Synthesis-Stuttgart最新文献

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4区 化学
Synthesis-Stuttgart Pub Date : 2023-09-07 DOI: 10.1055/s-0040-1720091
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引用次数: 0
Erratum - Synthesis of N -Propargyl Pyrrolylamides and Theoretical Study of Pyrrolylimide Reduction by NaBH 4 N -丙炔基吡咯酰胺的合成及nabh4还原吡咯酰亚胺的理论研究
IF 2.6 4区 化学
Synthesis-Stuttgart Pub Date : 2023-09-07 DOI: 10.1055/s-0040-1720090
Sinan Basceken
{"title":"Erratum - Synthesis of N -Propargyl Pyrrolylamides and Theoretical Study of Pyrrolylimide Reduction by NaBH 4","authors":"Sinan Basceken","doi":"10.1055/s-0040-1720090","DOIUrl":"https://doi.org/10.1055/s-0040-1720090","url":null,"abstract":"","PeriodicalId":49451,"journal":{"name":"Synthesis-Stuttgart","volume":"70 1","pages":""},"PeriodicalIF":2.6,"publicationDate":"2023-09-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84411865","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Bis(pinacoloto)diboran/4-phenyl pyridine system for one-pot photocatalyzed borylation and reduction of aldehyde: synthesis of tavaborole in a flow reactor 双(pinacoloto)diboran/4-苯基吡啶体系的一锅光催化硼化和醛还原:在流动反应器中合成tavaborole
IF 2.6 4区 化学
Synthesis-Stuttgart Pub Date : 2023-09-06 DOI: 10.1055/a-2169-6200
Kankanala Naveen Kumar, Mouzma Mhate, Velayutham Ravichandiran, S. Swain
{"title":"Bis(pinacoloto)diboran/4-phenyl pyridine system for one-pot photocatalyzed borylation and reduction of aldehyde: synthesis of tavaborole in a flow reactor","authors":"Kankanala Naveen Kumar, Mouzma Mhate, Velayutham Ravichandiran, S. Swain","doi":"10.1055/a-2169-6200","DOIUrl":"https://doi.org/10.1055/a-2169-6200","url":null,"abstract":"A photocatalyzed one-pot borylation of haloarene and reduction of aldehyde by cocatalysis of bis(pinacoloto)diboran/4-phenyl pyridine is reported. The reaction was carried out in a flow reactor by irradiating the reaction at 410nm, with residence time of 10 min. The method was successfully applied for the synthesis of tavaborole in a single step with 81% yield.","PeriodicalId":49451,"journal":{"name":"Synthesis-Stuttgart","volume":"2 1","pages":""},"PeriodicalIF":2.6,"publicationDate":"2023-09-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74399390","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Reactions of Benzylboronate Nucleophiles. 苄基硼酸亲核试剂的反应。
IF 2.2 4区 化学
Synthesis-Stuttgart Pub Date : 2023-09-01 Epub Date: 2023-05-08 DOI: 10.1055/a-2072-2754
Timothy J Barker, Andrew Bogatkevich, Dallas W Crowder, Sophia G Gierszal, Jacob C Hayes, Michael R Hollerbach, Richard W Russell
{"title":"Reactions of Benzylboronate Nucleophiles.","authors":"Timothy J Barker, Andrew Bogatkevich, Dallas W Crowder, Sophia G Gierszal, Jacob C Hayes, Michael R Hollerbach, Richard W Russell","doi":"10.1055/a-2072-2754","DOIUrl":"10.1055/a-2072-2754","url":null,"abstract":"<p><p>This short review summarizes our laboratory's development of benzylboronic esters as nucleophiles. Activation of the benzylboronic ester is achieved by irreversible coordination of an alkyllithium Lewis base to form a nucleophilic benzylboronate. This boronate was found to react with aldehydes, imines, ketones and alkyl bromides. A copper catalyst was employed in reactions of the boronate with epoxides and aziridines.</p>","PeriodicalId":49451,"journal":{"name":"Synthesis-Stuttgart","volume":"55 17","pages":"2639-2647"},"PeriodicalIF":2.2,"publicationDate":"2023-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10545366/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41171502","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Linked PDF of Table of Contents 链接的PDF目录
4区 化学
Synthesis-Stuttgart Pub Date : 2023-08-29 DOI: 10.1055/s-0040-1720089
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引用次数: 0
Erratum - Synthesis and Optical Resolution of Inherently Chiral Fluorescent Calix[4]arenes and Their Application in Chiral Recognition 固有手性荧光杯[4]芳烃的合成、光学分辨及其在手性识别中的应用
IF 2.6 4区 化学
Synthesis-Stuttgart Pub Date : 2023-08-17 DOI: 10.1055/s-0040-1720085
Fu Yang, Jun Luo, Yi-Chieh Chen, W. Chung
{"title":"Erratum - Synthesis and Optical Resolution of Inherently Chiral Fluorescent Calix[4]arenes and Their Application in Chiral Recognition","authors":"Fu Yang, Jun Luo, Yi-Chieh Chen, W. Chung","doi":"10.1055/s-0040-1720085","DOIUrl":"https://doi.org/10.1055/s-0040-1720085","url":null,"abstract":"","PeriodicalId":49451,"journal":{"name":"Synthesis-Stuttgart","volume":"42 2 1","pages":"e1 - e1"},"PeriodicalIF":2.6,"publicationDate":"2023-08-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84113399","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Heteroatom-Embedding Annulative π-Extension (Hetero-APEX) Reactions: An Overview 杂原子包埋环性π扩展反应综述
IF 2.6 4区 化学
Synthesis-Stuttgart Pub Date : 2023-08-17 DOI: 10.1055/a-2169-4078
Hideto Ito, Kou P Kawahara, Kenichiro Itami
