M. Kadanik, L. Burgschat, M. Reich, S. Petersen, O. Kessler
{"title":"Experimental Determination of Heat Transfer using a Polymer Solution Shower during Induction Hardening*","authors":"M. Kadanik, L. Burgschat, M. Reich, S. Petersen, O. Kessler","doi":"10.1515/htm-2021-0007","DOIUrl":"https://doi.org/10.1515/htm-2021-0007","url":null,"abstract":"Abstract Heat treatment simulation of inductive surface hardening of large bearing rings is a challenging multi-physical task. Besides the determination of material and process parameters of induction heating, the quenching process must be modelled to obtain realistic results concerning surface hardening depth as well as information about residual stresses and distortions of the bearing rings. A common method to model quenching processes is to determine heat transfer coefficients for the specific process depending on component surface temperature. This method was used to characterize the shower cooling process using an aqueous polymer solution of a modified polyalkylene glycol (PAG) type. A specifically designed test set-up allowed to determine the heat transfer coefficients for different distances between shower and hot specimen as well as for different impingement angles of the fluid relative to gravitation. Additionally, the calculated heat transfer coefficients were checked and corrected by FEM simulations.","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81064341","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Tribological Stress Behaviour of Cast Iron without and with Surface Treatment under Concentrated Contact Load*","authors":"A. Holst, A. Buchwalder, R. Zenker","doi":"10.1515/htm-2021-0010","DOIUrl":"https://doi.org/10.1515/htm-2021-0010","url":null,"abstract":"Abstract The graphite inclusions typical of grey solidified cast iron materials reduce the load-bearing capacity under locally concentrated pressure and simultaneous sliding stress. Surface treatment processes such as nitriding and electron beam remelting are known to improve the local stress behaviour. In this paper, the effects of the above-mentioned individual processes and their combination on the tribological stress behaviour of ferritic and pearlitic cast irons with different graphite morphologies are discussed. The results obtained in the model wear test ball-plate show that the specific wear coefficient of the investigated cast irons with different graphite morphology can already be reduced by at least one order of magnitude by an approx. 0.5–0.9 mm thick remelted surface layer with a surface hardness of 650–750 HV1. This treatment eliminates the graphite and produces ledeburitic carbides instead. The potential of an additional nitriding treatment depends on the parameters used, i. e. the nitrided layer thickness produced as well as the phase composition and the pore fraction of the compound layer. Based on stress calculations, the experimentally determined main influences such as the coefficient of friction, the pore fraction in the compound layer and the magnitude of the Hertzian pressure on the contact stress could essentially be confirmed.","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83171803","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
S. Hoja, D. Nadolski, M. Steinbacher, R. Fechte-Heinen
{"title":"Optimized Nitriding for Subsequent Induction Heat Treatment","authors":"S. Hoja, D. Nadolski, M. Steinbacher, R. Fechte-Heinen","doi":"10.1515/htm-2021-0008","DOIUrl":"https://doi.org/10.1515/htm-2021-0008","url":null,"abstract":"Abstract Nitriding is used to achieve a high hardness in the surface layer through the precipitation of nitrides. However, to realize high nitriding hardness depths, treatment times of many hours are necessary, which usually also result in a decrease in strength within the nitrided layer and base material. With induction heat treatment, on the other hand, high hardness depths can be achieved in a very short time. However, the maximum hardness increase is limited by the alloy content of the material. By combining nitriding and induction hardening, high hardness depths can be achieved in short treatment times as an alternative to deep nitriding. In addition to a significant saving in process energy surface layer properties that cannot be achieved with the individual processes are expected. In order to fully exploit the potential of the combination treatment, at first suitable conditions must be set during nitriding for the subsequent induction hardening. In the present work, nitriding layers with low-porosity compound layers as well as only diffusion layers were produced and analyzed on typical nitriding and tempering steels for this purpose.","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79659171","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
A. Fischer, B. Scholtes, T. Niendorf, M. S. A. Fischer, Dr.-Ing. habil. Berthold Scholtes, Prof. Dr.-Ing. Thomas Niendorf
