Journal of Magnetic Resonance, Series B最新文献

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Multinuclear MR Frequency Shifts of Hydrated Ions as a Function of Applied Pressure and Temperature 水合离子的多核磁共振频移作为施加压力和温度的函数
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0131
Subhendra N. Sarkar , Harold W. Dodgen , John P. Hunt
{"title":"Multinuclear MR Frequency Shifts of Hydrated Ions as a Function of Applied Pressure and Temperature","authors":"Subhendra N. Sarkar , Harold W. Dodgen , John P. Hunt","doi":"10.1006/jmrb.1996.0131","DOIUrl":"10.1006/jmrb.1996.0131","url":null,"abstract":"","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 197-199"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0131","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781164","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
An Optimized 3D NOESY–HSQC 优化的3D噪声- hsqc
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0132
Sekhar Talluri, Gerhard Wagner
{"title":"An Optimized 3D NOESY–HSQC","authors":"Sekhar Talluri, Gerhard Wagner","doi":"10.1006/jmrb.1996.0132","DOIUrl":"10.1006/jmrb.1996.0132","url":null,"abstract":"","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 200-205"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0132","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781165","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 145
Use of Amplitude and Frequency Transformations to Generate Adiabatic Pulses of Wide Bandwidth and Low RF Power Deposition 利用振幅和频率变换产生宽带宽和低射频功率的绝热脉冲沉积
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0123
Jun Shen
{"title":"Use of Amplitude and Frequency Transformations to Generate Adiabatic Pulses of Wide Bandwidth and Low RF Power Deposition","authors":"Jun Shen","doi":"10.1006/jmrb.1996.0123","DOIUrl":"10.1006/jmrb.1996.0123","url":null,"abstract":"<div><p>An amplitude transformation of adiabatic pulses stated previously [Baum<em>et al., Phys. Rev. A</em>32, 3435–3447 (1985)] is generalized using the Bloch equations. Both amplitude and frequency transformations are used to create new adiabatic pulses of wide bandwidth and low RF power deposition. Several adiabatic pulses (including the tanh/tan pulse used for construction of BIR-4, SSAP, and BISEP pulses) are transformed into new pulses. These new pulses are demonstrated numerically and experimentally to operate at a significantly lower RF power level while maintaining the same performance or over a wider bandwidth while using the same RF power. They are expected to be useful for<em>in vivo</em>NMR experiments, especially for applications involving wide frequency dispersion and pulse sequences composed of many adiabatic half-passage pulses.</p></div>","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 131-140"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0123","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781156","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 17
The Manipulation of Water Relaxation and Water Suppression in Biological Systems Using the Water-PRESS Pulse Sequence 利用水压脉冲序列操纵生物系统中的水松弛和水抑制
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0129
William S. Price , Yoji Arata
{"title":"The Manipulation of Water Relaxation and Water Suppression in Biological Systems Using the Water-PRESS Pulse Sequence","authors":"William S. Price ,&nbsp;Yoji Arata","doi":"10.1006/jmrb.1996.0129","DOIUrl":"10.1006/jmrb.1996.0129","url":null,"abstract":"","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 190-192"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0129","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781162","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 17
New Double-Quantum Filtering Schemes 新的双量子滤波方案
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0119
K.J. Jung , J.S. Tauskela , J. Katz
{"title":"New Double-Quantum Filtering Schemes","authors":"K.J. Jung ,&nbsp;J.S. Tauskela ,&nbsp;J. Katz","doi":"10.1006/jmrb.1996.0119","DOIUrl":"10.1006/jmrb.1996.0119","url":null,"abstract":"<div><p>New double-quantum filtering (DQF) schemes are theoretically developed by reformulating the equations describing the double-quantum (DQ) signal. The equations describing the second- and third-rank DQ signals are simplified by restricting the RF phases as required for DQF. The equations are then factorized into two terms representing the separate contribution to the DQ signal from the RF pulses involved in the preparation and evolution times. This allows analysis of the DQ signal of a particular DQF scheme