{"title":"Heteroatom-Embedding Annulative π-Extension (Hetero-APEX) Reactions: An Overview","authors":"Hideto Ito, Kou P Kawahara, Kenichiro Itami","doi":"10.1055/a-2169-4078","DOIUrl":"https://doi.org/10.1055/a-2169-4078","url":null,"abstract":"Heteroatom-embedded polycyclic aromatic compounds (hetero-PACs) are a class of organic compounds contributing to a variety of research fields such as materials science, chemical biology and so on. For applications using hetero-PACs, efficient preparation of hetero-PACs is essential. In particular, reactions transforming unfunctionalized aromatic compounds to hetero-PACs using appropriate heteroatom-containing aromatic compounds (π-extending agents) represent the most ideal way to prepare hetero-PACs. In this review, such heteroatom-embedding annulative π-extension (hetero-APEX) reactions including their reaction mechanisms and scope of substrates are described.","PeriodicalId":49451,"journal":{"name":"Synthesis-Stuttgart","volume":"798 1","pages":""},"PeriodicalIF":2.6,"publicationDate":"2023-08-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85445000","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Linked PDF of Table of Contents 链接的PDF目录
4区 化学
Synthesis-Stuttgart Pub Date : 2023-08-15 DOI: 10.1055/s-0040-1720083
{"title":"Linked PDF of Table of Contents","authors":"","doi":"10.1055/s-0040-1720083","DOIUrl":"https://doi.org/10.1055/s-0040-1720083","url":null,"abstract":"","PeriodicalId":49451,"journal":{"name":"Synthesis-Stuttgart","volume":"10 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-08-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135065281","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
SYNFORM ISSUE 2023/9 Synform issue 2023/9
IF 2.6 4区 化学
Synthesis-Stuttgart Pub Date : 2023-08-15 DOI: 10.1055/s-0040-1720607
M. Zanda
{"title":"SYNFORM ISSUE 2023/9","authors":"M. Zanda","doi":"10.1055/s-0040-1720607","DOIUrl":"https://doi.org/10.1055/s-0040-1720607","url":null,"abstract":"INTERVIEW SYNFORM You are a leading researcher in the field of organic synthesis. Could you tell us more about the importance of that field and your current research activities? Prof. T. S. Lee Since three scientists were awarded the No bel prize on “Electrically conductive plastic” in 2000, tons of organic materials have been developed for electronics and pho to nics. As a result, we can see various information through OLED-based smart phones and laptops. Electro-and photo-active organic materials are synthesized based on organic synthetic techniques, including many coupling reactions like Suzuki, Stille, Yamamoto, and Heck reactions. SYNFORM Please comment on your role as a member of the Associate Board of SynOpen. Prof. T. S. Lee My role is to assist with the rapid publication of high-graded papers. SYNFORM Could you tell us something about yourself outside the lab, such as your hobbies or extra-work interests? Prof. T. S. Lee My hobbies include running, golfing, boxing, watching TV, and reading.","PeriodicalId":49451,"journal":{"name":"Synthesis-Stuttgart","volume":"348 1","pages":"A149 - A166"},"PeriodicalIF":2.6,"publicationDate":"2023-08-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77785565","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis and Immunological Evaluation of Escherichia coli O1- Derived Oligosaccharide–Protein Conjugates toward Avian Pathogenic Escherichia coli O1 Vaccine Development 禽致病性大肠杆菌O1疫苗中大肠杆菌寡糖蛋白偶联物的合成及免疫学评价
4区 化学
Synthesis-Stuttgart Pub Date : 2023-08-10 DOI: 10.1055/a-2152-0255
Katsunori Seki, Takumi Makikawa, Kazunobu Toshima, Daisuke Takahashi
{"title":"Synthesis and Immunological Evaluation of Escherichia coli O1- Derived Oligosaccharide–Protein Conjugates toward Avian Pathogenic Escherichia coli O1 Vaccine Development","authors":"Katsunori Seki, Takumi Makikawa, Kazunobu Toshima, Daisuke Takahashi","doi":"10.1055/a-2152-0255","DOIUrl":"https://doi.org/10.1055/a-2152-0255","url":null,"abstract":"Abstract Avian pathogenic Escherichia coli O1 (APEC O1) is a pathogenic bacterium that causes significant economic losses in the poultry industry and raises concerns about zoonotic infections. The development of effective vaccines against APEC O1 is essential due to antibiotic resistance and the potential for severe symptoms in both chickens and humans. In this context, we have been focusing on the O1A, O1B, and O1C antigen structures derived from E. coli O1 lipopolysaccharide (LPS). In this study, the first synthesis of the pentasaccharide repeating units of the O1B and O1C antigens was successfully achieved. The synthesis and immunological evaluation of their conjugates with bovine serum albumin (BSA) were conducted. Only the O1A-pentasaccharide structure is a glycotope candidate for APEC O1. Keyhole limpet hemocyanin (KLH)–O1A-pentasaccharide conjugate was also synthesized, and its immunogenicity was evaluated by the ELISA assay. The efficient production of antibodies capable of binding to both APEC O1 LPS and the O1A-pentasaccharide structure was observed, indicating that O1A-pentasaccharide is a promising vaccine candidate against APEC O1.","PeriodicalId":49451,"journal":{"name":"Synthesis-Stuttgart","volume":"10 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-08-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135491942","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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