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Crystal structure of dipotassium chlorobromotungstate(IV), K2WCl5.4Br0.6 氯溴钨酸二钾(IV) K2WCl5.4Br0.6的晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.54
Y.-Q. Zheng, K. Peters, H. Schnering
{"title":"Crystal structure of dipotassium chlorobromotungstate(IV), K2WCl5.4Br0.6","authors":"Y.-Q. Zheng, K. Peters, H. Schnering","doi":"10.1524/ZKRI.1997.212.1.54","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.54","url":null,"abstract":"","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"47 1","pages":"54 - 54"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76245981","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of lutetium ytterbium oxide sulfide (1.33/0.67/2/1), Lu1.33Yb0.67O2S lutetium yterysulfide (1.33/0.67/2/1)， Lu1.33Yb0.67O2S晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.49
P. Li, K. Range, M. Andratschke
{"title":"Crystal structure of lutetium ytterbium oxide sulfide (1.33/0.67/2/1), Lu1.33Yb0.67O2S","authors":"P. Li, K. Range, M. Andratschke","doi":"10.1524/ZKRI.1997.212.1.49","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.49","url":null,"abstract":"","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"50 1","pages":"49 - 49"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78704262","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Crystal structure of 2,3-diisocyano-2,3-diphenylbutane, [H3CC(NC)(C6H5)]2 2,3-二异氰酸酯-2,3-二苯基丁烷[H3CC(NC)(C6H5)]的晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.75
K. Peters, E. Peters, H. Schnering, J. Pakusch, Hans-Dieter Beckhaus, C. Rüchardt
{"title":"Crystal structure of 2,3-diisocyano-2,3-diphenylbutane, [H3CC(NC)(C6H5)]2","authors":"K. Peters, E. Peters, H. Schnering, J. Pakusch, Hans-Dieter Beckhaus, C. Rüchardt","doi":"10.1524/ZKRI.1997.212.1.75","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.75","url":null,"abstract":"","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"212 1","pages":"75 - 75"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81289961","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Crystal structure of Ce2O2.5S, an oxidized form of Ce2O2S, from neutron and X-ray powder diffraction 中子和x射线粉末衍射分析Ce2O2S氧化态Ce2O2.5S的晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.24
R. Mauricot, J. Gareh, M. Evain
{"title":"Crystal structure of Ce2O2.5S, an oxidized form of Ce2O2S, from neutron and X-ray powder diffraction","authors":"R. Mauricot, J. Gareh, M. Evain","doi":"10.1524/ZKRI.1997.212.1.24","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.24","url":null,"abstract":"The structure of Ce 2 O 2.5 S, a form of Ce 2 O 2 S oxidized by exposure to air, was determined from combined X-ray and neutron powder diffraction data. The phase retains the trigonal symmetry and the P3m1 space group of the parent compound with cell parameters a = 3.96671(10) A and c = 6.8214(2) A and Z = 1. Refinements of 46 parameters by the Rietveld method, using 80 (X-ray) and 138 (neutron) reflections, led to Rp = 0.102 and R wp = 0.129 (X-ray), Rp = 0.063 and R wp = 0.048 (neutron), R p = 0.086 and R wp = 0.113 (global). The oxidation process is shown to correspond to an insertion of oxygen anions in the hexagonal prismatic bipyramidal cavity of the host structure. These additional oxygen atoms occupy a well defined off centered position of the cage, thereby forming short Ce-O and O-O distances. However, due to the disordered nature of the structure, no precise O-O distances and therefore phase charge balance information have been established.","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"10 1","pages":"24 - 28"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75509597","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Crystal structure of diethyl 4-aza-4-methyll7]- paracyclophane-9,10-dicarboxylate, C19H27NO4 4-氮杂-4-甲基[17]-对环番烷-9,10-二羧酸酯C19H27NO4的晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.71
K. Peters, E. Peters, H. Schnering, S. Meyer-Ahrens, W. Tochtermann
{"title":"Crystal structure of diethyl 4-aza-4-methyll7]- paracyclophane-9,10-dicarboxylate, C19H27NO4","authors":"K. Peters, E. Peters, H. Schnering, S. Meyer-Ahrens, W. Tochtermann","doi":"10.1524/ZKRI.1997.212.1.71","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.71","url":null,"abstract":"","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"48 1","pages":"71 - 72"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74931067","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of diethylammonium 2-(2,6-dichloroanilino)phenylacetate, C18H22Cl2N2O2 2-(2,6-二氯苯胺)苯乙酸二乙基铵C18H22Cl2N2O2的晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.61
