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Re-Examination of Turkey Red 火鸡红的复验
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790039
Recep Karadag, Emre Dolen
{"title":"Re-Examination of Turkey Red","authors":"Recep Karadag,&nbsp;Emre Dolen","doi":"10.1002/adic.200790039","DOIUrl":"10.1002/adic.200790039","url":null,"abstract":"<p>Cotton yarn was dyed in Turkey red using madder through a special method. Amount of the dyestuffs bound to mordanted cotton fibre and the oiling numbers of the cotton yarn was investigated by using TLC (thin layer chromatography) and spectrophotometry. Sn(II) in the bright red cotton yarn was analysed by X-ray diffraction method.</p>","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790039","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40973748","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 20
Introduction: Annali di Chimica 7/2007 介绍:化学年鉴7/2007
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790042
{"title":"Introduction: Annali di Chimica 7/2007","authors":"","doi":"10.1002/adic.200790042","DOIUrl":"https://doi.org/10.1002/adic.200790042","url":null,"abstract":"","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790042","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"109169071","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Application of a Portable XRF Spectrometer for the Non-Invasive analysis of Museum Metal Artefacts 便携式XRF光谱仪在博物馆金属文物无创分析中的应用
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790028
A. G. Karydas
{"title":"Application of a Portable XRF Spectrometer for the Non-Invasive analysis of Museum Metal Artefacts","authors":"A. G. Karydas","doi":"10.1002/adic.200790028","DOIUrl":"10.1002/adic.200790028","url":null,"abstract":"<p>The present paper reviews examples of the application of a portable - in house developed- XRF spectrometer for the analysis of museum metal artefacts in Greece. Specific topics are addressed, in particular, to which extent the qualitative or quantitative XRF analyses reveal important information about the raw materials and manufacture techniques used for gold, silver and bronze alloys in antiquity. The analytical information that it is gained by means of the XRF measurements is further assessed in comparison with the existing archaeometallurgical knowledge.</p>","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790028","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41040277","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 60
Analysis of Frankincense in Archaeological Samples by Gas Chromatography-Mass Spectrometry 考古样品中乳香的气相色谱-质谱分析
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790029
Carole Mathe, Jacques Connan, Paul Archier, Michel Mouton, Catherine Vieillescazes
{"title":"Analysis of Frankincense in Archaeological Samples by Gas Chromatography-Mass Spectrometry","authors":"Carole Mathe,&nbsp;Jacques Connan,&nbsp;Paul Archier,&nbsp;Michel Mouton,&nbsp;Catherine Vieillescazes","doi":"10.1002/adic.200790029","DOIUrl":"10.1002/adic.200790029","url":null,"abstract":"<p>Four archaeological samples, unearthed from Qana in Yemen were analysed by analytical technique, currently applied in the field of petroleum geochemistry, and by gas chromatography coupled with a mass spectrometer (GC-MS). Sample no 1286 comes from a burned warehouse and samples no 964, 963 and 962 from the central sanctuary. These specimens were probably exposed to a heating source. In each case olibanum resin was identified according to the presence of their chemical markers corresponding to α-, β-boswellic and lupeolic acids (3α-hydroxy-olean-12-en-24-oic, 3α-hydroxy-urs-12-en-24-oic and 3α-hydroxy-lup-20(29)en-24-oic acids) and their respective <i>O</i>-acetyled derivatives (3α- <i>O</i>-acetyl -olean-12-en-24-oic, 3α-<i>O</i>-acetyl-urs-12-en-24-oic and 3-<i>O</i>-acetyl-lup-20(29)-en-24-oic acids). Concerning the thermal degradation state of samples, the GC-MS results are in agreement with the geochemical ones. Sample no 1286 and 964 correspond to ageing incense which has not undergone any heating action and are consequently relatively well preserved. Lastly, samples no 963 and 962 are thermally degraded resins and their gross composition data permits to conclude that sample no 963 is only partially burnt while sample no 962 has been much more degraded.</p>","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790029","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41040278","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 30
Filler Segmentation of Sem Paper Images Based on Mathematical Morphology 基于数学形态学的Sem纸图像填充分割
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790038
M. Ait Kbir, Rachid Benslimane, Elisabetta Princi, Silvia Vicini, Enrico Pedemonte
{"title":"Filler Segmentation of Sem Paper Images Based on Mathematical Morphology","authors":"M. Ait Kbir,&nbsp;Rachid Benslimane,&nbsp;Elisabetta Princi,&nbsp;Silvia Vicini,&nbsp;Enrico Pedemonte","doi":"10.1002/adic.200790038","DOIUrl":"10.1002/adic.200790038","url":null,"abstract":"<p>Recent developments in microscopy and image processing have made digital measurements on high-resolution images of fibrous materials possible. This helps to gain a better understanding of the structure and other properties of the material at micro level. In this paper SEM image segmentation based on mathematical morphology is proposed. In fact, paper models images (Whatman, Murillo, Watercolor, Newsprint paper) selected in the context of the Euro Mediterranean PaperTech Project have different distributions of fibers and fillers, caused by the presence of SiAl and CaCO<sub>3</sub> particles. It is a microscopy challenge to make filler particles in the sheet distinguishable from the other components of the paper surface. This objectif is reached here by using switable strutural elements and mathematical morphology operators.</p>","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790038","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"40973747","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
A Cultural Heritage Virtual Learning Community 文化遗产虚拟学习社区
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790043