separately for each of these times in a concise manner. By use of the reformulated equations, the conventional DQF scheme is shown to be only one of four possible DQF schemes. The three new DQF schemes offer some desirable properties over the conventional DQF scheme. In the conventional DQF scheme, the third-rank DQ signal declines rapidly to null as the flip angles of the creation and readout RF pulses deviate from 90° to 54.7° or 125.3°. In addition, the second- and third-rank DQ signals in the conventional DQF scheme are opposite in their polarities, resulting in attenuation of the total DQ signal due to destructive interference between them. In one of three new DQF schemes, the DQ signal does not vanish at 54.7° and 125.3°, but varies smoothly with the same functional dependence on the RF flip angles as the second-rank DQ and triple-quantum signals. Furthermore, in two of the three new DQF schemes, the second- and third-rank DQ signals have the same polarity so that the total DQ signal may be enhanced through constructive interference between them. These features of new DQF schemes have been confirmed experimentally.</p></div>","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 103-110"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0119","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781206","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Detection of Different Water Populations in Brain Tissue Using2H Single- and Double-Quantum-Filtered Diffusion NMR Spectroscopy 利用2h单和双量子过滤扩散核磁共振光谱检测脑组织中不同的水群
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0125
Yaniv Assaf, Yoram Cohen
{"title":"Detection of Different Water Populations in Brain Tissue Using2H Single- and Double-Quantum-Filtered Diffusion NMR Spectroscopy","authors":"Yaniv Assaf,&nbsp;Yoram Cohen","doi":"10.1006/jmrb.1996.0125","DOIUrl":"10.1006/jmrb.1996.0125","url":null,"abstract":"<div><p>This paper presents the first simultaneous<sup>2</sup>H single- and double-quantum (SQ and DQ, respectively) diffusion study of excised brain tissue. The apparent diffusion coefficients (ADCs) of the<sup>2</sup>H SQ and DQ signals were measured at a fixed diffusion time (Δ − δ/3 = 21.3 ms) and as a function of the diffusion time to assess restricted diffusion [(Δ − δ/3) was changed from 21.3 to 271.3 ms]. As expected, the ADC of the SQ signal was higher than that of the DQ signal [0.53 ± 0.03 × 10<sup>−5</sup>(<em>n</em>= 3) and 0.30 ± 0.03 × 10<sup>−5</sup>cm<sup>2</sup>s<sup>−1</sup>(<em>n</em>= 4), respectively]. When the ADCs of the SQ and DQ signals were measured as a function of the diffusion time, two components, a fast and a slow component, were observed in each case. The ADCs for the SQ signal were 1.16 ± 0.2 × 10<sup>−5</sup>and 0.35 ± 0.06 × 10<sup>−5</sup>cm<sup>2</sup>s<sup>−1</sup>(<em>n</em>= 3) for the fast and the slow components, respectively. The ADCs for the DQ signal were 0.31 ± 0.05 × 10<sup>−5</sup>and ∼0.03 ± 0.03 × 10<sup>−5</sup>cm<sup>2</sup>s<sup>−1</sup>(<em>n</em>= 2) with the slow component being relatively small. Interestingly, the slow-diffusion component of the SQ signal was found to have an ADC similar to that of the fast component of the DQ signal. These results suggest that brain water can be divided into at least three water populations and that the DQ signal originates from water molecules which interact with slow-diffusing structural components of the brain. The new insights that one can obtain using simultaneous SQ and DQ diffusion measurement and the ability to distinguish among water populations in biological tissues using the above approach are discussed.</p></div>","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 151-159"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0125","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781158","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 34
Directed TOCSY, a Method for Selection of Directed Correlations by Optimal Combinations of Isotropic and Longitudinal Mixing 有向TOCSY:一种选择各向同性和纵向混合最优组合的有向相关性的方法
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0126
S.J. Glaser, H. Schwalbe, J.P. Marino, C. Griesinger
