RadiocarbonPub Date : 2024-03-19DOI: 10.1017/rdc.2024.32
Fatima Pawełczyk, Magdalena Niedziałkowska, Sławomira Pawełczyk, Natalia Piotrowska, Maciej Sykut
{"title":"RETREATMENT OF BONE MATERIAL IN THE GLIWICE RADIOCARBON LABORATORY USING ULTRAFILTRATION","authors":"Fatima Pawełczyk, Magdalena Niedziałkowska, Sławomira Pawełczyk, Natalia Piotrowska, Maciej Sykut","doi":"10.1017/rdc.2024.32","DOIUrl":"https://doi.org/10.1017/rdc.2024.32","url":null,"abstract":"Preparation of bones for radiocarbon (<jats:sup>14</jats:sup>C) dating is still quite a challenge for researchers. The methods are being tested and improved, to increase reliability of dating results and to verify the previous ones. In this work, a set of gelatine samples, extracted from <jats:italic>Cervus elaphus</jats:italic> and <jats:italic>Cervus canadensis</jats:italic> bones from various sites in Europe and a set of human bones from archaeological sites in Poland were subjected to retreatment using ultrafiltration in Gliwice Radiocarbon Laboratory. The tested samples represent a wide range of ages, from older than 40,000 <jats:sup>14</jats:sup>C years BP to modern. The prepared material was subjected to the measurement of C/N atomic ratios and <jats:sup>14</jats:sup>C dating using the accelerator mass spectrometry (AMS) technique. Also, the stable isotopes (δ<jats:sup>13</jats:sup>C and δ<jats:sup>15</jats:sup>N) values were determined. In a few cases ultrafiltration allows to improve gelatine quality for long-stored samples, by increasing the %C and %N as well as decreasing C/N<jats:sub>at</jats:sub> ratios. Nevertheless, this effect was not observed for majority of the samples. Remeasurements of long-term stored samples give mostly the same <jats:sup>14</jats:sup>C ages for ultrafiltered ones and for those without ultrafiltration.","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-03-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140166110","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-03-14DOI: 10.1017/rdc.2024.18
Damian Wiktorowski, Marek Krąpiec, Jacek Pawlyta, Joanna Barniak, Andrzej Rakowski
{"title":"USING RAPID ATMOSPHERIC 14C CHANGES IN THE 7TH CENTURY BC TO PRECISELY DATE THE FLOATING CHRONOLOGY FOR PINE WOOD FROM JÓZEFOWO (NORTHERN POLAND)","authors":"Damian Wiktorowski, Marek Krąpiec, Jacek Pawlyta, Joanna Barniak, Andrzej Rakowski","doi":"10.1017/rdc.2024.18","DOIUrl":"https://doi.org/10.1017/rdc.2024.18","url":null,"abstract":"<p>The floating dendrochronological sequence of pine wood from Józefowo, N. Poland was expected to cover the ∼660 BC radiocarbon (<span>14</span>C) excursion. The sequence was radiocarbon dated using the OxCal wiggle matching procedure and the IntCal20 calibration curve. <span>14</span>C concentrations were measured in one-year α-cellulose samples from around 660 BC. The published data on the ∼660 BC <span>14</span>C excursion from Grabie, Poland were used to absolute date the Józefowo chronology with 1-year accuracy. The results confirm the occurrence of a rapid increase in Δ<span>14</span>C in 664/663 BC and its potential to be used as a fixing point for floating dendrochronological sequences.</p>","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-03-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140125034","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-03-11DOI: 10.1017/rdc.2024.24
David Boyer
{"title":"HORIZONTAL WATERMILL CHRONOLOGIES BASED ON 14C DATING OF ORGANICS IN MORTARS: A CASE STUDY FROM JARASH, JORDAN","authors":"David Boyer","doi":"10.1017/rdc.2024.24","DOIUrl":"https://doi.org/10.1017/rdc.2024.24","url":null,"abstract":"<p>Horizontal watermills in the southern Levant have proved difficult to date. This study investigates the use of radiocarbon (<span>14</span>C) dating of various organic carbon fractions in structural mortars and carbonate deposits to identify <span>terminus post quem</span> (TPQ) construction dates for seven arubah watermills and two chute watermills in northern Jordan. Dating results from the various organic fractions are discussed in the contexts of carbon fraction integrity and mortar type. The arubah watermill construction dates fall into two chronological groups. Four arubah watermills have Middle Islamic (late 12th to early 14th century AD) construction dates based on macrocharcoal and bulk organic fraction ages, whereas the bulk organic fraction ages of two earlier arubah watermills straddle the Byzantine-Early Islamic transition. Their possible fifth to seventh-century construction dates are among the earliest in the southern Levant. Limited <span>14</span>C data from the chute water mills suggests that the earliest may