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Zeitschrift Fur Kristallographie-new Crystal Structures最新文献

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Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α]phenanthren-3-one O-(methacryloyl) oxime, C50H74N2O4 (3E,5S,10S,13S,14S,17Z)-17-乙基-10,13-二甲基十六氢- 3h -环五[α]菲-3-一O-(甲基丙烯酰)肟C50H74N2O4的合成与晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-23 DOI: 10.1515/ncrs-2023-0413
Peng Wei, Jin-Feng Zhao, Juan Zou, Jiang-Hai Ye, Kang He, Hong Xu
{"title":"Synthesis and crystal structure of (3<i>E</i>,5<i>S</i>,10<i>S</i>,13<i>S</i>,14<i>S</i>,17<i>Z</i>)-17-ethylidene-10,13-dimethylhexadecahydro-3<i>H</i>-cyclopenta[<i>α</i>]phenanthren-3-one <i>O</i>-(methacryloyl) oxime, C<sub>50</sub>H<sub>74</sub>N<sub>2</sub>O<sub>4</sub>","authors":"Peng Wei, Jin-Feng Zhao, Juan Zou, Jiang-Hai Ye, Kang He, Hong Xu","doi":"10.1515/ncrs-2023-0413","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0413","url":null,"abstract":"Abstract C 50 H 74 N 2 O 4 , orthorhombic, P 1 (no. 1), a = 7.3320(3) Å, b = 11.8132(4) Å, c = 13.1604(5) Å, α = 99.1910(10)°, β = 95.039(1)°, γ = 95.8560(10)°, V = 1113.06(7) Å 3 , Z = 1, R gt ( F ) = 0.0662, wR ref ( F 2 ) = 0.1655, T = 273(2) K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"29 5","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135365351","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The crystal structure of (E)-4-fluoro-N′-(1-(4-hydroxyphenyl)propylidene)benzohydrazide, C16H15FN2O2 (E)-4-氟- n ' -(1-(4-羟基苯基)丙基)苯并肼C16H15FN2O2的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-23 DOI: 10.1515/ncrs-2023-0404
Juanjuan Wen, Langlang Liu, Wenqiang Tang, Bin Liu
{"title":"The crystal structure of (<i>E</i>)-4-fluoro-<i>N</i>′-(1-(4-hydroxyphenyl)propylidene)benzohydrazide, C<sub>16</sub>H<sub>15</sub>FN<sub>2</sub>O<sub>2</sub>","authors":"Juanjuan Wen, Langlang Liu, Wenqiang Tang, Bin Liu","doi":"10.1515/ncrs-2023-0404","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0404","url":null,"abstract":"Abstract C 16 H 15 FN 2 O 2 , orthorhombic, P 2 1 2 1 2 1 (no. 19), a = 7.2516(6) Å, b = 11.3780(9) Å, c = 17.1177(13) Å, V = 1412.36(19) Å 3 , Z = 4, R gt (F) = 0.0498, wR ref ( F 2 ) = 0.1201, T = 293 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"34 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135365220","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of 1,4-dibromo-2,5-bis(prop-2-yn-1-yloxy)benzene, C12H8Br2O2 1,4-二溴-2,5-二(prop-2-yn-1-yloxy)苯C12H8Br2O2的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-23 DOI: 10.1515/ncrs-2023-0401
Zhi-Yong Wang, Qi-Long Zhang, Xiu-Ming Zhang, Xu Zhou, Xian-Jiong Yang, Hong Xu
