{"title":"Fast-scan magnetic resonance, principles and applications","authors":"W.S.B","doi":"10.1016/0022-2364(92)90072-F","DOIUrl":"10.1016/0022-2364(92)90072-F","url":null,"abstract":"","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Page 632"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90072-F","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"53145930","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"A transmitter modification which provides increased sensitivity for homonuclear decoupling experiments","authors":"Robert W Dykstra","doi":"10.1016/0022-2364(92)90061-B","DOIUrl":"10.1016/0022-2364(92)90061-B","url":null,"abstract":"","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Pages 571-574"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90061-B","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79930294","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Bimodal loop-gap resonator","authors":"A.I Tsapin , James S Hyde, W Froncisz","doi":"10.1016/0022-2364(92)90055-C","DOIUrl":"10.1016/0022-2364(92)90055-C","url":null,"abstract":"<div><p>A bimodal loop-gap resonator for electron-electron double resonance at X band is described. Considerable detail is given on frequency tuning; in one of the geometries described, a total tuning range of 500 MHz in the difference of the resonant frequencies of the two modes was achieved. The hypothesis is made that bimodal loop-gap resonators, because of their relatively low <em>Q</em> values, offer opportunities to arrive at structures that are more practical than bimodal cavities for routine EPR use. Data appear to support this hypothesis.</p></div>","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Pages 484-490"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90055-C","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"88431847","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Cumulative author index volumes 96–100","authors":"","doi":"10.1016/0022-2364(92)90075-I","DOIUrl":"https://doi.org/10.1016/0022-2364(92)90075-I","url":null,"abstract":"","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Pages 637-644"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90075-I","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136545213","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Suppression of artifacts in phase-sensitive COSY","authors":"Christopher J Turner , William C Hutton","doi":"10.1016/0022-2364(92)90054-B","DOIUrl":"10.1016/0022-2364(92)90054-B","url":null,"abstract":"<div><p>High repetition rates generate systematic errors in phase-sensitive COSY spectra because incomplete relaxation allows magnetization from one transient to carry over and interfere with the next. The resultant artifacts appear at integral multiples of the resonance offset in the <em>F</em><sub>1</sub>, dimension. Product-operator calculations are used to predict permutations of the RF phase cycle in which these artifacts are canceled. The success of these permutations is tested experimentally. It is shown that the axial-peak suppression and dummy transients are vital for the suppression of repetition-rate artifacts, but that quadrature-image suppression is irrelevant. The best permutations of the phase cycle reduce repetition-rate artifacts to about 1% of their parent peaks when recycle delays three times less than the longitudinal relaxation time are used.</p></div>","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Pages 469-483"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90054-B","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"72982433","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"13C-detected 1H dipolar magic-angle-spinning nmr experiments with isotropic mixing","authors":"Atsushi Kubo, Charles A McDowell","doi":"10.1016/0022-2364(92)90057-E","DOIUrl":"10.1016/0022-2364(92)90057-E","url":null,"abstract":"<div><p>Cross polarization using the WIM-24 (windowless isotropic mixing) pulse sequence and also <sup>13</sup>C-detected <sup>1</sup>H dipolar magic-angle-spinning nuclear magnetic resonance employing the WIM-24 pulse sequence during the mixing period on a sample of the urea tridecane inclusion compound was investigated. Numerical calculations of the theoretically expected spectra were performed, using equations derived by two methods: (l) from average Hamiltonian theory and (2) the time-evolution operator obtained by multiplying together the instantaneous time-evolution operators (the multistep method). In comparisons of the calculated <sup>13</sup>C-detected <sup>1</sup>H dipolar MAS NMR spectra from these two methods with the experimental spectra, quantitative agreement was found only with the results from the multistep method. The effects of errors in the pulse phases and amplitude of the WIM-24 pulse sequence were investigated by computer simulations based on equations derived from the multistep method. Although the WIM-24 cross-polarization curve was changed significantly by the presence of 2° errors of the pulse phases, or 10% errors in the pulse amplitudes, the <sup>13</sup>C-detected <sup>1</sup>H dipolar MAS NMR spectra obtained by using the WIM24 mixing were found to be rather insensitive to those pulse imperfections. Cross-polarization curves were also calculated for the WALTZ-4 pulse sequence applied synchronously to both the <sup>13</sup>C and the <sup>1</sup>H channels during the mixing period to study rotational resonance effects. The calculations were performed for dipolar and J mixing. The results show that the WALTZ-4 sequence couples with the sample rotation more intensely than does the WIM-24 sequence.</p></div>","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Pages 517-537"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90057-E","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84790497","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Instrumental techniques for low-temperature solid-state NMR studies of peptides and proteins","authors":"R McNamara, C.H Wu, S.J Opella","doi":"10.1016/0022-2364(92)90059-G","DOIUrl":"10.1016/0022-2364(92)90059-G","url":null,"abstract":"","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Pages 559-566"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90059-G","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"82410851","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"NMR, basic principles and progress, vol. 23","authors":"W.S.B","doi":"10.1016/0022-2364(92)90071-E","DOIUrl":"https://doi.org/10.1016/0022-2364(92)90071-E","url":null,"abstract":"","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Page 631"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90071-E","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"136532178","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Claudio Dalvit, Günter Bovermann, Klaus Memmert, Lukas Oberer, Hans Widmer, Mauro Zurini
{"title":"Suppression of the direct peaks in two-dimensional 15N-Edited NOESY Experiments of Proteins with Hetero-CORN","authors":"Claudio Dalvit, Günter Bovermann, Klaus Memmert, Lukas Oberer, Hans Widmer, Mauro Zurini","doi":"10.1016/0022-2364(92)90062-C","DOIUrl":"10.1016/0022-2364(92)90062-C","url":null,"abstract":"","PeriodicalId":100800,"journal":{"name":"Journal of Magnetic Resonance (1969)","volume":"100 3","pages":"Pages 575-580"},"PeriodicalIF":0.0,"publicationDate":"1992-12-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/0022-2364(92)90062-C","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75646287","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}