date to the sixth–seventh century period, concurrent with the older arubah watermills. The study supports the viability of the AMS <span>14</span>C method to provide estimated TPQ construction dates for watermills, providing caution is exercised. Short-lived macrocharcoals have the highest integrity but are subject to severe sample loss during pretreatment. <span>14</span>C ages from humic and humin fractions in earthen mortars are influenced by “old carbon” contamination, possibly a soil reservoir effect, and are centuries older than the probable construction date. Attention is drawn to the potential use of arubah carbonate deposits as proxy records of water flow, watermill use, and hydroclimate.</p>","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-03-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140099872","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-03-11DOI: 10.1017/rdc.2024.19
Angélica Santa Cruz
{"title":"CHRONOLOGICAL STUDY OF COLLECTIVE BURIALS IN THE NORTHERN IBERIAN PLATEAU: ANALYSIS OF RADIOCARBON DATES ON HUMAN BONES FROM THE MEGALITHIC COMPLEX OF LA LORA (BURGOS, SPAIN)","authors":"Angélica Santa Cruz","doi":"10.1017/rdc.2024.19","DOIUrl":"https://doi.org/10.1017/rdc.2024.19","url":null,"abstract":"<p>This paper offers a temporal analysis of the megalithic group of La Lora in the context of northern Iberian Plateau megalithism. For this purpose, 67 accelerator mass spectrometry radiocarbon (AMS <span>14</span>C) dates were obtained on human bone from the minimum number of individuals recovered from nine tombs. This is the first systematic dating project carried out in this dolmen group and has enabled the chronology of the main funerary series to be updated. The results reveal that the actual funerary use dates mainly to the 4th millennium BC, although, as deduced from the archaeological material, some tombs were reused in later periods. Additionally, the significant architectural polymorphism of the group, consisting mainly of simple dolmens and large corridor tombs, suggested a temporal evolution to monumentality. However, the dating shows a more complex reality, since it is likely that the large tombs functioned as funerary pantheons during the 4th millennium BC, characterized by a cyclical and recurrent use. In contrast, the simpler structures were preferred to be of shorter use and restricted to the first half of the 4th millennium.</p>","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-03-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140100205","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-03-11DOI: 10.1017/rdc.2024.22
Emma Loftus, Marlize Lombard, Maryna Steyn
{"title":"DATED HOLOCENE HUMAN REMAINS FROM SOUTH AFRICA: RECALIBRATION AND BROAD CONTEXTUALIZATION","authors":"Emma Loftus, Marlize Lombard, Maryna Steyn","doi":"10.1017/rdc.2024.22","DOIUrl":"https://doi.org/10.1017/rdc.2024.22","url":null,"abstract":"<p>The study of human remains can provide valuable information about aspects of past populations. Here we present an updated database consisting of 590 radiocarbon (<span>14</span>C) dates for human remains from Holocene South Africa before European contact. We calibrated or recalibrated all the previously published dates using the most recent calibration curve for the southern hemisphere. Each date is roughly georeferenced and plotted according to their Stone Age or Iron Age contexts, revealing the broad distribution pattern of dated Holocene human remains across South Africa—perhaps reflecting aspects of past population distribution and densities, but also underscoring historical collection practices, archaeological research focus, and preservation conditions. We use Kernel Density Estimation models to show peaks and troughs of dated remains through time, with Later Stone Age peaks at ∼5.5 ka cal BP, ∼2 ka cal BP and ∼0.5 ka cal BP, and Iron Age peaks ∼1.1 ka cal BP and ∼0.5 ka cal BP, some of which show broad correspondence to climatic data. Our data, based on dated remains only, do not provide a full reflection of past populations, and our large-scale, coarse-grained analysis cannot yet assess the reasons for the peaks in dated human remains in detail. Yet, the study provides a new resource, and a data-driven overview that highlights aspects to be explored with further contextual analyses against the available archaeological records, population histories and climatic indicators through time and across space.</p>","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-03-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140099874","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-02-27DOI: 10.1017/rdc.2024.11
Khaled Al-Bashaireh
