Samira Nazari Moghaddam, A. R. Shabari, Fahimeh Sabbaghi, M. Pourayoubi
{"title":"Synthesis, spectroscopic characterization, crystal structure and hirshfeld surface analysis of (4-Cl-C6H4O)(OC4H8N)2PO amodiphosphoester","authors":"Samira Nazari Moghaddam, A. R. Shabari, Fahimeh Sabbaghi, M. Pourayoubi","doi":"10.33224/RRCH/2019.64.3.01","DOIUrl":"https://doi.org/10.33224/RRCH/2019.64.3.01","url":null,"abstract":"A new amidophosphoester, (4-Cl-C6H4O)(OC4H8N)2PO, was synthesized and characterized by spectroscopic methods (IR, P-, C-, H-NMR) and single-crystal X-ray diffraction. The crystal belongs to the space group P21/c, and the asymmetric unit of structure is composed of one complete molecule. The P atom has a distorted tetrahedral (O)(N)2P(O) environment with one of the O═P—N angles as the maximum angle at the P atom and one of the O—P—N angles as the minimum angle. The oxygen atom of the P—O—C6H4-4-Cl part may be ascribed with the hybridization including a few more “s” character with respect to “sp”, reflected in the P—O—C angle (127°). In the crystal, the molecules are aggregated through CH...O hydrogen bonds forming a two-dimensional array along the bc plane.","PeriodicalId":21323,"journal":{"name":"Revue Roumaine De Chimie","volume":"1 1","pages":""},"PeriodicalIF":0.5,"publicationDate":"2019-03-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"49082336","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Quality of Analytical Results","authors":"P. Konieczka, J. Namieśnik","doi":"10.1201/9781315295015-2","DOIUrl":"https://doi.org/10.1201/9781315295015-2","url":null,"abstract":"The prevailing trend to determine analytes at increasingly lower concentrations brings about the issue of quality control and quality assurance of analytical results, which are the source of analytical information. The paper reviews basic concepts of quality assurance/quality control. The importance of traceability is also discussed.","PeriodicalId":21323,"journal":{"name":"Revue Roumaine De Chimie","volume":"46 1","pages":"953-962"},"PeriodicalIF":0.5,"publicationDate":"2001-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"65956310","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"ESR STUDY OF SOME COPPER(II)-1,4-DIHYDRAZINOPHTHALAZINE COMPOUNDS","authors":"L. David, O. Cozar, V. Chiș, S. Filip","doi":"10.1007/978-94-011-5622-6_286","DOIUrl":"https://doi.org/10.1007/978-94-011-5622-6_286","url":null,"abstract":"","PeriodicalId":21323,"journal":{"name":"Revue Roumaine De Chimie","volume":"42 1","pages":"629-630"},"PeriodicalIF":0.5,"publicationDate":"1997-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"51716164","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Effect of no. no and C1 on the corrosion behaviour of (lead - tin) alloy in acid medium","authors":"G. K. Gomma","doi":"10.1501/Commub_0000000415","DOIUrl":"https://doi.org/10.1501/Commub_0000000415","url":null,"abstract":"","PeriodicalId":21323,"journal":{"name":"Revue Roumaine De Chimie","volume":"1 1","pages":"073-082"},"PeriodicalIF":0.5,"publicationDate":"1994-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"66745114","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}