Vitae-revista De La Facultad De Quimica Farmaceutica最新文献

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Efecto de la inclusión de aceite esencial de orégano (Lippia origanoides) sobre perfil lipídico en carne de pollos de engorde 牛至精油(Lippia origanoides)对肉鸡脂质谱的影响
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-08-31 DOI: 10.17533/UDEA.VITAE.V25N2A03
T. Madrid-Garcés, A. López-Herrera, Jaime Parra-Suescún
{"title":"Efecto de la inclusión de aceite esencial de orégano (Lippia origanoides) sobre perfil lipídico en carne de pollos de engorde","authors":"T. Madrid-Garcés, A. López-Herrera, Jaime Parra-Suescún","doi":"10.17533/UDEA.VITAE.V25N2A03","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N2A03","url":null,"abstract":"Antecedentes: el deterioro del jamon cocido es un proceso complejo que puede manifestarse por alteraciones de tipo microbiologico, fisicoquimico y sensorial, que hasta hoy han sido determinadas por metodologias tradicionales que incluyen largos periodos de seguimiento y un numero importante de muestras. Objetivos: en el presente estudio se propuso un modelo para la prediccion probabilistica del deterioro de jamon cocido, por medio de analisis de componentes principales (ACP) y regresion logistica con aproximacion bayesiana. Metodos: para realizar el analisis, se evaluaron muestras provenientes de 300 lotes independientes de jamon de cerdo cocido, los cuales se conservaron en camaras de almacenamiento a temperaturas de 12±1°C. Se determinaron experimentalmente tres tipos de variables: fisicoquimicas (pH, sineresis, nitritos residuales, porcentaje de acido lactico), de textura (adhesividad, dureza, trabajo de puncion y firmeza instrumental) y microbiologicas (mesofilos aerobios y bacterias acidolacticas) en dos tiempos de medicion: 3 y 40 dias. Para realizar la creacion del modelo se seleccionaron aleatoriamente el 60% de los datos y para la validacion el 40% restante. Los datos obtenidos fueron procesados con el paquete estadistico R Core Team 2012. Resultados: los nitritos residuales y la sineresis fueron las variables mas representativas, ya que su distribucion, correlacion y carga, fueron las mas significativas, con mayor poder discriminante del fenomeno de deterioro en los dos momentos de medicion. El modelo desarrollado permitio correlacionar los parametros estudiados y predecir la probabilidad de deterioro del jamon, ademas de clasificarlo de acuerdo a su estado de calidad. La primera componente principal (CP1) (variables bioquimicas) explico el 73,3 % de la variacion total de los datos, siendo los nitritos residuales y la sineresis los factores mas relacionados con el deterioro. Conclusion: el modelo logistico con aproximacion bayesiana permitio obtener la probabilidad de deterioro del jamon cocido, almacenado a 12°C usando parametros fisicoquimicos. La aplicacion del ACP permitio correlacionar y clasificar los factores de deterioro del producto.","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"87 1 1","pages":"75-82"},"PeriodicalIF":0.0,"publicationDate":"2018-08-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91119739","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Modelo de predicción probabilística de deterioro en jamón de cerdo cocido 熟猪肉火腿变质概率预测模型
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-08-31 DOI: 10.17533/UDEA.VITAE.V25N2A02
Jhoan Sebastián Londoño Parra, Kenneth Roy Cabrera Torres, M. Hurtado
{"title":"Modelo de predicción probabilística de deterioro en jamón de cerdo cocido","authors":"Jhoan Sebastián Londoño Parra, Kenneth Roy Cabrera Torres, M. Hurtado","doi":"10.17533/UDEA.VITAE.V25N2A02","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N2A02","url":null,"abstract":"Antecedentes: el deterioro del jamon cocido es un proceso complejo que puede manifestarse por alteraciones de tipo microbiologico, fisicoquimico y sensorial, que hasta hoy han sido determinadas por metodologias tradicionales que incluyen largos periodos de seguimiento y un numero importante de muestras. Objetivos: en el presente estudio se propuso un modelo para la prediccion probabilistica del deterioro de jamon cocido, por medio de analisis de componentes principales (ACP) y regresion logistica con aproximacion bayesiana. Metodos: para realizar el analisis, se evaluaron muestras provenientes de 300 lotes independientes de jamon de cerdo cocido, los cuales se conservaron en camaras de almacenamiento a