Ioannis Kozaris, Evangelia A. Varella
{"title":"A Cultural Heritage Virtual Learning Community","authors":"Ioannis Kozaris,&nbsp;Evangelia A. Varella","doi":"10.1002/adic.200790043","DOIUrl":"10.1002/adic.200790043","url":null,"abstract":"","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790043","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83216932","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
The Simultaneous Analysis of Proteins, Lipids, and Diterpenoid Resins Found in Cultural Objects. 在文物中发现的蛋白质、脂类和二萜树脂的同时分析。
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790044
Brian Singer, Ross McGuigan
{"title":"The Simultaneous Analysis of Proteins, Lipids, and Diterpenoid Resins Found in Cultural Objects.","authors":"Brian Singer,&nbsp;Ross McGuigan","doi":"10.1002/adic.200790044","DOIUrl":"10.1002/adic.200790044","url":null,"abstract":"<p>We report a GC-MS method for the simultaneous analysis of proteins oil, and diterpenoid resins found in cultural objects. The method was initially designed for protein analysis of protenaceous paints and adhesives and involves acid hydrolysis as the first step. The amino acids in the protein hydrolysates, thus obtained, are treated with propan-1-ol/ hydrogen chloride and then pentafluoropropionic anhydride. The procedure was found also to yield the propyl esters of fatty acids derived from lipids and diterpenoid acids derived from natural resins, and thus allows the choice of a single method for the analysis of artists media which contain either oil s or proteins or mixtures of both proteins and oils or even resins. Thus natural mixtures such as egg yolk and also mixtures made by the artist such as animal glue / seed oil emulsions can be analysed. Coupled with FTIR analysis of paints and the staining of cross sections, to indicate layer structure the method can help to elucidate the paints and adhesives used by artists.</p>","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790044","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41040276","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 13
Energy Dispersive X-Ray Diffraction Potentiality in the Field of Cultural Heritage: Simultaneous Structural and Elemental Analysis of Various Artefacts 文化遗产领域的能量色散x射线衍射势:各种文物的同时结构和元素分析
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790031
Eugenio Caponetti, Ruggero Caminiti, Delia Chillura Martino, Maria Luisa Saladino
{"title":"Energy Dispersive X-Ray Diffraction Potentiality in the Field of Cultural Heritage: Simultaneous Structural and Elemental Analysis of Various Artefacts","authors":"Eugenio Caponetti,&nbsp;Ruggero Caminiti,&nbsp;Delia Chillura Martino,&nbsp;Maria Luisa Saladino","doi":"10.1002/adic.200790031","DOIUrl":"10.1002/adic.200790031","url":null,"abstract":"<p>The applicability of an Energy Dispersive X-ray Diffractometer to some technical questions in the field of Cultural Heritage is presented. This diffractometer, equipped with a white source, has been utilized for the structural and elemental analysis of some items having different nature. Given its design, the instrument allows to collect data from samples as big as a book or a little more. Samples, without collection of any portion and without any preliminary preparation, have been placed in the instrument and spectra have been collected in a wide energy range that contains X-ray fluorescence and diffraction features. In all cases, data acquired in air and in a non destructive way were reliable and their collection was fast. Fluorescence and X-ray diffraction information, when possible, have been compared with those obtained by XRF micro-analysis and by an Angle Dispersive X-ray Diffractometer equipped with a Cu X-ray source. By using the last two techniques, data have been collected from small areas of the samples.</p>","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790031","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41040280","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Contents: Annali di Chimica 7/2007
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790040
{"title":"Contents: Annali di Chimica 7/2007","authors":"","doi":"10.1002/adic.200790040","DOIUrl":"https://doi.org/10.1002/adic.200790040","url":null,"abstract":"","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790040","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"109169070","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Infrared and Raman Vibrational Spectroscopies Reveal the Palette of Frescos Found in the Medieval Monastery of Karaach Teke 红外和拉曼振动光谱揭示了中世纪卡拉赫特克修道院壁画的调色板
Annali di chimica Pub Date : 2007-05-14 DOI: 10.1002/adic.200790032
T. Zorba, K.S. Andrikopoulos, K.M. Paraskevopoulos, E. Pavlidou, K. Popkonstantinov, R. Kostova, V. Platnyov,  Sister Daniilia
{"title":"Infrared and Raman Vibrational Spectroscopies Reveal the Palette of Frescos Found in the Medieval Monastery of Karaach Teke","authors":"T. Zorba,&nbsp;K.S. Andrikopoulos,&nbsp;K.M. Paraskevopoulos,&nbsp;E. Pavlidou,&nbsp;K. Popkonstantinov,&nbsp;R. Kostova,&nbsp;V. Platnyov,&nbsp; Sister Daniilia","doi":"10.1002/adic.200790032","DOIUrl":"10.1002/adic.200790032","url":null,"abstract":"<p>Vibrational spectroscopy is applied on samples obtained from the excavation area of the medieval Monastery (10<sup>th</sup> century) of Karaach-Teke in Bulgaria. The results of the corresponding study, reveal the type of materials used for the creation of the wall-paintings and give evidence of Byzantine influence, a fact that further supports the well known impact of Byzantium on the technology and thematic-aesthetic features of iconography in Bulgaria during this era. In addition, the complementarity of FTIR and μ-Raman spectroscopies in the identification of pigments is indicated.</p>","PeriodicalId":8193,"journal":{"name":"Annali di chimica","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2007-05-14","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1002/adic.200790032","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41040281","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 15
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