{"title":"Influence of Deep Rolling and Induction Hardening on Microstructure Evolution of Crankshaft Sections made from 38MnSiVS5 and 42CrMo4","authors":"A. Fischer, B. Scholtes, T. Niendorf, M. S. A. Fischer, Dr.-Ing. habil. Berthold Scholtes, Prof. Dr.-Ing. Thomas Niendorf","doi":"10.1515/htm-2021-0002","DOIUrl":"https://doi.org/10.1515/htm-2021-0002","url":null,"abstract":"Abstract In order to improve properties of complex automotive components, such as crankshafts, in an application-oriented way, several surface hardening treatments can be applied. Concerning the material performance the definition of adequate process parameters influences the resulting surface properties and, thus, the effectiveness of surface hardening treatments. To analyze most relevant process-microstructure-property relationships, the present paper reports results obtained by two different well-established surface hardening procedures, i. e. deep rolling as a mechanical treatment and induction hardening as a thermal treatment. For each hardening process widely used crankshaft steel grades, i. e. a medium carbon 38MnSiVS5 microalloyed steel and a quenched and tempered 42CrMo4 were selected and thoroughly characterized upon processing, using equal parameter settings. The results reveal that deep rolling in contrast to induction hardening proves to be a less sensitive surface layer treatment with regard to small differences in the initial microstructure, the chemical composition and the applied process parameters. Differences in microstructure evolution with respect to the applied surface hardening treatment are studied and discussed for the highly stressed fillet region of automotive crankshaft sections for all conditions. In this context, high-resolution SEM-based techniques such as EBSD and ECCI are proven to be very effective for fast qualitative evaluation of induced microstructural changes.","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"76849053","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
R. Gansel, C. Zimmermann, L. Fricke, M. Lüdtke, H. Klümper-Westkamp, R. Fechte-Heinen, H. Maier, D. Zaremba
{"title":"Characterization of Graded Subsurface Zones in Industrial Case-Hardening Using a Non-Destructive Testing System","authors":"R. Gansel, C. Zimmermann, L. Fricke, M. Lüdtke, H. Klümper-Westkamp, R. Fechte-Heinen, H. Maier, D. Zaremba","doi":"10.1515/htm-2021-0006","DOIUrl":"https://doi.org/10.1515/htm-2021-0006","url":null,"abstract":"Abstract For process monitoring and quality assurance of case-hardened components, the determination of the case-hardening depth in the manufacturing process after hardening of the subsurface layer is a quality verification that is often required in industry. Currently, these quality assurance tests can only be realized with destructive measures. During case-hardening, the essential microstructural formation, and thus the key component properties are developed during the heat treatment in the cooling section. The testing technique used in the present study is based on the analysis of harmonic signals of eddy current testing. The aim of this project was to achieve an early identification of incorrect cooling processes in the case of a known transformation behaviour of the components during cooling. The data collected in the industrial hardening process show that an evaluation of the carburizing process on the basis of the case-hardening depth can be carried out non-destructively during component cooling and in the cooled state with the use of eddy current technology.","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81302350","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
B. Denkena, P. Kuhlemann, B. Breidenstein, M. Keitel, N. Vogel
{"title":"Influence of Turn-Rolling on the Residual Stresses and Microstructure of C45E and the Effects on Fatigue Life under Cyclic Loading","authors":"B. Denkena, P. Kuhlemann, B. Breidenstein, M. Keitel, N. Vogel","doi":"10.1515/htm-2021-0003","DOIUrl":"https://doi.org/10.1515/htm-2021-0003","url":null,"abstract":"Abstract The microstructure and the residual stress state have a significant influence on the service life of the component. The deep rolling process already enables a significant increase in the strength and service life of highly stressed components. By using the hybrid manufacturing process of turn rolling, the edge zone properties can be influenced to such an extent that the service life is further increased compared to conventional deep rolling. In addition to a change in the residual stress state, the use of the turning process temperature also leads to a significant grain refinement in the edge zone area, which has a positive effect on the component service life. This modification of the edge zone can be significantly influenced by the machining speed.","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74008786","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
A. Gassner, L. Waidelich, H. Palkowski, J. Wilde, H. Mozaffari-Jovein
{"title":"Tribocorrosion Mechanisms of Martensitic Stainless Steels","authors":"A. Gassner, L. Waidelich, H. Palkowski, J. Wilde, H. Mozaffari-Jovein","doi":"10.1515/htm-2021-0004","DOIUrl":"https://doi.org/10.1515/htm-2021-0004","url":null,"abstract":"Abstract In the present study, the influence of the electrochemical potential on the tribocorrosion behavior of X20Cr13 in 0.15 molar NaCl-solution was investigated with the aid of a universal-tribometer under potentiostatic control. The resulting material loss was determined through laser confocal microscopy, while the morphology of the wear tracks and the deformation of the material structure near the surface were observed using light and scanning electron microscopy. The results showed a clear dependence of the material loss and the wear mechanisms from the applied potential. Within the cathodic region, a small amount of the material degradation could be attributed to a strong adhesion and resulting strain hardening as a consequence of an electrochemical weakening and mechanical destruction of the passive layer. The maximum of wear during polarization at the free corrosion potential under friction was explained by galvanic coupling between the wear track and the passive surface near the stability threshold between Fe2+-Ion and Fe2O3 development. Through increasing Polarization onto the free corrosion potential in the absence of friction and into the passive region, a decrease in material loss could be observed which is presumably attributed to the stable passive layer that inhibits electrochemical degradation and favors the formation of a grain refinement zone that slows down mechanical destruction.","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81520795","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
