{"title":"Optimization of Soxhlet Extraction of Candlenut Oil (Aleurites moluccana (L.) willd) Using Factorial Experimental Design Level 23","authors":"Salsabila Fachrina, R. W. Broto","doi":"10.14710/jvsar.v5i1.17143","DOIUrl":"https://doi.org/10.14710/jvsar.v5i1.17143","url":null,"abstract":"Candlenut (Aleurites moluccana (L.) wild) is a plant of the Euphorbiceae family. Candlenut oil is obtained by extracting the oil content in candlenut seeds. Soxhlation is an effective method for solvent extraction, ensuring continuous contact between the solvent and the material to extract the oil efficiently while maintaining the purity of the solvent. In this study, optimization of candlenut oil extraction was carried out using the factorial experimental design level 23. Using this method, it can be determined that the extraction time is the most influential variable in the candlenut oil extraction process. The results showed that the optimum operating conditions were an extraction time of 185 min, a candlenut seed powder size of 20 mesh, and a ratio of material-solvent ratio of 1:6 g/g, resulting in an oil yield of 43.2%. The analysis of candlenut oil conducted at an extraction time of 185 min revealed the following results: a refractive index value of 1.4736, a moisture content of 0.08% bb/b, which complies with the standard SNI 01-4462-1998 for candlenut oil, a viscosity of 15.47 Cp, and a density of 0.869 g/mL. The analysis of the free fatty acid number of 2.4%bb/b and saponification number of 181.55 mg KOH/g is not consistent with SNI 01-4462-1998 candlenut oil.","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"3 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-06-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125426945","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"The Effect of Moisture Content on Reducing the Free Fatty Acid Content of Nyamplung Seed Oil (Callophylum inophyllum) Using Factorial Design Method","authors":"Faizal Pambayun, R.TD, W. Broto","doi":"10.14710/jvsar.v5i1.17619","DOIUrl":"https://doi.org/10.14710/jvsar.v5i1.17619","url":null,"abstract":"Nyamplung seeds (Calophyllum inophyllum) have an oil content of 50–70%, in Indonesia nyamplung seeds have a high productivity of 20 t/ha. The process of extracting nyamplung seed oil chemical process produces a higher yield than mechanical. Extraction was collected using the soxhletation extraction method because the oil can be extracted perfectly and requires little solvent. The FFA content is very high, ranging from 15-30% which causes high oil quality to decrease. The high FFA content is due to the high % water content (23-25%) in nyamplung seeds, which causes a hydrolysis process where triglycerides dissociate in the presence of water, glycerol and FFA. The research variables are the moisture content of nyamplung seeds (8% and 12%), the size of the material (15 and 25 mesh), and the ratio of the material to the solvent (1:4 and 1:6) using the factorial design method for research optimization using variable moisture content Nyamplung seed is 8%, size is 20 mesh, and raw material to solvent ratio is 1:5. Novelty value research is effect of % water content on reduction of free fatty acid(FFA) levels contained nyamplung seed oil. Whereas in previous research Adenuga et al., (2021) % water content was not the main parameter for reducing free fatty acid levels. But the main parameters are only drying temperature and oven temperature. FFA content without reducing the % water content of 24 mg KOH/g Jahirul et al. (2015) and 29.2 mg KOH/g Hasibuan et al. (2013) whereas the results of the study showed an FFA level of 13.30%, which means that there was a decrease in FFA levels directly proportional to the decrease in the moisture content of nyamplung seeds.","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"10 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-06-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130581090","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Optimization of Soxhlet Extraction Papaya Seed Oil (Carica papaya L.) with Petroleum Ether","authors":"Riski Andriana, R.TD, W. Broto","doi":"10.14710/jvsar.v5i1.17338","DOIUrl":"https://doi.org/10.14710/jvsar.v5i1.17338","url":null,"abstract":"Papaya seed oil is a high source of fatty acids, especially oleic acid, and palmitic acid. It has 71.60% oleic acid, 15.13% palmitic acid, and has a low cholesterol content so it can be useful as a food oil. This study aims to determine the effect of the ratio of ingredients, time, and particle size on the maximum extraction of papaya seed oil. Extraction of papaya seed oil was