{"title":"Crystal structure of 1,4-dibromo-2,5-bis(prop-2-yn-1-yloxy)benzene, C<sub>12</sub>H<sub>8</sub>Br<sub>2</sub>O<sub>2</sub>","authors":"Zhi-Yong Wang, Qi-Long Zhang, Xiu-Ming Zhang, Xu Zhou, Xian-Jiong Yang, Hong Xu","doi":"10.1515/ncrs-2023-0401","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0401","url":null,"abstract":"Abstract C 12 H 8 Br 2 O 2 , monoclinic, P 2 1 / c (no. 14), a = 4.1957(13) Å, b = 13.402(4) Å, c = 11.160(3) Å, β = 99.645(10)°, V = 618.7(3) Å 3 , Z = 2, R gt ( F ) = 0.0287, wR ref ( F 2 ) = 0.0701, T = 273(2) K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"370 2","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135365221","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of 2-amino-4-(2-fluoro-3-(trifluoromethyl)phenyl)-9-methoxy-1,4,5,6-tetrahydrobenzo[h]quinazolin-3-ium chloride, C20H18ClF4N3O 2-氨基-4-(2-氟-3-(三氟甲基)苯基)-9-甲氧基-1,4,5,6-四氢苯并[h]喹唑啉-3-氯化铵的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-11 DOI: 10.1515/ncrs-2023-0374
Lu Yu, Qing-Guo Meng, Gui-Ge Hou, Yong-Jun Liu, Zi-Kai Geng
{"title":"Crystal structure of 2-amino-4-(2-fluoro-3-(trifluoromethyl)phenyl)-9-methoxy-1,4,5,6-tetrahydrobenzo[<i>h</i>]quinazolin-3-ium chloride, C<sub>20</sub>H<sub>18</sub>ClF<sub>4</sub>N<sub>3</sub>O","authors":"Lu Yu, Qing-Guo Meng, Gui-Ge Hou, Yong-Jun Liu, Zi-Kai Geng","doi":"10.1515/ncrs-2023-0374","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0374","url":null,"abstract":"Abstract C 20 H 18 ClF 4 N 3 O, orthorhombic, Pbca (no. 61), a = 12.5254(4) Å, b = 12.6845(5) Å, c = 24.1490(11) Å, V = 3836.8(3) Å 3 , Z = 8, R gt ( F ) = 0.0485, wR ref ( F 2 ) = 0.1343, T = 293 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"21 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136059088","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of diethyl 1,9-bis(4-fluorophenyl)-4,6-diphenylhexahydro-3H-2,7,3,5-(epimethanetriyliminomethanetriyl)cyclopenta [b]pyridine-3,7(2H)-dicarboxylate, C40H36F2N2O4 二乙基1,9-二(4-氟苯基)-4,6-二苯基六氢- 3h -2,7,3,5-(epimethanetriyliminomethanetriyl)环五[b]吡啶-3,7(2H)-二羧酸C40H36F2N2O4的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-11 DOI: 10.1515/ncrs-2023-0388
Zi-Ang Zhang, Jun-Xiang Li, Sen-Bao Lu, Peng Li
{"title":"Crystal structure of diethyl 1,9-bis(4-fluorophenyl)-4,6-diphenylhexahydro-3<i>H</i>-2,7,3,5-(epimethanetriyliminomethanetriyl)cyclopenta [<i>b</i>]pyridine-3,7(2<i>H</i>)-dicarboxylate, C<sub>40</sub>H<sub>36</sub>F<sub>2</sub>N<sub>2</sub>O<sub>4</sub>","authors":"Zi-Ang Zhang, Jun-Xiang Li, Sen-Bao Lu, Peng Li","doi":"10.1515/ncrs-2023-0388","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0388","url":null,"abstract":"Abstract C 40 H 36 F 2 N 2 O 4 , monoclinic, P 2 1 / c (no. 14), a = 9.8180(16) Å, b = 19.355(3) Å, c = 17.930(3) Å, β = 102.353(3)°, V = 3328.3(9) Å 3 , Z = 4, R gt ( F ) = 0.0564, wR ref ( F 2 ) = 0.1866, T = 296(2) K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"28 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136059089","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of (3-hydroxy-4-methoxyphenyl)(pyrrolidin-1-yl)methanone, C12H15NO3 (3-羟基-4-甲氧基苯基)(吡咯烷-1-基)甲烷C12H15NO3的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-10 DOI: 10.1515/ncrs-2023-0376