temperaturas de 12±1°C. Se determinaron experimentalmente tres tipos de variables: fisicoquimicas (pH, sineresis, nitritos residuales, porcentaje de acido lactico), de textura (adhesividad, dureza, trabajo de puncion y firmeza instrumental) y microbiologicas (mesofilos aerobios y bacterias acidolacticas) en dos tiempos de medicion: 3 y 40 dias. Para realizar la creacion del modelo se seleccionaron aleatoriamente el 60% de los datos y para la validacion el 40% restante. Los datos obtenidos fueron procesados con el paquete estadistico R Core Team 2012. Resultados: los nitritos residuales y la sineresis fueron las variables mas representativas, ya que su distribucion, correlacion y carga, fueron las mas significativas, con mayor poder discriminante del fenomeno de deterioro en los dos momentos de medicion. El modelo desarrollado permitio correlacionar los parametros estudiados y predecir la probabilidad de deterioro del jamon, ademas de clasificarlo de acuerdo a su estado de calidad. La primera componente principal (CP1) (variables bioquimicas) explico el 73,3 % de la variacion total de los datos, siendo los nitritos residuales y la sineresis los factores mas relacionados con el deterioro. Conclusion: el modelo logistico con aproximacion bayesiana permitio obtener la probabilidad de deterioro del jamon cocido, almacenado a 12°C usando parametros fisicoquimicos. La aplicacion del ACP permitio correlacionar y clasificar los factores de deterioro del producto.","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"35 1","pages":"64-74"},"PeriodicalIF":0.0,"publicationDate":"2018-08-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77234408","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Inhibition of quorum sensing by compounds from two Eunicea species and synthetic saturated alkylglycerols 两种桉树属植物化合物及合成饱和烷基甘油对群体感应的抑制作用
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-08-31 DOI: 10.17533/UDEA.VITAE.V25N2A05
A. Barragán, G. Silva, M. Moreno, W. Mayorga
{"title":"Inhibition of quorum sensing by compounds from two Eunicea species and synthetic saturated alkylglycerols","authors":"A. Barragán, G. Silva, M. Moreno, W. Mayorga","doi":"10.17533/UDEA.VITAE.V25N2A05","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N2A05","url":null,"abstract":"Background: the emergence of bacterial resistance has led to a search for new natural products as alternatives starting points to prevent and control diseases caused by microorganisms. Among the potential candidates were bioactive compounds from octocorals of the genus Eunicea due to their chemical structures and their wide range of biological activities. Objective: the purpose of this study was to evaluate the quorum sensing inhibition (QSI) and antibacterial activity of compounds previously isolated from two Eunicea species and synthesized alkylglycerols (AKG). Methods: the QSI of three nonpolar compounds and a mixture of AKGs from Eunicea were evaluated by a microtiter plate assay using Chromobacterium violaceum (ATCC 31532). Four naturally occurring, saturated, and enantiomerically pure AKGs, all of which were derived from the chiral precursor (R)-solketal, were synthesized from alkyl chains of 12, 14, 16 and 18 carbons, and their structures were spectroscopically verified by NMR, ESI-MS and optical rotation data. Their QSI by the disc diffusion assay and minimum inhibitory concentrations (MIC) against 14 clinical bacterial isolates in microtiter plates were determined. Results: cembradiene 1, the AKG mixture and AKG (2S)-3-O-dodecyl-1,2-propanediol 4 inhibit QS at the same concentration as kojic acid (10 µg/well or 20 µg/disc, respectively). In this study, the bioactive compounds 1, stearyl oleate 2, acylglycerol 3 and AKGs 4 and (2S)-3-O-tetradecyl-1,2-propanediol 5 showed in vitro IQS activity for the first time. Additionally, 4 and 5 displayed in vitro antibacterial activity against Listeria innocua and Staphylococcus aureus (MIC = 32 µg/mL for both 4 and 5), Enterococcus faecalis (128 µg/mL and 64 µg/mL respectively), Micrococcus luteus (128 µg/mL for both) and Brevibacillus brevis (Bacillus brevis) (512 µg/mL and 64 µg/mL respectively). Conclusion: results suggest that natural compounds 1, 2, 3, 4 and 5 showed QSI, also 4 and 5 have antibacterial activity and they are an interesting alternative to continue researching their effect against pathogenic microorganisms.","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"8 1","pages":"92-103"},"PeriodicalIF":0.0,"publicationDate":"2018-08-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"89136541","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Microencapsulation: A technological alternative to preserve active ingredients in functional foods 微胶囊化:一种保存功能性食品中有效成分的替代技术
