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Journal of The Chemical Society D: Chemical Communications最新文献

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Nuclear magnetic resonance isotropic shifts of europium oxaloacetates 草酰乙酸铕的核磁共振各向同性位移
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C29710001047
C. Reyes-Zamora, C. Tsai
{"title":"Nuclear magnetic resonance isotropic shifts of europium oxaloacetates","authors":"C. Reyes-Zamora, C. Tsai","doi":"10.1039/C29710001047","DOIUrl":"https://doi.org/10.1039/C29710001047","url":null,"abstract":"N.m.r. isotropic shifts of the CH2 group of europium oxaloacetates provide spectral evidence for the formation of the α-oxocarboxylate complex between oxaloacetic acid and metal ions in aqueous solution.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"24 1","pages":"1047-1047"},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85491573","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
1,4-Shift of hydrogen from carbon to carbon in the lead tetra-acetate oxidation of monocyclic and acyclic alcohols 1,4-氢在四乙酸铅氧化单环和无环醇过程中由碳向碳的转变
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C29710001612
D. Jeremić, S. Milosavljevic, V. Andrejević, M. Jakovljević-Marinković, Ẑ. Čeković, M. Mihailović
{"title":"1,4-Shift of hydrogen from carbon to carbon in the lead tetra-acetate oxidation of monocyclic and acyclic alcohols","authors":"D. Jeremić, S. Milosavljevic, V. Andrejević, M. Jakovljević-Marinković, Ẑ. Čeković, M. Mihailović","doi":"10.1039/C29710001612","DOIUrl":"https://doi.org/10.1039/C29710001612","url":null,"abstract":"The use of α-deuteriated substrates has established that in the lead tetra-acetate oxidation of certain secondary alicyclic and open-chain alcohols, ketone formation proceeds, in part, by 1,4-transfer of hydrogen from the carbinol (α) carbon atom to the δ-carbon atom.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"223 1","pages":"1612-1613"},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"85930162","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Crystal structures of two organo-manganese complexes formed by acetyl migration to a co-ordinated double bond 乙酰基向配位双键迁移形成的两种有机锰配合物的晶体结构
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C29710000752
M. Bennett, G. B. Robertson, R. Watt, P. Whimp
{"title":"Crystal structures of two organo-manganese complexes formed by acetyl migration to a co-ordinated double bond","authors":"M. Bennett, G. B. Robertson, R. Watt, P. Whimp","doi":"10.1039/C29710000752","DOIUrl":"https://doi.org/10.1039/C29710000752","url":null,"abstract":"The structures of a delocalised pseudo-π-allylic (three electron)π-oxopropyl manganese tricarbonyl complex (A) and a σ-bonded Mn–C oxobutyl tricarbonyl complex (B) have been determined by three-dimensional X-ray structural analysis.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"333 1","pages":"752-753"},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76598084","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 9
Structure of evertetrose and everninonitrose evertrose和evernitrose的结构
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C29710000746
A. Ganguly, O. Sarre, S. Szmulewicz
{"title":"Structure of evertetrose and everninonitrose","authors":"A. Ganguly, O. Sarre, S. Szmulewicz","doi":"10.1039/C29710000746","DOIUrl":"https://doi.org/10.1039/C29710000746","url":null,"abstract":"The structure and absolute stereochemistry of evertetrose and everninonitrose, two degradation products of everninomicin “D”, have been established.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"406 1","pages":"746-746"},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76709776","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
Direct observation of the two forms of aquocyanocobyric acid in water by carbon-13 Fourier transform nuclear magnetic resonance 用碳-13傅里叶变换核磁共振直接观察水中两种形态的水氰酸
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C29710000728
D. Doddrell, A. Allerhand
{"title":"Direct observation of the two forms of aquocyanocobyric acid in water by carbon-13 Fourier transform nuclear magnetic resonance","authors":"D. Doddrell, A. Allerhand","doi":"10.1039/C29710000728","DOIUrl":"https://doi.org/10.1039/C29710000728","url":null,"abstract":"Proton-decoupled natural-abundance carbon-13 Fourier transform n.m.r. spectra of aqueous solutions of aquocyanocobyric acid and dicyanocobyric acid were recorded at 15·08 MHz: the spectrum of the first compound showed the presence of two isomers, and many of the carbon atoms showed large chemical shift variations between the two isomers.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"64 1","pages":"728-729"},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76863200","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
