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Journal of Liquid Chromatography & Related Technologies最新文献

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Online extraction and determination of active components from Huangqi Chifeng Decoction based on a homemade monolithic adsorbent with a micron-tube structure 基于自制微米管结构整体吸附剂的黄芪赤风汤有效成分在线提取及测定
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-12-23 DOI: 10.1080/10826076.2025.2602141
Yunting Mao, Xinli Yang, Xiaoyu Zhang, Ligai Bai
{"title":"Online extraction and determination of active components from Huangqi Chifeng Decoction based on a homemade monolithic adsorbent with a micron-tube structure","authors":"Yunting Mao, Xinli Yang, Xiaoyu Zhang, Ligai Bai","doi":"10.1080/10826076.2025.2602141","DOIUrl":"https://doi.org/10.1080/10826076.2025.2602141","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"1 1","pages":"1-9"},"PeriodicalIF":0.0,"publicationDate":"2025-12-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147334212","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Relationship between capillary electrophoretic mobility and zeta potential of arginine poly (ester amide)-albumin complex 精氨酸聚（酯酰胺）-白蛋白复合物毛细管电泳迁移率与zeta电位的关系
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-12-22 DOI: 10.1080/10826076.2025.2604729
Rui Xie, Fengzhi Zhou, Y M Chen, Chen Sun, Rong Xie, Jianjun Zhang, Yuqi Sun
{"title":"Relationship between capillary electrophoretic mobility and zeta potential of arginine poly (ester amide)-albumin complex","authors":"Rui Xie, Fengzhi Zhou, Y M Chen, Chen Sun, Rong Xie, Jianjun Zhang, Yuqi Sun","doi":"10.1080/10826076.2025.2604729","DOIUrl":"https://doi.org/10.1080/10826076.2025.2604729","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"1 1","pages":"1-8"},"PeriodicalIF":0.0,"publicationDate":"2025-12-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147334092","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A simple, rapid, and green method for determination of three flavonoids in alpine bistort rhizome and Zhuyaliao Zhixie Granules by LC-MS/MS 高效液相色谱-质谱联用（LC-MS/MS）法测定高山参和竹叶调止泻颗粒中三种黄酮类化合物的含量
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-12-15 DOI: 10.1080/10826076.2025.2598213
Liping Hu, Zhuobin He, Boyong Chen, Liling Jin, Qi Huang, Zhengming Qian
{"title":"A simple, rapid, and green method for determination of three flavonoids in alpine bistort rhizome and Zhuyaliao Zhixie Granules by LC-MS/MS","authors":"Liping Hu, Zhuobin He, Boyong Chen, Liling Jin, Qi Huang, Zhengming Qian","doi":"10.1080/10826076.2025.2598213","DOIUrl":"https://doi.org/10.1080/10826076.2025.2598213","url":null,"abstract":"This study developed a rapid and green liquid chromatography-tandem mass spectrometry (LC–MS/MS) method for the simultaneous quantification of three major flavonoids (cianidanol, saxifragin, and miquelianin) in alpine bistort rhizome (ABR) and Zhuyaliao Zhixie Granules (ZZG). To our knowledge, this is the first simultaneous determination of these three compounds in Polygonaceae. Following ultrasonic extraction with 70% methanol, separation was achieved on a Poroshell 120 EC‑C18 column using 0.1% formic acid in water and methanol as the mobile phase. LC–MS/MS detection was performed in the negative ion mode using multiple‑reaction monitoring, with a total analysis time of only 6 min per sample. All analytes showed excellent linearity (<i>r</i> &gt; 0.998) and satisfactory recoveries (94.0–107%) with low relative standard deviations (1.06–2.87%). Quantitative profiling revealed that both source type and provenance significantly affected flavonoid levels in ABR, whereas the granules exhibited markedly reduced levels of these flavonoids compared to the raw botanical materials. Compared to previously reported LC methods, this approach exhibited greater analytical efficiency and was both practical and green according to the Blue Applicability Grade Index (BAGI). The developed method provides a reliable tool for ABR quality evaluation and promotes greener, faster modernization of traditional Chinese medicine analysis.","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"49 1-4","pages":"24-34"},"PeriodicalIF":0.0,"publicationDate":"2025-12-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147905512","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Structure elucidation, synthesis, and RRF determination of a praziquantel degradant in a liquid finished drug product 液体制剂中吡喹酮降解物的结构解析、合成和RRF测定
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-08-06 DOI: 10.1080/10826076.2025.2542776
Jiangtao He, Abu M. Rustum
{"title":"Structure elucidation, synthesis, and RRF determination of a praziquantel degradant in a liquid finished drug product","authors":"Jiangtao He, Abu M. Rustum","doi":"10.1080/10826076.2025.2542776","DOIUrl":"https://doi.org/10.1080/10826076.2025.2542776","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"48 16-20","pages":"583-595"},"PeriodicalIF":0.0,"publicationDate":"2025-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147879662","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Field isolation and capture of fluoroquinolones in the water environment with magnetic solid-phase extraction technique prior to HPLC quantification 在高效液相色谱定量之前，采用磁固相萃取技术对水体中氟喹诺酮类药物进行现场分离和捕获
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-07-26 DOI: 10.1080/10826076.2025.2536779
Ou Sha, Yuan Xu, Yunfan Wu, Dewei Wang, Yang Yao, Kaixuan Zhang