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-08-31 DOI: 10.17533/UDEA.VITAE.V25N2A01
J. Escobar, Diana Margarita Márquez Fernández
{"title":"Microencapsulation: A technological alternative to preserve active ingredients in functional foods","authors":"J. Escobar, Diana Margarita Márquez Fernández","doi":"10.17533/UDEA.VITAE.V25N2A01","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N2A01","url":null,"abstract":"In the late 80’s started the rise of researches related to the obtainment of food capable of supplying the energetic demand, promoting growth and encompassing better properties and benefits for the human being (1-4). Due to their nutritional and pharmacological features, these foods were called nutraceutical or functional foods as they comprise one or more components, not necessarily nutrients, that promote health, prevent diseases and strengthen the immune system or exhibit medical properties (1, 2). Regardless such researches increase and despite the approval for use and commercialization of these foods, in most countries there is neither a statutory definition nor any specific legislation that governs them (3, 4).","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"24 1","pages":"62-63"},"PeriodicalIF":0.0,"publicationDate":"2018-08-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84367414","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Actividad antioxidante del complejo de inclusión del extracto de semilla de Bixa orellana en β-ciclodextrina obtenido por CO2 supercrítico 超临界CO2法制备的β-环糊精中Bixa orellana种子提取物包合物的抗氧化活性
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-08-31 DOI: 10.17533/UDEA.VITAE.V25N2A04
Erika V. Meñaca, J. Restrepo, Ana J Colmenares
{"title":"Actividad antioxidante del complejo de inclusión del extracto de semilla de Bixa orellana en β-ciclodextrina obtenido por CO2 supercrítico","authors":"Erika V. Meñaca, J. Restrepo, Ana J Colmenares","doi":"10.17533/UDEA.VITAE.V25N2A04","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N2A04","url":null,"abstract":"Antecedentes: los extractos de Bixa orellana son utilizados como colorante de alimentos, y presentan una actividad antioxidante de importancia farmaceutica. Su uso puede limitarse por su inestabilidad, donde el proceso de inclusion en β-ciclodextrina (β-CD) por fluido supercritico con CO2 (FSC-CO2) es una alternativa para mediar esta desventaja. Objetivos: comparar diferentes condiciones de temperatura y presion de extraccion por FSC-CO2, para determinar cual de estas permite obtener un extracto de Bixa orellana con mayor actividad antioxidante, y evaluar el efecto de la inclusion en β-CD, en dicha capacidad antioxidante. Metodos: se obtuvieron extractos por FSC-CO2 variando condiciones de presion y temperatura: (I) 3583 psi, 35°C, (II) 1413 psi, 35°C, (III) 2184 psi, 45°C, (IV) 5076 psi, 45°C, y (V) 2300 psi, 40°C. Se evaluo la actividad antioxidante de los extractos obtenidos mediante el metodo DPPH, determinando su IC50. Se realizo el complejo de inclusion en β-CD del extracto que presento la mayor actividad antioxidante, por el metodo FSC-CO2, y fue caracterizado por IR, DSC y RMN. Mediante analisis comparativo de los espectros de la β-CD, extracto libre y el complejo extracto/β-CD, se verifico el acomplejamiento, y se evaluo la capacidad antioxidante del complejo de inclusion. Resultados: el extracto con mayor actividad antioxidante se obtuvo bajo la condicion de extraccion IV, con un IC50 de 23,55 μg/mL, seguido del extracto II (28,76 μg/mL), del extracto III (37,23 μg/mL), del extracto V (81,09 μg/mL) y del extracto I (193,82 μg/mL), los cuales presentaron diferencias significativas (P<0,01). Los espectros obtenidos por IR, DSC y RMN presentaron desplazamientos propios del proceso de encapsulamiento. El valor IC50 del complejo extracto/β-CD fue de 104,84 μg/mL, siendo significativamente mayor al valor obtenido para el extracto puro (23,55 µg/mL). Conclusion: el extracto de Bixa orellana con una actividad antioxidante mayor se obtuvo por fluido supercritico a 5076 psi de presion y 45°C de temperatura. Las variaciones de los espectros IR, DSC y RMN demuestran la inclusion del extracto en la β-CD, y los valores de IC50 indican el efecto protector de la β-CD ante la reaccion con el radical DPPH.","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"29 1","pages":"83-91"},"PeriodicalIF":0.0,"publicationDate":"2018-08-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73383361","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Osmotic dehydration of green mango samples (Mangifera indica L., Filipino var.) in ternary solutions 绿芒果样品(Mangifera indica L., philippine var.)在三元溶液中的渗透脱水