The synthesis of cis,cis-1,3,5-triaminocyclohexane-NN′N′-triacetic acid and its cobalt(III) complex 顺式，顺式-1,3,5-三氨基环己烷- nn ' n ' -三乙酸及其钴(III)配合物的合成
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C2971000065B
L. J. Zompa, J. Shindler
{"title":"The synthesis of cis,cis-1,3,5-triaminocyclohexane-NN′N′-triacetic acid and its cobalt(III) complex","authors":"L. J. Zompa, J. Shindler","doi":"10.1039/C2971000065B","DOIUrl":"https://doi.org/10.1039/C2971000065B","url":null,"abstract":"The synthesis of a new stereospecific amino-acid cis,cis-1,3,5-triaminocyclohexane-NN′N″-triacetic acid and its cobalt(III) complex are reported.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"42 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76872277","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Metal reductions of malonates and oxalates. A covenient decarboxylation route for disubstituted malonates and synthesis of keten acetals 丙二酸盐和草酸盐的金属还原。二取代丙二酸酯的便捷脱羧途径及酮缩醛的合成
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C29710000136
Y. Kuo, Francis. Chen, C. Ainsworth, J. Bloomfield
{"title":"Metal reductions of malonates and oxalates. A covenient decarboxylation route for disubstituted malonates and synthesis of keten acetals","authors":"Y. Kuo, Francis. Chen, C. Ainsworth, J. Bloomfield","doi":"10.1039/C29710000136","DOIUrl":"https://doi.org/10.1039/C29710000136","url":null,"abstract":"Alkali-metal reduction of disubstituted malonates or treatment of esters with base in the presence of trimethylchlorosilane gives high yields of the reactive disubstituted keten alkyl trimethylsilyl acetals, while diethyl oxalate, under similar conditions is reduced to 1,2-diethyl-1,2-bis(trimethylsilyloxy)ethylene.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"1 1","pages":"136-137"},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77010295","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 19
The +⅓ oxidation state of mercury 汞的+ 1 / 3氧化态
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C2971001168A
R. Gillespie, P. Ummat
{"title":"The +⅓ oxidation state of mercury","authors":"R. Gillespie, P. Ummat","doi":"10.1039/C2971001168A","DOIUrl":"https://doi.org/10.1039/C2971001168A","url":null,"abstract":"The new compound Hg62+(AsF6–)2 containing mercury in the previously unknown oxidation state of +⅓ has been obtained by the reaction of mercury with arsenic pentafluoride in liquid SO2.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"15 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77142048","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
Sisomicin: stereochemistry and attachment of the unsaturated sugar moiety 西索米星:立体化学和不饱和糖部分的附着
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C29710000924
H. Reimann, R. Jaret, D. Cooper
{"title":"Sisomicin: stereochemistry and attachment of the unsaturated sugar moiety","authors":"H. Reimann, R. Jaret, D. Cooper","doi":"10.1039/C29710000924","DOIUrl":"https://doi.org/10.1039/C29710000924","url":null,"abstract":"","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"517 1","pages":"924-925"},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77143110","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 9
The crystal and molecular structure of Pollards salt, (NH4)6(AuCl4)3Ag2Cl5 Pollards盐(NH4)6(AuCl4)3Ag2Cl5的晶体和分子结构
Journal of The Chemical Society D: Chemical Communications Pub Date : 1971-01-01 DOI: 10.1039/C29710001523
J. Bowles, D. Hall
{"title":"The crystal and molecular structure of Pollards salt, (NH4)6(AuCl4)3Ag2Cl5","authors":"J. Bowles, D. Hall","doi":"10.1039/C29710001523","DOIUrl":"https://doi.org/10.1039/C29710001523","url":null,"abstract":"Crystal structure determination of (NH4)6Au3Ag2Cl17 has shown that it contains the anions AuCl4– and the hitherto unreported Ag2Cl53–, the ions being so arranged that intervalence exchange occurs between them.","PeriodicalId":17278,"journal":{"name":"Journal of The Chemical Society D: Chemical Communications","volume":"26 1","pages":"1523-1523"},"PeriodicalIF":0.0,"publicationDate":"1971-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77223706","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
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