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Chromatographic separation to determine doxycycline monohydrate and ornidazole 用色谱分离法测定一水多西环素和奥硝唑
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-07-04 DOI: 10.1002/sscp.202300061
Bhoomi Patel, S. Patel
{"title":"Chromatographic separation to determine doxycycline monohydrate and ornidazole","authors":"Bhoomi Patel, S. Patel","doi":"10.1002/sscp.202300061","DOIUrl":"https://doi.org/10.1002/sscp.202300061","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-07-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47204648","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Reversed phase‐high‐performance liquid chromatography simultaneous estimation of phenolic compounds in hydroalcoholic extract of Potentilla fulgens root 反相高效液相色谱法同时测定白草根水醇提取物中酚类化合物的含量
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-07-02 DOI: 10.1002/sscp.202300048
S. Chaudhary, K. C. Sharma, I. Sarangthem, A. Kar, P. Bhardwaj, Nanaocha Sharma, P. Mukherjee
{"title":"Reversed phase‐high‐performance liquid chromatography simultaneous estimation of phenolic compounds in hydroalcoholic extract of Potentilla fulgens root","authors":"S. Chaudhary, K. C. Sharma, I. Sarangthem, A. Kar, P. Bhardwaj, Nanaocha Sharma, P. Mukherjee","doi":"10.1002/sscp.202300048","DOIUrl":"https://doi.org/10.1002/sscp.202300048","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-07-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47811822","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Determination of Valbenazine related substances by liquid chromatography method complying with the current regulatory guidelines. Method robustness evaluation by Design of Experiments software 液相色谱法测定丙苯嗪相关物质符合现行法规。方法采用实验软件设计进行稳健性评价
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-06-27 DOI: 10.1002/sscp.202300010
B. R. Deshmukh, Parameswari Akshinthala, N. Katari, Girish K Deshpande, Leela Prasad Kowtharapu, Sreenivasa Rao Battula, R. Gundla
{"title":"Determination of Valbenazine related substances by liquid chromatography method complying with the current regulatory guidelines. Method robustness evaluation by Design of Experiments software","authors":"B. R. Deshmukh, Parameswari Akshinthala, N. Katari, Girish K Deshpande, Leela Prasad Kowtharapu, Sreenivasa Rao Battula, R. Gundla","doi":"10.1002/sscp.202300010","DOIUrl":"https://doi.org/10.1002/sscp.202300010","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44251338","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Enantiomeric separation of ketoprofen using Frovatriptan as a chiral derivatizing reagent 佛罗替坦作为手性衍生试剂分离酮洛芬对映体
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-06-25 DOI: 10.1002/sscp.202300087
V. K. Vashistha, R. Bala, R. V. Pullabhotla, A. Mittal
{"title":"Enantiomeric separation of ketoprofen using Frovatriptan as a chiral derivatizing reagent","authors":"V. K. Vashistha, R. Bala, R. V. Pullabhotla, A. Mittal","doi":"10.1002/sscp.202300087","DOIUrl":"https://doi.org/10.1002/sscp.202300087","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-06-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47180766","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Polypyrrole‐coated rubber foam sorbent for extraction of fipronil and fipronil sulfone in tea 聚吡咯涂层橡胶泡沫吸附剂提取茶叶中的氟虫腈和氟虫腈砜
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-06-23 DOI: 10.1002/sscp.202300005
Sonam Choden, Deki Deki, Suwatchanee Maneeratanachot, N. Lehman, E. Kalkornsurapranee, M. Kaewpet, Dhassida Sooksawat, Itthipon Jeerapan, Apon Numnuam, P. Kanatharana, P. Thavarungkul, Chongdee Thammakhet-Buranachai
{"title":"Polypyrrole‐coated rubber foam sorbent for extraction of fipronil and fipronil sulfone in tea","authors":"Sonam Choden, Deki Deki, Suwatchanee Maneeratanachot, N. Lehman, E. Kalkornsurapranee, M. Kaewpet, Dhassida Sooksawat, Itthipon Jeerapan, Apon Numnuam, P. Kanatharana, P. Thavarungkul, Chongdee Thammakhet-Buranachai","doi":"10.1002/sscp.202300005","DOIUrl":"https://doi.org/10.1002/sscp.202300005","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-06-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"42629276","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A liquid chromatography‐tandem mass spectrometry method for the analysis of sucralose and five glycoside sweeteners 三氯蔗糖和五种糖苷类甜味剂的液相色谱串联质谱分析方法
SEPARATION SCIENCE PLUS Pub Date : 2023-06-21 DOI: 10.1002/sscp.202300068
Serban C. Moldoveanu