carried out by the soxhletation extraction method using petroleum ether solvent. The factorial experimental design of 23 was used to determine the significant parameters for the resulting papaya seed oil: yield, density, fatty acid content, viscosity, and water content. The most influential process variable is particle size. The most optimal papaya seed oil extraction results were obtained at a particle size of 20 mesh, an extraction time of 180 minutes, and a ratio of ingredients to the dissolution of 1:9 (35 gram500 mL). That value obtains a yield of 57.029%.","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"34 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-06-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130605905","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Optimization of Papaya Seed Oil Production Process (Carica papaya L.) with Soxhlation Extraction Method using Factorial Design","authors":"Salsabila Salsabila, R. W. Wisnu Broto","doi":"10.14710/jvsar.v5i1.17308","DOIUrl":"https://doi.org/10.14710/jvsar.v5i1.17308","url":null,"abstract":"This study aims to optimize the extraction of papaya seed oil (Carica papaya L.) using a factorial design level 2. Papaya seeds are a significant component of the fruit, comprising approximately 14.3% of the total fruit weight. These seeds contain about 25% vegetable oil, predominantly composed of unsaturated fatty acids, which have the potential to be processed into consumable oil. The extraction method employed is Soxhlet extraction using a non-polar solvent, n-hexane. A factorial design level 23 was utilized to determine the most influential process variables. The variables were considered to the ratio of papaya seed mass to solvent volume (1:7 and 1:11), particle size (10 and 30 mesh), and extraction time (170 and 190 min). Optimization was conducted using the quicker method calculation, where the determination of the largest effect and the largest main effect played a crucial role. The analysis revealed that the ratio of papaya seed mass to solvent volume had the most significant main effect, with an effect value of 0.1217. From the analysis, it was found that the 1:7 ratio produced the lowest level of Free Fatty Acids (FFA) in the oil, at 0.5076%, which aligns with the Indonesian National Standard (SNI) requirement of 0.36-0.82% FFA content. Furthermore, an analysis of density, viscosity, and moisture content was conducted on the 1:7 ratio. The test results showed that the 1:7 ratio resulted in an oil density of 0.924 g/mL, moisture content of 0.07127%, and FFA content of 0.5076%. However, based on theoretical knowledge, an increase in FFA content leads to a decrease in oil quality. Additionally, higher ratios corresponded to increased moisture content and density. In conclusion, the papaya seed oil produced in this study complies with the Indonesian National Standard (SNI, 01-3555-1998) regarding FFA content (0.36-0.82%), moisture content (maximum 0.15%), and density (0.924-0.929 g/mL).","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"44 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-06-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"122499486","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Optimization Extraction of Sunflower Seed Oil (Helianthus Annus) Using Factorial Design Experiment with Soxhlation Method","authors":"Shabrina Shabrina, R. W. Wisnu Broto","doi":"10.14710/jvsar.v5i1.17105","DOIUrl":"https://doi.org/10.14710/jvsar.v5i1.17105","url":null,"abstract":"Sunflower seed oil is one type of vegetable oil whose growth is still in its early stages in Indonesia. Due to a shortage of domestic availability, several edible oil enterprises in Indonesia still need to import a significant amount of sunflower seed oil. Rukmana (2004) states that the content of sunflower oil's content ranges from 23 to 45%. 11.7% oleic acid and 44-72% linoleic acid are both present in sunflower oil. The goal of this study was to identify the best process factors in light of the obtained oil yield. This study's used Fractional Design Experiment 23 with Quicker Method analysis. The results showed that the optimal operating conditions were an extraction time of 185 min, temperature of 60 ℃, and material-solvent ratio of (R) of 1:6, yielding an oil of 51.6%.","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"197 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-06-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"122829175","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
S. Sumardiono, Arsy Novitasari, Fiky Zakiyatul Awaliyah, Wahyudita Meganingtyas