Xiaona Xu, Hongjuan Tong, Zhoujing Zhu, Bin Liu
{"title":"Crystal structure of (3-hydroxy-4-methoxyphenyl)(pyrrolidin-1-yl)methanone, C<sub>12</sub>H<sub>15</sub>NO<sub>3</sub>","authors":"Xiaona Xu, Hongjuan Tong, Zhoujing Zhu, Bin Liu","doi":"10.1515/ncrs-2023-0376","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0376","url":null,"abstract":"Abstract C 12 H 15 NO 3 , monoclinic, P 2 1 / c (no. 14), a = 6.7230(2) Å, b = 11.1182(3) Å, c = 14.4996(5) Å, β = <m:math xmlns:m=\"http://www.w3.org/1998/Math/MathML\" overflow=\"scroll\"> <m:mrow> <m:mn>94.8870</m:mn> <m:mrow> <m:mrow> <m:mo>(</m:mo> <m:mn>10</m:mn> <m:mo>)</m:mo> </m:mrow> <m:mo>°</m:mo> </m:mrow> </m:mrow> </m:math> $94.8870(10){}^{circ}$ , V = 1079.87(6) Å 3 , Z = 4, R gt ( F ) = 0.0511, wR ref ( <m:math xmlns:m=\"http://www.w3.org/1998/Math/MathML\" overflow=\"scroll\"> <m:mrow> <m:msup> <m:mi>F</m:mi> <m:mn>2</m:mn> </m:msup> </m:mrow> </m:math> ${F}^{2}$ ) = 0.1525, T = 170 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"22 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136293220","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of ethyl 2-((2,6-dichloro-4-(cyanomethyl)phenyl) amino)benzoate, C17H14Cl2N2O2 2-((2,6-二氯-4-(氰乙基)苯基)氨基苯甲酸乙酯C17H14Cl2N2O2的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-10 DOI: 10.1515/ncrs-2023-0341
Meimei Zhao, Mo Du, Bin Liu
{"title":"Crystal structure of ethyl 2-((2,6-dichloro-4-(cyanomethyl)phenyl) amino)benzoate, C<sub>17</sub>H<sub>14</sub>Cl<sub>2</sub>N<sub>2</sub>O<sub>2</sub>","authors":"Meimei Zhao, Mo Du, Bin Liu","doi":"10.1515/ncrs-2023-0341","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0341","url":null,"abstract":"Abstract C 17 H 14 Cl 2 N 2 O 2 , monoclinic, P 2 1 / n (no. 14), a = 8.4863(17) Å, b = 12.654(2) Å, c = 15.088(3) Å, β = 103.612(5)°, V = 1574.8(5) Å 3 , Z = 4, R gt ( F ) = 0.0423, wR ref ( F 2 ) = 0.1472, T = 205 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"36 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136292760","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The crystal structure of (bis(benzimidazol-2-yl-methyl)amine-κ3N,N′,N″ )-(dihydrogen L-malate-κ2O,O ′)copper(II) perchlorate dihydrate, CuC20H24ClN5O12 (双(苯并咪唑-2-酰基甲基)胺-κ 3n,N '，N″)-(l-苹果酸二氢-κ 2o,O ')高氯酸铜(II)二水合物CuC20H24ClN5O12的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-10 DOI: 10.1515/ncrs-2023-0384
Yu Yang, Huanru Liu, Yuhang Wang, Xianggao Meng
