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Enhanced Productivity of Paclitaxel and Related Taxanes in Plant Cell Culture Including Aliphatic Ionic Liquids 包括脂肪族离子液体在内的植物细胞培养中紫杉醇和相关紫杉醇类化合物的产量提高
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2018-01-01 DOI: 10.15261/SERDJ.25.125
Shinjiro Yamamoto, Y. Sonoda, T. Kataoka, S. Hayashi, H. Miyasaka
{"title":"Enhanced Productivity of Paclitaxel and Related Taxanes in Plant Cell Culture Including Aliphatic Ionic Liquids","authors":"Shinjiro Yamamoto, Y. Sonoda, T. Kataoka, S. Hayashi, H. Miyasaka","doi":"10.15261/SERDJ.25.125","DOIUrl":"https://doi.org/10.15261/SERDJ.25.125","url":null,"abstract":"We report here on hydrophobic ionic liquids (ILs) which enhance the productivity of paclitaxel and the related taxanes of 10-deacetyl baccatin III, baccatin III and cepharomannine with in situ extraction from an aqueous medium in the suspension cell culture of Taxus cuspidata in the IL-medium two phase culture system. Two aliphatic ILs of N-methyl-n-propylpiperidinium bis(trifluoromethane-sulfonyl)imide (PP13-TFSI) and N-methyl-n-butylpyrrolidinium bis(trifluoromethanesulfonyl)imide (P14-TFSI) were used. It was found that the two ILs had no cytotoxicity and enhanced productivity of paclitaxel and the related taxanes in the cell culture. In particular, the more hydrophobic P14-TFSI, which enhanced the productivity of paclitaxel and the total taxanes by a factor of more than 2 compared to PP13-TFSI, could be an effective extractant.","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2018-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79408521","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
A Comprehensive Extraction Study Using a Mono-alkylated Diglycolamic Acid Extractant: Comparison Between a Secondary Amide Group and a Tertiary Amide Group 单烷基化二乙醇酸萃取剂的综合萃取研究:仲酰胺基与叔酰胺基的比较
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.61
T. Sugita, Iori Fujiwara, H. Okamura, T. Oshima, Y. Baba, H. Naganawa, K. Shimojo
{"title":"A Comprehensive Extraction Study Using a Mono-alkylated Diglycolamic Acid Extractant: Comparison Between a Secondary Amide Group and a Tertiary Amide Group","authors":"T. Sugita, Iori Fujiwara, H. Okamura, T. Oshima, Y. Baba, H. Naganawa, K. Shimojo","doi":"10.15261/SERDJ.24.61","DOIUrl":"https://doi.org/10.15261/SERDJ.24.61","url":null,"abstract":"Tsuyoshi SUGITA1, Iori FUJIWARA1,2, Hiroyuki OKAMURA1, Tatsuya OSHIMA2, Yoshinari BABA2, Hirochika NAGANAWA1 and Kojiro SHIMOJO1,* 1Advance Science Research Center, Japan Atomic Energy Agency (JAEA), 2-4 Shirakata, Tokai-mura, Ibaraki 319-1195, Japan; 2Department of Applied Chemistry, University of Miyazaki, 1-1 Gakuen Kibanadai Nishi, Miyazaki 889-2192, Japan (Received December 28, 2016; Accepted March 3, 2017)","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74311588","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Modeling of Equilibria for the Solvent Extraction of Ammonia with LIX84I 用LIX84I萃取氨的平衡模型
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.71
Shubin Wang, Jie Li, H. Narita, Mikiya Tanaka
{"title":"Modeling of Equilibria for the Solvent Extraction of Ammonia with LIX84I","authors":"Shubin Wang, Jie Li, H. Narita, Mikiya Tanaka","doi":"10.15261/SERDJ.24.71","DOIUrl":"https://doi.org/10.15261/SERDJ.24.71","url":null,"abstract":"Solvent extraction of valuable metals such as copper and nickel is often carried out from ammoniacal alkaline solutions with chelating extractants, during which coextraction of ammonia is inevitable. In the present study, as a basis of modeling of the whole ammoniacal extraction process, the equilibrium distribution ratios of ammonia between a 3 mol L-1 ammonium nitrate solution and LIX84I (the active component of which is 2-hydroxy-5-nonylacetophenone oxime, HR) dissolved in a nonpolar diluent were measured as a function of pH and LIX84I concentration at 298 K. We successfully modeled the measurement results by assuming the formation of two associated species, (HR)n・(NH3) and (HR・NH3)n, the aggregation of HR, and the dissociation of NH4. Fourier transform infrared spectroscopy results suggested that ammonia was extracted via hydrogen bonding with HR, and these results were in accord with the proposed equilibrium model.","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86733962","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Enhanced Extraction of Tris(pentane-2,4-dionato)cobalt(III) in Supercritical Carbon Dioxide/Water Systems by Association with Fluorinated Phenols 超临界二氧化碳/水体系中氟化苯酚对三(戊烷-2,4-迪奥纳托)钴(III)的强化萃取