{"title":"RECONSTRUCTING THE CHRONOLOGY OF BUILDING THE SOUTHWEST CHURCH OF UMM EL-JIMAL, JORDAN BY AMS RADIOCARBON DATING OF MORTAR AND PLASTER","authors":"Khaled Al-Bashaireh","doi":"10.1017/rdc.2024.11","DOIUrl":"https://doi.org/10.1017/rdc.2024.11","url":null,"abstract":"The research aims to reconstruct the chronology of building the Southwest Church, Umm el-Jimal, Jordan by AMS radiocarbon dating organic inclusions uncovered from the mortars collected from the floor of the church, seat of the apse and the base of the north wall. It sheds light on the major aspects of mortar recipes at the time of their production. Samples were examined macroscopically with magnifying lenses and characterized using archaeometric techniques of optical microscopy and X-ray diffraction. The radiocarbon dates showed that 594–643 AD is the most probable age for flooring and plastering the church and 995–1154 AD is the earliest possible date for its final collapse. The preparatory layers of the church floor were laid on an older one, probably of a yard, and its north wall was raised on an older base, both most probably date to the late fifth–early sixth century AD. The production recipe of the mortars is made from a lime binder and inclusions mainly of organic (charcoal) and inorganic (quartz, grog, volcanics). The mortars have the same recipe regardless their bedding and jointing functions which remained unchanged during the building stages of church complex.","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-02-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140007651","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-02-27DOI: 10.1017/rdc.2024.13
Karin Nemoto, Yusuke Yokoyama, Satoshi Horiike, Stephen P Obrochta, Yosuke Miyairi
{"title":"MERIDIONAL MIGRATIONS OF THE INTERTROPICAL CONVERGENCE ZONE DURING THE LAST DEGLACIATION IN THE TIMOR SEA DETECTED BY EXTENSIVE RADIOCARBON DATING","authors":"Karin Nemoto, Yusuke Yokoyama, Satoshi Horiike, Stephen P Obrochta, Yosuke Miyairi","doi":"10.1017/rdc.2024.13","DOIUrl":"https://doi.org/10.1017/rdc.2024.13","url":null,"abstract":"At the Intertropical Convergence Zone (ITCZ), the northern and southern Tradewinds converge, and this region is characterized by low atmospheric pressure and high precipitation. The climate in the Timor Sea is characterized by seasonal precipitation changes driven by meridional migrations of the ITCZ and the monsoonal front. The ITCZ shifts in response to changes in the thermal balance between the northern and southern hemispheres. Thus, reconstruction of paleo-precipitation in the Timor Sea is expected to reveal past changes in both regional and global climate, the latter through inference of the ITCZ position. To reconstruct paleo-precipitation in the Timor Sea, we performed extensive radiocarbon analysis on both planktonic foraminifera and total organic carbon (TOC), which is derived from terrestrial and marine sources. Increased precipitation enhances the fraction of relatively old, terrestrial carbon to the core site, which in turn increases the difference between the ages of TOC and planktonic foraminifera. Variations in radiocarbon ages reveal that during northern hemisphere cooling intervals such as Heinrich Stadial 1 and the Younger Dryas, the ITCZ was in a southern position, thus increasing precipitation in the Timor Sea. However, the Timor Sea was dryer during the Bølling–Allerød warming as the ITCZ shifted northward.","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-02-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140007601","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-02-27DOI: 10.1017/rdc.2024.14
Marine Wojcieszak, Laurent Fontaine, Jan Elsen, Roald Hayen, Alexander Lehouck, Mathieu Boudin
{"title":"HISTORIC LIME MORTARS COMPOSITION AND TERMINOLOGY FOR RADIOCARBON DATING—CASE STUDIES BASED ON THIN-SECTION PETROGRAPHY AND CATHODOLUMINESCENCE","authors":"Marine Wojcieszak, Laurent Fontaine, Jan Elsen, Roald Hayen, Alexander Lehouck, Mathieu Boudin","doi":"10.1017/rdc.2024.14","DOIUrl":"https://doi.org/10.1017/rdc.2024.14","url":null,"abstract":"Since the first developments of anthropogenic lime materials radiocarbon (<jats:sup>14</jats:sup>C) dating in the 1960s, numerous studies have been undertaken and developed to investigate the topic further. Historic mortars are complex composite and open system materials that can incorporate a large range of components. Due to the complexity of the historic lime mortars composition, they are not part of a routine protocol in most radiocarbon laboratories and reliable dating is not always achieved. A thorough characterization needs to be performed and