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-06-03 DOI: 10.17533/UDEA.VITAE.V25N1A02
A. Ayala-Aponte, Andrea Molina-Cortés, L. Serna-Cock
{"title":"Osmotic dehydration of green mango samples (Mangifera indica L., Filipino var.) in ternary solutions","authors":"A. Ayala-Aponte, Andrea Molina-Cortés, L. Serna-Cock","doi":"10.17533/UDEA.VITAE.V25N1A02","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N1A02","url":null,"abstract":"Background: in Colombia the consumption of fresh green mango (also known as mango “biche”) is quite popular, and is consumed with lemon juice, salt, and honey. However, its high humidity content and high water activity makes of mango a highly perishable fruit, thus requiring processing alternatives. Osmotic dehydration (OD) is an interesting alternative for the conservation of mango. In OD, binary solutions (Solute + water) and ternary solutions (2 Solutes + water), have been traditionally used, however, more water removal can be achieved using ternary solutions, which leads to the improved organoleptic properties of dehydrated products. Objetives: to evaluate the kinetic water loss (WL), solutes gain (SG), weight reduction (WR), water activity (aw), and volume (Shrinking Coefficient, SC) in green mango (Mangifera indica L. Filipino variety) osmotically dehydrated (OD). Additionally, to calculate water and solutes diffusivity (Def ) for each treatment. Methods: green mango samples, with maturity scale zero, were used. Ternary solutions of sucrose at 40% and NaCl at 3, 6 and 9% were used for OD. The binary solution of sucrose with water as control treatment, was used. In the osmotic process samples were taken out at different times of OD (15, 30, 60, 90, 180, 240, and 300 min). Results: the findings show that at a higher concentration of NaCl, the dehydration kinetics was more rapid, aw and SC were smaller and water and solutes Def were higher. The samples dehydrated with the greatest solutes concentration (40-9%) reached the highest WL, SG, and WR with 89.52, 13.10, and 46.68%, respectively. Coefficients Defw and Defs showed a magnitude order of 10-10 m2/s, which is within the interval of dehydrated foods. Conclusions: this research showed that binary (sucrose + water) and ternary (NaCl + sucrose + water) solutions, are suitable for dehydrating green mango, however, the ternary solutions were more effective.","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"53 1","pages":"8-16"},"PeriodicalIF":0.0,"publicationDate":"2018-06-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85403120","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Kinetic modeling of the enzymatic hydrolysis of proteins of visceras from red tilapia (Oreochromis sp.): effect of substrate and enzyme concentration 红罗非鱼(Oreochromis sp.)内脏蛋白酶解动力学模型:底物和酶浓度的影响
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-06-03 DOI: 10.17533/UDEA.VITAE.V25N1A03
J. E. Zapata-Montoya, Diego Enrique Giraldo-Rios, Andrea Johana Baéz-Suarez
{"title":"Kinetic modeling of the enzymatic hydrolysis of proteins of visceras from red tilapia (Oreochromis sp.): effect of substrate and enzyme concentration","authors":"J. E. Zapata-Montoya, Diego Enrique Giraldo-Rios, Andrea Johana Baéz-Suarez","doi":"10.17533/UDEA.VITAE.V25N1A03","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N1A03","url":null,"abstract":"Background:  The Growth of world Aquaculture has generated important environmental impacts as discard residues that are important sources of protein which have been used to manufacture low-value products, such as animal food, fish flour and fertilizers. Objectives: To evaluate the effect of enzyme and substrate concentration on the degree of hydrolysis (DH) of proteins in the red tilapia ( Oreochromis sp .) viscera (RTV). Methods: The commercial Alcalase 2.4 L enzyme was used at different