M. Sommer, S. Hoja, M. Steinbacher, R. Fechte-Heinen
{"title":"Investigation of Compound Layer Structures after Nitriding and Nitrocarburizing of Quenched and Tempered Steels","authors":"M. Sommer, S. Hoja, M. Steinbacher, R. Fechte-Heinen","doi":"10.1515/htm-2021-0005","DOIUrl":"https://doi.org/10.1515/htm-2021-0005","url":null,"abstract":"Abstract A compound layer is formed by ingress of nitrogen from an external nitrogen source into the surface layer and the formation of nitrides when the solubility of nitrogen in the bulk material is exceeded. In the surface layer, where the nitrogen concentration is at its maximum level, the nitrides form a closed layer. The compound layer continues to contain alloy nitrides which have formed from the carbides and other precipitates from the bulk material. The properties of the compound layer have a decisive influence on the wear and fatigue behavior of the loaded surfaces. The current investigations deal with the extensive characterization of compound layers that have been produced in heat treatment processes with the aim of producing stress-resistant nitriding layers. The commonly used nitriding and quench and temper (Q&T) steels 31CrMoV9 and 42CrMo4 served as examination material. The structure of the compound layers was varied within the nitriding trials regarding the phase composition, porosity and layer thicknesses. The phase composition of the compound layers was determined by special etching, scanning electron microscopy (SEM), X-ray diffraction and GDOES.","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83570448","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Numerical Study to Understand the Distortion Behavior of a Weight-Reduced Counter Gear*","authors":"J. Kagathara, T. Lübben","doi":"10.1515/htm-2020-0009","DOIUrl":"https://doi.org/10.1515/htm-2020-0009","url":null,"abstract":"Abstract Objectives in the field of lightweight construction can be achieved by changing the component design, among other things. However, a design suitable for production would have to be taken into account, since serious distortion problems can occur after the final heat treatment due to reduced stiffness or asymmetries in the mass distribution. To illustrate this problem area, case hardening experiments using the example of a weight-reduced counter gear made of 20MnCr5 were carried out and have shown significantly different distortion behavior depending on the geometry and process parameters. However, it is difficult or even impossible to understand such a distortion behavior only through experiments, since many different variables can be responsible for dimensional and shape changes. In this context, a simulation tool can be very helpful to identify important variables that cause dimensional and shape changes and to understand the associated processes. This paper attempts to answer some open questions that arise from experiments on distortion behavior through simulations. ◼","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74716505","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"A Model to Predict the Microstructural Constituents after Quenching and Partitioning of Martensitic Stainless Steels","authors":"S. Kresser, R. Schneider, H. Zunko, C. Sommitsch","doi":"10.1515/htm-2020-0008","DOIUrl":"https://doi.org/10.1515/htm-2020-0008","url":null,"abstract":"Abstract The typical heat treatment of martensitic stainless steels comprises hardening and subsequent tempering. Depending on the application and size of the component, tempering is carried out either at low temperatures (< 300 °C) or at high temperatures (> 500 °C). In this paper, tempering at lower temperatures is examined. First, the austenitizing step is considered in greater detail and an optimized formula for the calculation of the MS temperature of such steel grades is created in order to enable to be modelled. For the calculations, the austenite composition is determined at different austenitizing temperatures using thermodynamic simulation. Furthermore, the transformation of austenite into martensite during quenching is described with the help of the Koistinen-Marburger equation. The second part deals with effects in the material at low holding temperatures. Here, the influence of different hardening temperatures and interception temperatures of the quenching procedure is investigated. There is no complete partitioning at temperatures of 300 °C. Certain tempering processes can also take place, such as the formation of transition carbides, so-called M3C carbides. A typical tempering with formation of stable Cr-rich carbides does not occur at this low temperature. Finally, the calculated results of the model correlate well with microstructural investigations (XRD, LOM). ◼","PeriodicalId":44294,"journal":{"name":"HTM-Journal of Heat Treatment and Materials","volume":null,"pages":null},"PeriodicalIF":0.6,"publicationDate":"2021-04-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"82892198","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}