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.1
Ohashi Akira, Shiratori Kiyohiro, Kim Haeng‐Boo
{"title":"Enhanced Extraction of Tris(pentane-2,4-dionato)cobalt(III) in Supercritical Carbon Dioxide/Water Systems by Association with Fluorinated Phenols","authors":"Ohashi Akira, Shiratori Kiyohiro, Kim Haeng‐Boo","doi":"10.15261/SERDJ.24.1","DOIUrl":"https://doi.org/10.15261/SERDJ.24.1","url":null,"abstract":"","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88866666","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Ultrasound-assisted Extraction of Fe(III) from Wet-process Phosphoric Acid 超声波辅助提取湿法磷酸中铁(III)的研究
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.11
Li Xingbin, Liu Daijun, Ji Junyi, C. Jianjun, Yang Tao
{"title":"Ultrasound-assisted Extraction of Fe(III) from Wet-process Phosphoric Acid","authors":"Li Xingbin, Liu Daijun, Ji Junyi, C. Jianjun, Yang Tao","doi":"10.15261/SERDJ.24.11","DOIUrl":"https://doi.org/10.15261/SERDJ.24.11","url":null,"abstract":"An ultrasound-assisted extraction (UAE) method was developed for the extraction of Fe (III) from wet-process phosphoric acid with di (2-ethylhexyl) phosphoric acid (D2EHPA). The influences of UAE parameters, including ultrasonic power, extraction time, concentration of D2EHPA and extraction temperature, were systematically studied. The response surface methodology, a statistical technique, was used to obtain the optimal conditions and evaluate the significance of variables affecting the extraction efficiency of the UAE. It was found that ultrasound could markedly improve the extraction rate of Fe (III) with D2EHPA, the largest improvement is up to 7 times compared with the traditional solvent extraction method. However, the extraction equilibrium of the extraction system was not affected by ultrasound. It is believed that the cavitation effect of ultrasound, along with the increased interfacial surface area, contribute to the enhancement of the extraction rate.","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81868463","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Purification of Wet Process Phosphoric Acid by Solvent Extraction using Cyclohexanol 环己醇溶剂萃取法纯化湿法磷酸
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.23
Xing Li, Jun Li, Jianhong Luo, Yang Jin, Da-Jiang Zou
{"title":"Purification of Wet Process Phosphoric Acid by Solvent Extraction using Cyclohexanol","authors":"Xing Li, Jun Li, Jianhong Luo, Yang Jin, Da-Jiang Zou","doi":"10.15261/SERDJ.24.23","DOIUrl":"https://doi.org/10.15261/SERDJ.24.23","url":null,"abstract":"","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86701340","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 21
Extraction and Separation of Pt and Pd by an Imidazolium-Based Ionic Liquid Combined with Phosphonium Chloride 咪唑基离子液体与氯化磷复合萃取分离Pt和Pd
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.97
Fukiko Kubota, Eiko Shigyo, Wataru Yoshida, M. Goto
{"title":"Extraction and Separation of Pt and Pd by an Imidazolium-Based Ionic Liquid Combined with Phosphonium Chloride","authors":"Fukiko Kubota, Eiko Shigyo, Wataru Yoshida, M. Goto","doi":"10.15261/SERDJ.24.97","DOIUrl":"https://doi.org/10.15261/SERDJ.24.97","url":null,"abstract":"","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"72713046","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 17
Salting-out Extraction of 3-Hydroxypropionic Acid with Reactive Extraction and Aqueous Two-phase Systems 反应萃取-双水相体系盐析萃取3-羟基丙酸
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.141
M. Matsumoto, M. Shibazaki, Ryohei Yuasa, Kazuo Kondo