concentrations to hydrolyse the proteins in RTV at 53.5 °C and a pH of 9.5 in a 1 L magnetically stirred, jacketed, glass batch reactor connected to an automatic titrator. Each experiment was conducted over 6 h in which every consumed volume of base was recorded every 5 min to determine the corresponding DH at each point. Results: The results indicated that increasing the enzyme concentration produced an increase in the DH and in the reaction rate, while increasing the substrate concentration produced a decrease in both parameters. For this reason, a mathematical model was adjusted for the inhibition of substrate from the exponential kinetic Equation d(DH)/dt = a*EXP[-b*(DH)] to explain the behavior of the DH as a function of substrate concentration in this hydrolytic process. The parameters a and b were estimated from a nonlinear regression. Based on these results, the reaction constants were determined as K s =456.75 g L -1 , K 2 =1.2191 min -1 , K d =0.2224 min -1 , K M =1.8963and K 3 = 0.1173 L g -1 min -1 , which allowed the generation of a strong correlation between the predicted and experimental values at the different evaluated operating conditions. This correlation was supported by a low average relative error (ARE) of 3.26%. Conclusion: Under evaluated experimental conditions, the kinetics of the hydrolysis reaction followed a substrate inhibition mechanism, which was adjusted through a typical exponential Equation that involves two parameters (a and b) associated with the kinetic constants (Ks, K 2 , and K d ).","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"5 1","pages":"17-25"},"PeriodicalIF":0.0,"publicationDate":"2018-06-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81606091","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
Influence of spray drying process on the quality of avocado powder: a functional food with great industrial potential 喷雾干燥工艺对牛油果粉品质的影响——牛油果粉是一种极具工业潜力的功能性食品
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-06-03 DOI: 10.17533/UDEA.VITAE.V25N1A05
Alejandra Marulanda, M. Ruiz-Ruiz, M. Cortés-Rodríguez
{"title":"Influence of spray drying process on the quality of avocado powder: a functional food with great industrial potential","authors":"Alejandra Marulanda, M. Ruiz-Ruiz, M. Cortés-Rodríguez","doi":"10.17533/UDEA.VITAE.V25N1A05","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N1A05","url":null,"abstract":"ABSTRACT BACKGROUND: Colombia is the fifth largest producer of avocado and its agribusiness chain lacks value-added diversified products. Therefore, at the governmental level, there has been promotion of internationalization policies aimed at opening up new markets and innovation with improved technology and food consumption patterns, while spray drying is an alternative conservation for avocado, a highly perishable fruit. OBJECTIVES: the aim of this study was to optimize the spray drying process for obtaining Hass avocado powder with better physicochemical properties and processing. METHODS: an experimental design \"Optimal\" was used in the response surface methodology based on four factors: (A) maltodextrin (MD) concentration (2.81 to 11.25% w/w), (B) air inlet temperature (140-160 °C), (C) outlet air temperature (80-90 °C) and (D) atomizer disk speed (20000-26000 rpm). RESULTS: The response variables where statistically significant differences (p <0.05) were found including: moisture, water activity, solubility, color coordinates (L*, a*, b*) hygroscopicity, wettability, extractable oil and deposit formation versus factors studied. Optimized value factors were: (A) 6.93% (B) 160 °C (C) 84 °C and (D) 26000 rpm. CONCLUSIONS: The experimental process optimization is presented as an effective tool for agribusiness, which improves product quality in terms of the factors that affect it, and in the case of avocado, allows the development of new value-added products, with potential uses in the food industry, pharmaceutical, cosmeceutical, among others .","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"26 1","pages":"37-48"},"PeriodicalIF":0.0,"publicationDate":"2018-06-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91264651","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 11
PHYSICOCHEMICAL COMPARISON OF COMMERCIAL VS. EXTRACTED β-GLUCANS AND STRUCTURAL CHARACTERIZATION AFTER ENZYMATIC PURIFICATION 商品β-葡聚糖与萃取β-葡聚糖的理化比较及酶纯化后的结构表征