{"title":"Field isolation and capture of fluoroquinolones in the water environment with magnetic solid-phase extraction technique prior to HPLC quantification","authors":"Ou Sha, Yuan Xu, Yunfan Wu, Dewei Wang, Yang Yao, Kaixuan Zhang","doi":"10.1080/10826076.2025.2536779","DOIUrl":"https://doi.org/10.1080/10826076.2025.2536779","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"48 16-20","pages":"572-582"},"PeriodicalIF":0.0,"publicationDate":"2025-07-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147898605","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
A HPLC-MS method for quantitative analysis of 9 components in Ginkgo biloba leaf concentrate based on the analytical quality by design 建立了基于分析质量设计的银杏叶浓缩液中9种成分的HPLC-MS定量分析方法
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-05-24 DOI: 10.1080/10826076.2025.2507957
Jinhao Li, Yuanyuan Wang, Juan Du, Huanhuan Meng, Yingchao Wang, Xingchu Gong
{"title":"A HPLC-MS method for quantitative analysis of 9 components in Ginkgo biloba leaf concentrate based on the analytical quality by design","authors":"Jinhao Li, Yuanyuan Wang, Juan Du, Huanhuan Meng, Yingchao Wang, Xingchu Gong","doi":"10.1080/10826076.2025.2507957","DOIUrl":"https://doi.org/10.1080/10826076.2025.2507957","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"48 16-20","pages":"484-493"},"PeriodicalIF":0.0,"publicationDate":"2025-05-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147331139","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Development and validation of a detection method of alendronate in human plasma by high-performance liquid chromatography/tandem mass spectrometry (HPLC–MS/MS) 高效液相色谱/串联质谱（HPLC-MS /MS）检测人血浆中阿仑膦酸钠方法的建立与验证
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-05-19 DOI: 10.1080/10826076.2025.2495039
Xuefeng Zhao, Qinling Ou, Lijia Wang, Mingjie Yu, Jin-xing Huang, Feng Qiu
{"title":"Development and validation of a detection method of alendronate in human plasma by high-performance liquid chromatography/tandem mass spectrometry (HPLC–MS/MS)","authors":"Xuefeng Zhao, Qinling Ou, Lijia Wang, Mingjie Yu, Jin-xing Huang, Feng Qiu","doi":"10.1080/10826076.2025.2495039","DOIUrl":"https://doi.org/10.1080/10826076.2025.2495039","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"48 16-20","pages":"443-451"},"PeriodicalIF":0.0,"publicationDate":"2025-05-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147917853","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis of amide-incorporated silica monolith stationary phase for the separation of benzene derivatives with better chromatographic performance: Experimental and computational analysis 用于苯衍生物分离的酰胺型硅胶整体固定相的合成：实验与计算分析
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-04-03 DOI: 10.1080/10826076.2025.2484776
Faiz Ali, Nashrah Azad, Muhammad Shoaib Ismail, Zeid A. ALOthman, Won Jo Cheong
{"title":"Synthesis of amide-incorporated silica monolith stationary phase for the separation of benzene derivatives with better chromatographic performance: Experimental and computational analysis","authors":"Faiz Ali, Nashrah Azad, Muhammad Shoaib Ismail, Zeid A. ALOthman, Won Jo Cheong","doi":"10.1080/10826076.2025.2484776","DOIUrl":"https://doi.org/10.1080/10826076.2025.2484776","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"48 16-20","pages":"366-380"},"PeriodicalIF":0.0,"publicationDate":"2025-04-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147902501","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis and high performance liquid chromatographic analysis of butoxylation byproducts 丁氧基化副产物的合成及高效液相色谱分析
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-03-13 DOI: 10.1080/10826076.2025.2475280
Fengqin Li, Jingjie Zhou, Chunyu Wang, Yukai Wang, Ke Zhang, Jinyuan Sun, Huibin Liang, Yuqi Liu, Tao Geng
{"title":"Synthesis and high performance liquid chromatographic analysis of butoxylation byproducts","authors":"Fengqin Li, Jingjie Zhou, Chunyu Wang, Yukai Wang, Ke Zhang, Jinyuan Sun, Huibin Liang, Yuqi Liu, Tao Geng","doi":"10.1080/10826076.2025.2475280","DOIUrl":"https://doi.org/10.1080/10826076.2025.2475280","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"48 11-15","pages":"302-312"},"PeriodicalIF":0.0,"publicationDate":"2025-03-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147885842","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
An improved ultrasound-assisted extraction (UAE) and HPLC-PDA methods for multiclass analysis of pharmaceutical residues in fish 改进的超声辅助提取（UAE）和高效液相色谱- pda方法用于鱼类中药物残留的多类分析
4区 化学
Journal of Liquid Chromatography & Related Technologies Pub Date : 2025-02-12 DOI: 10.1080/10826076.2025.2460155
Yusran Ibrahim, Tuan Fauzan Tuan Omar, Adiana Ghazali, May Ong
{"title":"An improved ultrasound-assisted extraction (UAE) and HPLC-PDA methods for multiclass analysis of pharmaceutical residues in fish","authors":"Yusran Ibrahim, Tuan Fauzan Tuan Omar, Adiana Ghazali, May Ong","doi":"10.1080/10826076.2025.2460155","DOIUrl":"https://doi.org/10.1080/10826076.2025.2460155","url":null,"abstract":"","PeriodicalId":16295,"journal":{"name":"Journal of Liquid Chromatography & Related Technologies","volume":"48 11-15","pages":"263-270"},"PeriodicalIF":0.0,"publicationDate":"2025-02-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"147918395","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
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