{"title":"A liquid chromatography‐tandem mass spectrometry method for the analysis of sucralose and five glycoside sweeteners","authors":"Serban C. Moldoveanu","doi":"10.1002/sscp.202300068","DOIUrl":"https://doi.org/10.1002/sscp.202300068","url":null,"abstract":"Abstract The present study describes sensitive liquid chromatography‐tandem mass spectrometry methods for the analysis of sucralose, mogroside V, neohesperidin dihydrochalcone, rebaudioside A, stevioside, and glycyrrhizic acid. All these compounds are used as sugar substitutes in food, beverages, and dietary supplements, and can be present in environmental and biological samples. The method describes the quantitation at levels as low as 10 ng/ml with a signal‐to‐noise significantly higher than 10 for the lowest standard, indicating a very low limit of quantification for all analytes. The method uses positive ionization liquid chromatography‐tandem mass spectrometry with the molecular ion [M + Cs] + and Cs + fragment ion (M is the analyte). The molecular ion [M + Cs] + is generated by adding a low level of Cs + in the mobile phase of high‐performance liquid chromatography separation. The advantages obtained using [M + Cs] + as molecular ions are related to the high sensitivity and simplicity of the method compared to other liquid chromatography‐tandem mass spectrometry procedures. As proof of functionality, the method was utilized for the analysis of sweeteners in several energy drinks. The high sensitivity of the liquid chromatography‐tandem mass spectrometry method was not needed for this type of analysis but for samples with low levels of sweeteners, the method can be highly beneficial.","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":"18 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-06-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136355715","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Development and validation of high‐performance thin layer chromatographic method for simultaneous quantitation of novel combination perindopril erbumine and moxonidine hydrochloride 高效薄层色谱法同时定量新复方哌哚普利与盐酸莫索尼定的建立与验证
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-06-17 DOI: 10.1002/sscp.202300051
A. Akabari, J. Surati, Sagar Patel, Bhumin Pathak, A. Patel, C. Patel, Sagarkumar K. Patel
{"title":"Development and validation of high‐performance thin layer chromatographic method for simultaneous quantitation of novel combination perindopril erbumine and moxonidine hydrochloride","authors":"A. Akabari, J. Surati, Sagar Patel, Bhumin Pathak, A. Patel, C. Patel, Sagarkumar K. Patel","doi":"10.1002/sscp.202300051","DOIUrl":"https://doi.org/10.1002/sscp.202300051","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-06-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48217613","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Simultaneous quantification of Fluticasone propionate and Olopatadine hydrochloride by High‐performance thin‐layer chromatography 高效薄层色谱法同时定量丙酸氟替卡松和盐酸奥洛他定
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-06-17 DOI: 10.1002/sscp.202300070
Bhoomi Patel, S. Patel
{"title":"Simultaneous quantification of Fluticasone propionate and Olopatadine hydrochloride by High‐performance thin‐layer chromatography","authors":"Bhoomi Patel, S. Patel","doi":"10.1002/sscp.202300070","DOIUrl":"https://doi.org/10.1002/sscp.202300070","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-06-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"45794562","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Thin layer chromatography‐densitometric method for quantification of apigenin, oleanolic acid, and β‐sitosterol in clerodendrum serratum (Bharangi) root extract 薄层色谱-密度法定量测定白栎根提取物中芹菜素、齐墩果酸和β -谷甾醇的含量
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-06-15 DOI: 10.1002/sscp.202300038
Lima Patel, D. Shah, Puja Bhavsar, Zanza Patel, Zeel Shah
{"title":"Thin layer chromatography‐densitometric method for quantification of apigenin, oleanolic acid, and β‐sitosterol in clerodendrum serratum (Bharangi) root extract","authors":"Lima Patel, D. Shah, Puja Bhavsar, Zanza Patel, Zeel Shah","doi":"10.1002/sscp.202300038","DOIUrl":"https://doi.org/10.1002/sscp.202300038","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-06-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41628441","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Simultaneous determination of paclitaxel and dasatinib in rat plasma and pharmacokinetic study on liquid chromatography‐tandem mass spectrometry 大鼠血浆中紫杉醇和达沙替尼的同时测定及液相色谱-串联质谱法的药代动力学研究
IF 1.1
SEPARATION SCIENCE PLUS Pub Date : 2023-06-13 DOI: 10.1002/sscp.202300055
Yuan Liang, Jun Yin, Yu Yang, Ruiyan Huang, Penghui Hu, Chang Shu
{"title":"Simultaneous determination of paclitaxel and dasatinib in rat plasma and pharmacokinetic study on liquid chromatography‐tandem mass spectrometry","authors":"Yuan Liang, Jun Yin, Yu Yang, Ruiyan Huang, Penghui Hu, Chang Shu","doi":"10.1002/sscp.202300055","DOIUrl":"https://doi.org/10.1002/sscp.202300055","url":null,"abstract":"","PeriodicalId":21639,"journal":{"name":"SEPARATION SCIENCE PLUS","volume":" ","pages":""},"PeriodicalIF":1.1,"publicationDate":"2023-06-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47147244","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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