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-06-03 DOI: 10.17533/UDEA.VITAE.V25N1A04
S. M. V. Mejía, A. D. Francisco, P. Barreto, B. Mattioni, A. W. Zibetti, L. Molognoni, H. Daguer
{"title":"PHYSICOCHEMICAL COMPARISON OF COMMERCIAL VS. EXTRACTED β-GLUCANS AND STRUCTURAL CHARACTERIZATION AFTER ENZYMATIC PURIFICATION","authors":"S. M. V. Mejía, A. D. Francisco, P. Barreto, B. Mattioni, A. W. Zibetti, L. Molognoni, H. Daguer","doi":"10.17533/UDEA.VITAE.V25N1A04","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N1A04","url":null,"abstract":"Background: β-glucans (1-3: 1-4) are soluble fibers applied to foods due to their technological properties (water binding capacity, viscosity, emulsification and stabilization) and their beneficial effects on health. The functional properties of β-glucans can be lost during the extraction and purification processes. The high viscosity of β-glucans is related to a high molecular weight and its physiological properties in the intestine. Therefore, to characterize the fiber after its extraction and purification is fundamental to understand its possible applications in foods. Objectives: characterize β-glucans extracted (EβG) and compare them with three commercial β-glucans (CβG-A, CβG-B and CβG-C) to identify its possible applications in foods and to evaluate if enzymatic purification affects molecular and structurally the β-glucans. Methods: barley β-glucans were extracted (EβG), characterized by chemical analyzes, rheological behavior, and color, and compared to three commercial β-glucans samples. Then, the extract was purified and its structural and molecular characteristics were calculated. Results: EβG contained 64.38 ± 3.54% of β-glucans, high starch contamination (12.70 ± 1.73%), high content of calcium (8894 mg/kg), pseudoplastic behavior, and dark color (L* = 52.77 ± 0.7). All commercial samples showed low starch contamination, lighter color, and Newtonian behavior. After purification starch and protein contamination decreased (0.85 ± 0.46% and 5.50 ± 0.12% respectively), increased the content of βG (69.45 ± 0.81%) and increased brightness (L* = 92.60 ± 1.70). Purified β-glucans (PβG) showed a molar weight of 690 ± 1.6 kDa and species with degree polymerization 3 (DP3) to 11 (DP11) were identified on the structure. Conclusions: EβG extracts before the purification presented a high viscosity and contamination. The enzymatic purification process was effective and allowed to maintain a high molar mass of PβG and its distinctive molecular structures (species with DP3 and DP4). The commercial samples CβG-A and CβG-B showed a low content of β-glucans. Finally, CβG-C presented the best physicochemical and rheological properties for its subsequent application in food.","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"42 1","pages":"26-36"},"PeriodicalIF":0.0,"publicationDate":"2018-06-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80111927","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
PROTEINS FUNCTIONALIZATION: A STRATEGY THAT BOOST THE PERFORMANCE OF THESE MACROMOLECULES FOR INNOVATIVE PHARMACEUTICAL AND FOOD DEVELOPMENTS 蛋白质功能化:一种提高这些大分子性能的策略,用于创新制药和食品开发
Vitae-revista De La Facultad De Quimica Farmaceutica Pub Date : 2018-06-03 DOI: 10.17533/UDEA.VITAE.V25N1A01
J. Q. Quiroz, Jhon Jairo Rojas Camargo
{"title":"PROTEINS FUNCTIONALIZATION: A STRATEGY THAT BOOST THE PERFORMANCE OF THESE MACROMOLECULES FOR INNOVATIVE PHARMACEUTICAL AND FOOD DEVELOPMENTS","authors":"J. Q. Quiroz, Jhon Jairo Rojas Camargo","doi":"10.17533/UDEA.VITAE.V25N1A01","DOIUrl":"https://doi.org/10.17533/UDEA.VITAE.V25N1A01","url":null,"abstract":"Proteins are macromolecules exhibiting amphiphilic properties, good biocompatibility, biodegradability, high nutritional value, and show strong interactions with several types of active compounds via hydrogen bonding and electrostatic interactions. These plant or animal-derived macromolecules differ in their molecular size depending on the number of amino acids present in their structure, which in turn, are linked by peptide bonds between the carbonyl (-CO-) and amino groups (-NH).","PeriodicalId":23515,"journal":{"name":"Vitae-revista De La Facultad De Quimica Farmaceutica","volume":"77 1","pages":"6-7"},"PeriodicalIF":0.0,"publicationDate":"2018-06-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73549992","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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