{"title":"Directed TOCSY, a Method for Selection of Directed Correlations by Optimal Combinations of Isotropic and Longitudinal Mixing","authors":"S.J. Glaser,&nbsp;H. Schwalbe,&nbsp;J.P. Marino,&nbsp;C. Griesinger","doi":"10.1006/jmrb.1996.0126","DOIUrl":"10.1006/jmrb.1996.0126","url":null,"abstract":"<div><p>The directed TOCSY pulse sequence element transfers coherence predominantly into “forward-directed” antiphase coherences while simultaneously suppressing in-phase and “backward-directed” antiphase coherences. This novel selection principle, based on the “direction” of the target coherences, provides a new approach for the simplification of crowded spectra. In this article, the theory of directed TOCSY is presented for linear spin systems that are frequently found in carbon-labeled biomolecules.</p></div>","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 160-180"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0126","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781159","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 22
Estimation of Signal Intensities in 2D NMR Spectra with Severe Baseline Distortion by Combined Linear-Prediction and Least-Squares Analyses 结合线性预测和最小二乘分析估计具有严重基线失真的二维核磁共振光谱信号强度
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0130
Søren M. Kristensen , Morten Dahl Sørensen, Henrik Gesmar, Jens J. Led
{"title":"Estimation of Signal Intensities in 2D NMR Spectra with Severe Baseline Distortion by Combined Linear-Prediction and Least-Squares Analyses","authors":"Søren M. Kristensen ,&nbsp;Morten Dahl Sørensen,&nbsp;Henrik Gesmar,&nbsp;Jens J. Led","doi":"10.1006/jmrb.1996.0130","DOIUrl":"10.1006/jmrb.1996.0130","url":null,"abstract":"","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 193-196"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0130","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781163","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
SRS-FT, a Fourier Imaging Method Based on Sparse Radial Scanning and Bayesian Estimation SRS-FT是一种基于稀疏径向扫描和贝叶斯估计的傅里叶成像方法
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0121
D. Graveron-Demilly , G.J. Marseille , Y. Crémillieux , S. Cavassila , D. van Ormond
{"title":"SRS-FT, a Fourier Imaging Method Based on Sparse Radial Scanning and Bayesian Estimation","authors":"D. Graveron-Demilly ,&nbsp;G.J. Marseille ,&nbsp;Y. Crémillieux ,&nbsp;S. Cavassila ,&nbsp;D. van Ormond","doi":"10.1006/jmrb.1996.0121","DOIUrl":"10.1006/jmrb.1996.0121","url":null,"abstract":"<div><p>A new 3D Fourier imaging method based on sparse radial scanning (SRS-FT) of<em>k</em>space is proposed. It allows acquisition of FIDs and is therefore well suited to imaging objects with very short<em>T</em><sub>2</sub>. Use of a Bayesian procedure allows (1) an important reduction of scan time to below that of the projection-reconstruction (PR) method by reducing the number of “Cartesian radial” encoding directions, and (2) a good image quality by estimating missing and corrupted Cartesian samples. SRS-FT images reconstructed from FIDs are compared to conventional FT and PR images.</p></div>","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 119-123"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0121","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781208","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
Proton Exchange Rates Measured by Saturation Transfer Using Delayed Randomization of the Solvent Magnetization 利用溶剂磁化延迟随机化的饱和转移测量质子交换率
Journal of Magnetic Resonance, Series B Pub Date : 1996-08-01 DOI: 10.1006/jmrb.1996.0127
Mikael Leijon
{"title":"Proton Exchange Rates Measured by Saturation Transfer Using Delayed Randomization of the Solvent Magnetization","authors":"Mikael Leijon","doi":"10.1006/jmrb.1996.0127","DOIUrl":"10.1006/jmrb.1996.0127","url":null,"abstract":"<div><p>The spin-lock saturation transfer experiment introduced by B. Adams and L. Lerner (<em>J. Magn. Reson.</em>96, 604–607, 1992) is analyzed in terms of the Bloch equations. It is shown that the<em>T</em><sub>1ρ</sub>relaxation of the solvent is introduced in the decay of the exchangeable protons under conditions of relatively rapid exchange. An alternative experiment is suggested that randomizes the solvent magnetization with a pulsed field gradient before the observe pulse. This gives a single exponential intensity decay for the exchanging protons at all exchange rates. In addition, efficient water suppression and an even excitation profile are obtained.</p></div>","PeriodicalId":16130,"journal":{"name":"Journal of Magnetic Resonance, Series B","volume":"112 2","pages":"Pages 181-185"},"PeriodicalIF":0.0,"publicationDate":"1996-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1006/jmrb.1996.0127","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"19781160","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
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