different preparation methods can be considered as a function of their compositions. A vast range of terms are employed to qualify the lime mortars components and alterations that can possibly have an influence on the dating result. Here, a detailed description of these components and the various terms used is listed. To illustrate this, images obtained by thin-section petrography and cathodoluminescence are presented in addition to radiocarbon results using stepwise acid hydrolysis on Belgian mortars having different provenance, state, age and composition. Depending on the type of aggregate used, the type of binder and its conservation state, the eventual presence of weathering carbonates and the assumed speed of the carbonation process, the reliability of radiocarbon measurements using the stepwise acid hydrolysis technique is discussed and confronted with presumed historical constraints.","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-02-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140007645","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-02-27DOI: 10.1017/rdc.2024.10
Jennifer Birch, Sturt W Manning, John P Hart, Brita Lorentzen
{"title":"EVALUATING THE TIMING OF EARLY VILLAGE DEVELOPMENT IN NEW YORK: MORE DATES FROM CLASSIC NEW YORK SITES","authors":"Jennifer Birch, Sturt W Manning, John P Hart, Brita Lorentzen","doi":"10.1017/rdc.2024.10","DOIUrl":"https://doi.org/10.1017/rdc.2024.10","url":null,"abstract":"Five sites in present-day New York have played important roles in archaeological narratives surrounding the development of settled village life in northeastern North America. Excavated in the mid-twentieth century, the Roundtop, Maxon-Derby, Sackett or Canandaigua, Bates, and Kelso sites include evidence related to the transition from semisedentary settlement-subsistence patterns during the twelfth through fourteenth centuries AD to those associated with fifteenth century and later settled Iroquoian villagers. Radiocarbon dates for each site were obtained early in the development of the method and again following the transition to AMS dating. Here, we present new or recently-published dates for these sites, combined with reliable existing dates in Bayesian models, including in some cases short tree-ring sequenced wiggle-matches on wood charcoal. Our results clarify the timing of each site’s occupation(s), revealing both continuity and discontinuity in the development of longhouse dwellings, sedentism, and the repeated re-use of some site locations over hundreds of years.","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-02-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140007603","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
RadiocarbonPub Date : 2024-02-27DOI: 10.1017/rdc.2024.4
A V Petrozhitskiy, E V Parkhomchuk, M M Ignatov, D V Kuleshov, L A Kutnyakova, E S Konstantinov, V V Parkhomchuk
{"title":"COMPARATIVE FEATURES OF BINP AMS AND MICADAS FACILITIES WORKING AT AMS GOLDEN VALLEY, RUSSIA","authors":"A V Petrozhitskiy, E V Parkhomchuk, M M Ignatov, D V Kuleshov, L A Kutnyakova, E S Konstantinov, V V Parkhomchuk","doi":"10.1017/rdc.2024.4","DOIUrl":"https://doi.org/10.1017/rdc.2024.4","url":null,"abstract":"The AMS Golden Valley radiocarbon analysis laboratory is equipped with two accelerator mass spectrometers: AMS facility from Budker Institute of Nuclear Physics (BINP AMS) and MIni CArbon DAting System (MICADAS-28) from Ionplus AG and two graphitization systems: Automated Graphitization Equipment (AGE-3) from Ionplus AG and Absorption-catalytic setup developed in Boreskov Institute of Catalysis (ACS BIC). The laboratory provides routine <jats:sup>14</jats:sup>C analyses of various samples: collagen, cellulose, humic acids, carbonates from sediments, etc. The main focus of the laboratory is to determine the age of archaeological artifacts by radiocarbon dating. This work presents a comprehensive description of the BINP AMS facility, with its operation compared with that of MICADAS in the same laboratory. In 2022, the AMS Golden Valley laboratory participated for the first time in the Glasgow International Radiocarbon Inter-comparison (GIRI). The samples were graphitized on the AGE-3 and subsequently measured in both AMS facilities. A comparison of the results of the two series of experiments, namely AGE-3 + MICADAS-28 and AGE-3 + BINP AMS, is given.","PeriodicalId":21020,"journal":{"name":"Radiocarbon","volume":null,"pages":null},"PeriodicalIF":8.3,"publicationDate":"2024-02-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140007644","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"地球科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}