025-00934-z
Malika Nouimi, Abdel-Nour Zaim, El Bahri Ould Chikh, Boudjellel Moulai Ali, Hadj Miloud Meddah, Bel Abbes Bachir Bouiadjra
{"title":"Investigating the Impact of Different Loading Modes on the Mechanical Behavior of a Semi-crystalline Polymer","authors":"Malika Nouimi,&nbsp;Abdel-Nour Zaim,&nbsp;El Bahri Ould Chikh,&nbsp;Boudjellel Moulai Ali,&nbsp;Hadj Miloud Meddah,&nbsp;Bel Abbes Bachir Bouiadjra","doi":"10.1007/s12221-025-00934-z","DOIUrl":"10.1007/s12221-025-00934-z","url":null,"abstract":"<div><p>The study delved into the mechanical behavior of high-density polyethylene HDPE when subjected to various loading conditions. To cover a wider range of stress conditions, we performed experiments using notched round bar samples of varying curvature radii, employing a video-controlled tensile testing apparatus. In addition, we explored traditional mechanical loading scenarios such as uniaxial tension/compression, cyclic loading, and simple shear tests to gain deeper insights into their effects on HDPE’s stress response. The mechanical properties were significantly influenced by stress triaxiality, with higher levels leading to more pronounced damage and reduced hardening. Stress triaxiality also played a role in the early necking observed in uniaxial tests, with a more noticeable reduction in diametral deformation at rupture as stress triaxiality increased. An examination of volumetric strain changes showed deformation and damage mechanisms, highlighting the prominence of plastic volumetric strain under high-stress triaxiality. In the case of simple shear, HDPE exhibited limited work hardening but demonstrated increased plastic hardening at higher strain rates in the compression test. Lastly, cyclic tensile tests unveiled a temporary decrease in the elastic modulus linked to cavitation damage, followed by stabilization and eventual augmentation attributed to apparent plastic flow driven by molecular orientation. These findings contribute significantly to our comprehensive understanding of HDPE’s mechanical response, offering valuable insights for a wide range of industrial applications.</p></div>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"1867 - 1877"},"PeriodicalIF":2.2,"publicationDate":"2025-04-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879650","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Covalent Bioincorporation of Chitosan Nanoparticles Containing Eucalyptus and Lavender Essential Oil on Cotton Fabrics 含桉树和薰衣草精油的壳聚糖纳米颗粒在棉织物上的共价生物掺入
IF 2.2 4区 工程技术
Fibers and Polymers Pub Date : 2025-04-09 DOI: 10.1007/s12221-025-00937-w
Fernanda Cristina da Rosa, Pedro Gabriel Valente Silva, Wendhy Carolina Vicente, Marcel Afonso Provenzi, Marília Miotto, Tales da Silva Daitx, Ismael Casagrande Bellettini, Andrea Cristiane Krause Bierhalz, Patrícia Bulegon Brondani, Larissa Nardini Carli
{"title":"Covalent Bioincorporation of Chitosan Nanoparticles Containing Eucalyptus and Lavender Essential Oil on Cotton Fabrics","authors":"Fernanda Cristina da Rosa,&nbsp;Pedro Gabriel Valente Silva,&nbsp;Wendhy Carolina Vicente,&nbsp;Marcel Afonso Provenzi,&nbsp;Marília Miotto,&nbsp;Tales da Silva Daitx,&nbsp;Ismael Casagrande Bellettini,&nbsp;Andrea Cristiane Krause Bierhalz,&nbsp;Patrícia Bulegon Brondani,&nbsp;Larissa Nardini Carli","doi":"10.1007/s12221-025-00937-w","DOIUrl":"10.1007/s12221-025-00937-w","url":null,"abstract":"<div><p>Cotton is one of the most used fibers in the textile sector but is highly prone to microbial growth. Surface functionalization of cotton fabric is an alternative to overcome this problem and grant new properties to this product. This work aimed to develop a new methodology for the surface functionalization of cotton fabric, carrying out bio-oxidation catalyzed by laccases followed by the covalent incorporation of chitosan nanoparticles (CHINPs) containing eucalyptus or lavender essential oil to obtain fabrics with antibacterial properties. The cellulose bio-oxidation process was optimized considering the types of laccase and mediator used. The optimal conditions consisted of using laccase from <i>Pleurotus ostreatus</i>, TEMPO as a mediator, and a post-treatment with 1 mol L<sup>−1</sup> of a NaOH solution. CHINPs were synthesized using the oil-in-water emulsification method followed by ionic gelation. The characterization of the CHINPs confirmed the formation of spherical nanoparticles with diameters ranging from 12 to 40 nm and the presence of encapsulated lavender (12.5%) or eucalyptus essential oil (31.2%). The CHINPs were incorporated into the fabric by reacting the NH<sub>2</sub> groups of chitosan with the COOH groups of the bio-oxidized cellulose, generating a covalent bond. The antibacterial assay with <i>E. coli</i> and <i>S. aureus</i> indicated a reduction in bacterial growth in fabrics functionalized with nanoparticles compared to the non-functionalized one. Furthermore, the CHINPs and essential oils remained on the cotton surface even after at least five washing cycles, showing the effectiveness of the binding of the nanoparticles to the fiber surface.</p></div>","PeriodicalId":557,"journal":{"name":"Fibers and Polymers","volume":"26 5","pages":"1979 - 1992"},"PeriodicalIF":2.2,"publicationDate":"2025-04-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"143879648","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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