{"title":"The Effect of Composite Flour Ratio (Cassava, Gembili, Koro Pedang, and Corn) and Extrusion Temperature on Analog Rice Production","authors":"S. Sumardiono, Arsy Novitasari, Fiky Zakiyatul Awaliyah, Wahyudita Meganingtyas","doi":"10.14710/jvsar.v5i1.17610","DOIUrl":"https://doi.org/10.14710/jvsar.v5i1.17610","url":null,"abstract":"The growing population affects an increasing number of Indonesian people, influencing their rice consumption and encouraging Indonesia to import rice. One of the alternatives is to use raw materials such as potential non-rice tubers. In this study, raw material composite flour was made from cassava (Manihot esculenta), gembili (Dioscorea esculenta), koro pedang (Canavalia ensiformis), and corn (Zea mays), which is the basic ingredient of rice maker analog. This research aimed to examine the influence of the raw material composition on the value of nutrients, the physical-chemical properties of analog rice compared to a rice paddy, and the best temperature of analog rice using organoleptic tests. The process of producing analog rice consists of several stages of research, including the manufacturing of composite flour, the cooking of dough with composite flour, the production of analog rice, and the drying of analog rice. Based on the results, samples of 5 (60% cassava flour, 5% gembili flour, 10% koro pedang, and 25% corn flour) as an analog of rice with the best formulations in various compositions. Based on a proximate analysis of the effect of temperature, a temperature of 75 °C is the optimum temperature for the extrusion process. The results of the physical analysis of the best analog rice in this study have a density of 0.46 g/mL, water absorption of 60.52%, and a cooking time is 46 minutes. The analog rice has the same texture, aroma, and appearance as rice in general, although the rice from the analog composite flour tends to have a savory flavor arising from koro pedang. According to the results of this study, the analog rice could be used as a substitute to lessen dependence on paddy rice.","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"44 3 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2023-05-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"132971802","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Implementation of Ambon Banana Peel (Musa Paradisiaca) as Foaming Agent of Banana Fruitghurt using Foam Mat Drying Method","authors":"Cindyana Putry, V. Paramita, I. Hartati","doi":"10.14710/jvsar.v4i2.15821","DOIUrl":"https://doi.org/10.14710/jvsar.v4i2.15821","url":null,"abstract":"Fruitghurt is a product of lactic acid fermentation, namely L. bulgaricus and S. Thermopillus in an acidic state enriched by nutrients from fruit such as Ambon banana but has a short shelf life. Bananas have a role as an additional nutrient in the form of glucose which then becomes a nutrient for lactic acid bacteria. Foam mat drying itself is a drying method that is better than other types of drying because it does not require large production costs and protects the structure of the material through the formation of foam. Application of foam mat drying on fruitghurt using Ambon banana peel extract as a foaming agent is expected to increase the shelf life of fruitghurt as well as an alternative foaming agent derived from vegetable protein Ambon banana peel contains a protein content of about 0.64% when bananas experience a good level of maturity. In the manufacture of fruitghurt powder, the research method used is Response Surface Methodology (RSM) with variables changing the concentration of banana peel extract as a foaming agent, the concentration of maltodextrin as a binder and mixing time. The resulting fruitghurt powder will be analyzed for water content, total acid analysis and pH analysis. The research data were processed using minitab 19 software. The best fruitghurt powder results were found in the 9th variable, namely the minimase variable, where the optimum conditions were banana peel extract concentration of 2.38 ml, maltodextrin concentration of 30 grams and stirring time of 20 minutes. Fruitghurt variable 9 has a pH of 5 after drying which is in accordance with SNI 01-2981-2009, water content is 0.64% and total acid is 1.08%","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"1 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-12-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129462228","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Ria Tasmalia, Nida Hamidah Prameswari, V. Paramita