{"title":"The crystal structure of (bis(benzimidazol-2-yl-methyl)amine-<i>κ<sup>3</sup>N,N<sup>′</sup>,N<sup>″</sup> </i>)-(dihydrogen L-malate-<i>κ<sup>2</sup>O</i>,<i>O</i> <sup>′</sup>)copper(II) perchlorate dihydrate, CuC<sub>20</sub>H<sub>24</sub>ClN<sub>5</sub>O<sub>12</sub>","authors":"Yu Yang, Huanru Liu, Yuhang Wang, Xianggao Meng","doi":"10.1515/ncrs-2023-0384","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0384","url":null,"abstract":"Abstract CuC 20 H 24 ClN 5 O 12 , monoclinic, P <m:math xmlns:m=\"http://www.w3.org/1998/Math/MathML\" overflow=\"scroll\"> <m:mrow> <m:mover accent=\"true\"> <m:mn>1</m:mn> <m:mo>‾</m:mo> </m:mover> </m:mrow> </m:math> $overline{1}$ (no. 4), a = 7.4467(4) Å, b = 17.3823(9) Å, c = 9.6974(5) Å, α = 90°, β = 103.373(2)°, γ = 90°, V = 1221.20(11) Å 3 , Z = 2, R gt ( F ) = 0.0642, wR ref ( F 2 ) = 0.1757, T = 100(2) K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"2015 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136295187","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The crystal structure of bis(trimethylsulfoxonium) catena-poly[µ2-hexabromido-indium(III)sodium(I)] C6H18O2S2NaInBr6 双(三甲基亚砜)链-聚[2-六溴代-铟(III)钠(I)] C6H18O2S2NaInBr6的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-10 DOI: 10.1515/ncrs-2023-0377
Shifeng Jin, Jiali Lu
{"title":"The crystal structure of bis(trimethylsulfoxonium) <i>catena</i>-poly[µ<sub>2</sub>-hexabromido-indium(III)sodium(I)] C<sub>6</sub>H<sub>18</sub>O<sub>2</sub>S<sub>2</sub>NaInBr<sub>6</sub>","authors":"Shifeng Jin, Jiali Lu","doi":"10.1515/ncrs-2023-0377","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0377","url":null,"abstract":"Abstract C 6 H 18 O 2 S 2 NaInBr 6 , orthorhombic, Pmn 2 1 (no. 31), a = 10.5451(3) Å, b = 7.1169(2) Å, c = 13.7034(4) Å, V = 1028.42(5) Å 3 , Z = 2, R gt ( F ) = 0.0354, wR ref ( F 2 ) = 0.0923, T = 293 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"107 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136292757","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structure of 2-((2-fluoro-4-(trifluoromethyl)phenyl)(hydroxy)methyl)-7-methoxy-3,4-dihydronaphthalen-1((2H))-one, C19H16F4O3 2-((2-氟-4-(三氟甲基)苯基)(羟基)甲基)-7-甲氧基-3,4-二氢萘-1((2H))- 1, C19H16F4O3的晶体结构
4区 化学
Zeitschrift Fur Kristallographie-new Crystal Structures Pub Date : 2023-10-10 DOI: 10.1515/ncrs-2023-0373
Yu-Lun Li, Qing-Guo Meng, Gui-Ge Hou, Zi-Kai Geng
{"title":"Crystal structure of 2-((2-fluoro-4-(trifluoromethyl)phenyl)(hydroxy)methyl)-7-methoxy-3,4-dihydronaphthalen-1((2<i>H</i>))-one, C<sub>19</sub>H<sub>16</sub>F<sub>4</sub>O<sub>3</sub>","authors":"Yu-Lun Li, Qing-Guo Meng, Gui-Ge Hou, Zi-Kai Geng","doi":"10.1515/ncrs-2023-0373","DOIUrl":"https://doi.org/10.1515/ncrs-2023-0373","url":null,"abstract":"Abstract C 19 H 16 F 4 O 3 , monoclinic, P 2 1 / n (no. 14), a = 9.5792(5) Å, b = 9.5542(4) Å, c = 17.6986(9) Å, β = 99.508(5) ∘ , V = 1597.55(14) Å 3 , Z = 4, R gt ( F ) = 0.0481, wR ref ( F 2 ) = 0.1153, T = 293 K.","PeriodicalId":23792,"journal":{"name":"Zeitschrift Fur Kristallographie-new Crystal Structures","volume":"17 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136295188","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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