R. Pomes-Hernandez, J. Duque-Rodríguez, H. Novoa-de-Armas, R. Toscano
{"title":"Crystal structure of diethylammonium 2-(2,6-dichloroanilino)phenylacetate, C18H22Cl2N2O2","authors":"R. Pomes-Hernandez, J. Duque-Rodríguez, H. Novoa-de-Armas, R. Toscano","doi":"10.1524/ZKRI.1997.212.1.61","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.61","url":null,"abstract":"","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"4 1","pages":"61 - 62"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"72715365","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Crystal structure of 5,6,7,8-tetrahydro-4H-cyclohepta[d]isothiazol-3(2 H)-one 1,1 -dioxide, C8H11NO3S 5,6,7,8-四氢- 4h -环庚[d]异噻唑-3(2h)- 1,1 -二氧化C8H11NO3S的晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.59
B. Schulze, K. Illgen, S. Ng,
{"title":"Crystal structure of 5,6,7,8-tetrahydro-4H-cyclohepta[d]isothiazol-3(2 H)-one 1,1 -dioxide, C8H11NO3S","authors":"B. Schulze, K. Illgen, S. Ng,","doi":"10.1524/ZKRI.1997.212.1.59","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.59","url":null,"abstract":"","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"24 1","pages":"59 - 60"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77733958","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A binuclear oxo-bridged iron(III) complex: structure of {(μ-oxo)-bis[cis-chloro-bis(2,2/ -bipyridyl)iron(lll)]} dichloride • 0.7 n-amyl alcohol solvate 双核氧桥铁(III)配合物:{(μ-氧)-双[顺-氯-双(2,2/ -联吡啶)铁(ll)]}二氯•0.7 n-戊醇溶剂的结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.44
S. R. Choudhury, J. Traquair, J. Vittal
{"title":"A binuclear oxo-bridged iron(III) complex: structure of {(μ-oxo)-bis[cis-chloro-bis(2,2/ -bipyridyl)iron(lll)]} dichloride • 0.7 n-amyl alcohol solvate","authors":"S. R. Choudhury, J. Traquair, J. Vittal","doi":"10.1524/ZKRI.1997.212.1.44","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.44","url":null,"abstract":"The title compound [(μ-O){Fe(C1)(bpy) 2 } 2 ] 2 Cl 2 0.7 C5H 11 OH (bpy = 2,2'-bipyridyl) crystallizes in orthorhombic system with the space group Pnna (No. 52). Crystal data: a = 16.892(2) A, b = 17.656(2) A, c = 16.552(2) A, V = 4936.6(12) A 3 , Z = 4, d calc = 1.286 g.cm -3 . The full-matrix least-squares on F 2 was refined for 1804 reflections with (I > 2σ(I)) and 213 parameters to R1 = 0.0912. A crystallographic 2-fold symmetry is present in the cation, in which the bridging oxygen atom lies on the 2-fold axis and bonded to two Fe atoms. Each iron(III) center has a distorted octahedral geometry with the bpy ligands attached in cis fashion. The Fe-O, Fe-Cl and Fe-N distances respectively are 1.790(2)A, 2.323(3)A and 2.143(8) A-2.279(9)A. Fe-O-Fe angle and the Fe... Fe separations are 167.6(6)° and 3.559(2) A, respectively.","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"27 1","pages":"44 - 47"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"82301880","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Crystal structure of bismuth(III) silicate, Bi4(SiO4)3 铋(III)硅酸盐Bi4(SiO4)3的晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.48
H. Liu, C. Kuo
{"title":"Crystal structure of bismuth(III) silicate, Bi4(SiO4)3","authors":"H. Liu, C. Kuo","doi":"10.1524/ZKRI.1997.212.1.48","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.48","url":null,"abstract":"","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"26 1","pages":"48 - 48"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86532562","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Crystal structure of dicesium hexabromotungstate(IV), Cs 2WBr6 六溴钨酸二铵(IV) c2wbr6的晶体结构
Zeitschrift für Kristallographie - Crystalline Materials Pub Date : 1997-12-01 DOI: 10.1524/ZKRI.1997.212.1.55
Y.-Q. Zheng, K. Peters, H. Schnering
{"title":"Crystal structure of dicesium hexabromotungstate(IV), Cs 2WBr6","authors":"Y.-Q. Zheng, K. Peters, H. Schnering","doi":"10.1524/ZKRI.1997.212.1.55","DOIUrl":"https://doi.org/10.1524/ZKRI.1997.212.1.55","url":null,"abstract":"","PeriodicalId":23855,"journal":{"name":"Zeitschrift für Kristallographie - Crystalline Materials","volume":"130 1","pages":"55 - 55"},"PeriodicalIF":0.0,"publicationDate":"1997-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"78890233","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
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