{"title":"Salting-out Extraction of 3-Hydroxypropionic Acid with Reactive Extraction and Aqueous Two-phase Systems","authors":"M. Matsumoto, M. Shibazaki, Ryohei Yuasa, Kazuo Kondo","doi":"10.15261/SERDJ.24.141","DOIUrl":"https://doi.org/10.15261/SERDJ.24.141","url":null,"abstract":"3-Hydroxypropionic acid (3-HP) is an isomer of 2-hydroxypropionic acid (2-HP) and an important platform molecule. A biological production route of 3-HP has become of interest as a sustainable alternative to the chemical route. However, its hydrophilic property makes the separation of 3-HP from the fermentation broth difficult. In this study, reactive solvent extraction and an aqueous two phase system (ATPS) were utilized to extract 3-HP from an aqueous solution. In the reactive extraction system, synergism, which was found in the reactive extraction of 2-HP, was not observed with mixed extractants of TBP and TOA diluted in heptane. TOA diluted in 1-octanol gave the highest extractability in the reactive extraction system. There was little effect on the extractability of 3-HP by the addition of salt to the system. In an ATPS composed of alcohols and salts, binodal curves and tie lines were measured, and then 3-HP was extracted with the ATPS. The highest extractability and distribution ratio were obtained by using an ATPS composed of t-BuOH and Na2SO4. The maximum distribution ratios in both systems were similar.","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"73124407","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Structural Evaluation of the Aggregate of Palladium(II)-Pyridylazophenol Complex at the Heptane-Water Interface by the Centrifugal Liquid Membrane Method 用离心液膜法评价钯(II)-吡啶偶氮酚配合物在庚烷-水界面上的聚集体结构
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.105
A. Ohashi, Takafusa Kiminarita, H. Watarai
{"title":"Structural Evaluation of the Aggregate of Palladium(II)-Pyridylazophenol Complex at the Heptane-Water Interface by the Centrifugal Liquid Membrane Method","authors":"A. Ohashi, Takafusa Kiminarita, H. Watarai","doi":"10.15261/SERDJ.24.105","DOIUrl":"https://doi.org/10.15261/SERDJ.24.105","url":null,"abstract":"2, 2017) The formation and aggregation of the Pd(II) complex with 2-(5-bromo-2-pyridylazo)-5-diethylaminophenol (HL) at the heptane-water interface was investigated by UV-vis absorption and resonance Raman spectrometry using the centrifugal liquid membrane (CLM) method. The interfacial aggregate had an absorption maximum wavelength at 488 nm, showing a hypsochromic shift from the absorption maximum wavelength at 580 nm of the complex monomer (PdLCl). The critical aggregation concentration of PdLCl was determined to be 2.6  10 -10 mol cm -2 . The observed UV-vis absorption and resonance Raman spectra implied that the ligand in the interfacial aggregate was mainly in the state of azo form, because the spectra were very similar to those of the PdLCl complex obtained in a low-polarity solvent","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87137903","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Selective Extraction of Indium(III) and Gallium(III) with 2-Ethylhexyl Thioglycolate 2-乙基己基巯基乙酸盐选择性萃取铟(III)和镓(III
IF 0.7 4区 工程技术
Solvent Extraction Research and Development, Japan Pub Date : 2017-01-01 DOI: 10.15261/SERDJ.24.123
Rieko Miura, Megumi Tokumaru, T. Oshima, Y. Baba
{"title":"Selective Extraction of Indium(III) and Gallium(III) with 2-Ethylhexyl Thioglycolate","authors":"Rieko Miura, Megumi Tokumaru, T. Oshima, Y. Baba","doi":"10.15261/SERDJ.24.123","DOIUrl":"https://doi.org/10.15261/SERDJ.24.123","url":null,"abstract":"Extraction selectivity of In (III) and Ga (III) was investigated using 2-ethylhexyl thioglycolate (EHTG) with a thiol group and an oxygen atom to recover these metals from zinc refinery residue and waste solar panels. The extraction order with EHTG was Cu(II)>In(III)>Ga(III)>Zn(II), while Al (III) was hardly extracted at all. While In(III) and Ga(III) were not extracted at all with 1-dodecanethiol (DDT) with contains only a thiol group although Zn (II) and Cu (II) were extracted. This indicates that the oxygen atom in the EHTG ester plays an important role in the extraction of these metals. The mutual separation of In(III), Ga(III), Zn(II) and Cu(II) is possible in almost one step with EHTG. The extraction equilibria of In(III) and Ga(III) with EHTG are also discussed. Furthermore, the stripping of In(III) and Ga(III) extracted into the organic phase was achieved using appropriate concentrations of NaOH and acids.","PeriodicalId":21805,"journal":{"name":"Solvent Extraction Research and Development, Japan","volume":null,"pages":null},"PeriodicalIF":0.7,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86014393","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
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