{"title":"Optimization of Biosorbent on Cd(II) Metal Biosorption Using Duck Eggshell Waste","authors":"Ria Tasmalia, Nida Hamidah Prameswari, V. Paramita","doi":"10.14710/jvsar.v4i2.14749","DOIUrl":"https://doi.org/10.14710/jvsar.v4i2.14749","url":null,"abstract":"Every year the production of duck eggs in Indonesia has increased, this case leads to an increase in the waste of duck eggshells. Duck eggshell waste has components that can be utilized into a biosorbent. To improve the quality of the biosorbent, can be done with an activation method and immobilization method. The purpose of this study was to determine the effectiveness of biosorbents made from duck eggshell waste in absorbing Cd(II) metal. In this study, duck eggshells were activated with physical activation by heating in a furnace at a temperature of 900oC for 2 hours. Independent variables of this study are biosorbent mass, contact time and concentration of cadmium solution. Critical values for Cd levels optimization conditions are accomplished when the biosorbent mass 1.45 grams, contact time 100 minutes and Cd solution concentration 86 ppm with a percentage decrease in Cd levels in the amount of 89%.","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"32 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-12-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"124154521","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Optimization of Liquid Soap Preparation Formula with the Addition of Black Rice (Oryza Sativa L. Indica) Extract as Anti-Radical Free based Virgin Coconut Oil (VCO)","authors":"R. A. S. Imamsyah, V. Paramita","doi":"10.14710/jvsar.v4i2.14697","DOIUrl":"https://doi.org/10.14710/jvsar.v4i2.14697","url":null,"abstract":"An imbalance in the body's number of antioxidants and free radicals can cause oxidative stress and trigger various degenerative diseases (WHO, 2016). One way to prevent free radicals from entering the body is to bathe with soap. Black rice extract can be an antioxidant in soap because it contains anthocyanin pigments and has high bioactive compounds (Chakuton et al., 2012). Selection of Virgin Coconut Oil (VCO) as a raw material for soap because it has a high lauric acid content and is helpful for moisturizing and smoothing the skin (Afrozi et al., 2021). This study aimed to analyze the quality of liquid soap from the hydrolyzed Virgin Coconut Oil (VCO) and the effect of using bases KOH, NH4OH, and black rice extract accompanied by varying base concentrations, time, and temperature treatments. The independent variables for process optimization were the concentration of KOH: NH4OH (30:70, 50:50, 70:30)%, stirring time (65, 85, 105) minutes, and operating temperature (60, 75, 90) °C. Based on the results obtained, the optimum level of FFA (resulting in a small FFA%) was obtained with the minimized variable conditions, namely using a concentration of 16,4% KOH, and an operating temperature of 49,7 °C, a stirring time of 51.4 minutes, and composite desirability of 0,895897.","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"70 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-12-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"124847690","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
{"title":"Effect of Hydrophilic- Lipophilic Balance (HLB) Value on the Stability of Cosmetic Lotion Based on Walnut Oil (Canarium Indicium L.) Oil-in-Water Emulsion","authors":"Alza Izmuliana Eka Putri, H. D. Ariyanto","doi":"10.14710/jvsar.v4i2.15376","DOIUrl":"https://doi.org/10.14710/jvsar.v4i2.15376","url":null,"abstract":"Walnut oil is high source of fatty acid especially oleic acid compare to coconut oil. It has about 40-70% of oleic acid and suitable as moisturizing agent, anti-inflammatory and which contains antioxidants that are good for skin health as a primary ingredient for lotion. This study aims to determine the effect hydrophilic-lipophilic balance (HLB) on the stability of emulsion as a lotion material. The oil-in-water emulsion was formed by emulsification process using Ultra Turrax homogenizer (8000 and 32000 rpm) with addition of tween 80 and span 80 as emulsifiers. Completed randomized design and analysis of variance were used to determine the significant parameters on the stability of emulsion: homogeneity, creaming index, viscosity, density and morphology. Emulsion with the highest stability is sample 8 which is formed at 14.5 HLB value and 32000 rpm homogenizer speed during 5 min. It has complied with SNI-16-4399-1996.","PeriodicalId":170738,"journal":{"name":"Journal of Vocational Studies on Applied Research","volume":"17 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-12-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128121301","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}