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International Journal of Nanomanufacturing最新文献

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Synthesis and characterisation of rutin-calcium 芦丁钙的合成与表征
International Journal of Nanomanufacturing Pub Date : 2018-07-27 DOI: 10.1504/IJNM.2018.10014647
Yansong Jiang, Qiuwei Liu, G. Zhai
{"title":"Synthesis and characterisation of rutin-calcium","authors":"Yansong Jiang, Qiuwei Liu, G. Zhai","doi":"10.1504/IJNM.2018.10014647","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10014647","url":null,"abstract":"Rutin and calcium acetate at 86°C, pH = 8.5, reflux 6h, A rutin-ca complex was synthesised in methanol. UV-Vis spectroscopy: band I shifted from 355 nm to 359 nm, red shifted to 4 nm. Band II moved from 257 nm to 266 nm and shifted red by 9 nm. IR: the absorption peak of ruthenium is broadened, υC = O 1,632.45 cm–1, red shift of 23 cm–1, the characteristic absorption peak of benzene ring has not changed, and the absorption peak of 618.43 cm–1, metal coordination bond υCa-O stretching vibration peak. 1H-NMR: 3'-OH and 4'-OH hydroxyl groups disappear, showing coordination with calcium ions. Thermal analysis showed rutin with ane calcium ion complex.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"207"},"PeriodicalIF":0.0,"publicationDate":"2018-07-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41928049","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synthesis and characterisation of amine-grafted graphene oxide-TiO2 crystal/plate composite and its crystal growth 胺接枝氧化石墨烯-TiO2晶体/板复合材料的合成、表征及其晶体生长
International Journal of Nanomanufacturing Pub Date : 2018-07-27 DOI: 10.1504/IJNM.2018.10012502
Cun Chen, J. Chen, Jing Gao, Guohua Li
{"title":"Synthesis and characterisation of amine-grafted graphene oxide-TiO2 crystal/plate composite and its crystal growth","authors":"Cun Chen, J. Chen, Jing Gao, Guohua Li","doi":"10.1504/IJNM.2018.10012502","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10012502","url":null,"abstract":"Owning to their extensive practical application, the controllable synthesis of well-faceted TiO2 crystal with high percentage of reactive facets has attracted increasing attention. When adjusting the concentration of HF at 120 mM and 240 mM, anatase TiO2 crystal and plate with exposed {001} facets had been fabricated on the amine-grafted graphene oxide (AGO) via a facile hydrothermal method. The influence of experiment conditions on the morphology of the final products was investigated in detail. The results showed that the morphology of TiO2 crystal on AGO transforms cube-like structure into truncated tetragonal bipyramid structure when extending the reaction time, and the size of TiO2 crystal were affected by the molar ratio of F/Ti. In addition, the dispersion of TiO2 plate were improved by amino or oxygen-containing group on AGO sheet.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"268"},"PeriodicalIF":0.0,"publicationDate":"2018-07-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48839117","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Preparation of tungsten trioxide film with mesoporosity by anodisation 阳极氧化法制备介孔型三氧化钨薄膜
International Journal of Nanomanufacturing Pub Date : 2018-07-27 DOI: 10.1504/IJNM.2018.10014651
Shizhao Wu, Yuru Li, Jing Gao, Guohua Li, Xiaojuan Wang
{"title":"Preparation of tungsten trioxide film with mesoporosity by anodisation","authors":"Shizhao Wu, Yuru Li, Jing Gao, Guohua Li, Xiaojuan Wang","doi":"10.1504/IJNM.2018.10014651","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10014651","url":null,"abstract":"The mesostructured WO3 film on tungsten was investigated by anodic oxidation in ethylene glycol electrolytes containing low concentrations of ionic liquids (EMim.BF4, 0.6-1.6 vol. %). The surface structure of the WO3 film as prepared can be adjusted by changing the time, potential and temperature of anodisation, and the concentration of ILs and water in the electrolyte. The sample was characterised by X-ray diffraction (XRD) and field-emission scanning electron microscope (SEM) respectively. A self-organised mesostructured WO3 can be obtained under optimised parameters. The mesostructured WO3 film is arranged in sections of arrays with an average granular diameter of 30 nm.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"256"},"PeriodicalIF":0.0,"publicationDate":"2018-07-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47097223","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Nonlinear phase error compensation for fringe deflectometry measuring system 条纹偏转测量系统的非线性相位误差补偿
International Journal of Nanomanufacturing Pub Date : 2018-05-09 DOI: 10.1504/IJNM.2018.10012671
Lili Jiang, Xiaodong Zhang, F. Fang
{"title":"Nonlinear phase error compensation for fringe deflectometry measuring system","authors":"Lili Jiang, Xiaodong Zhang, F. Fang","doi":"10.1504/IJNM.2018.10012671","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10012671","url":null,"abstract":"Fringe deflectometry technique (FDT) plays a more and more important role in specular surface measurement due to its large slope measurement range. However, its accuracy is heavily dependent on the quality of the extracted phase. The gamma effect of liquid crystal display (LCD) and CCD introduces significant phase distortion, resulting in a periodical phase error and measurement error. A mathematical model is established to illustrate phase error introduced by gamma effect, and an optimal algorithm based on four-time four-step phase-shifting (FFPS) is proposed to retrieve phase. Simulation results prove that FFPS phase retrieval method can compensate for the phase error caused by the nonlinearity of the LCD and CCD point-by-point, thus it is immune not only to calibration error, but also to the non-unitary of the gamma effect spatially and temporally. Experimental results are also presented to verify the performance of the proposed method.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"115"},"PeriodicalIF":0.0,"publicationDate":"2018-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47035366","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Performance evaluation of coated cemented carbide inserts milling 508III steel 涂层硬质合金刀片铣削508III钢的性能评价
International Journal of Nanomanufacturing Pub Date : 2018-05-09 DOI: 10.1504/IJNM.2018.10012670
Li Liu, Yaonan Cheng, R. Guan, Ming Xu, Tong Wang
{"title":"Performance evaluation of coated cemented carbide inserts milling 508III steel","authors":"Li Liu, Yaonan Cheng, R. Guan, Ming Xu, Tong Wang","doi":"10.1504/IJNM.2018.10012670","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10012670","url":null,"abstract":"A large amount of material is removed during the milling of a water chamber head manufactured of high-strength 508III steel. The performance and service life of coated cemented carbide inserts have significant influences on processing efficiency and the quality of nuclear power components. This study will conduct single-factor milling experiments of water chamber heads relevant to practical working conditions. Influences of different milling parameters on the insert failure behaviour are analysed based on experimental results and simulation data. The failure mechanism of insert wear and fracture was also discussed. Finally, the influences of coating types and thickness values on the wear behaviour of cemented carbide insert while cutting 508III steel were investigated. The results of this research can be implemented in the improvement of coated cemented carbide inserts in regards to failure resistance and service life.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"101"},"PeriodicalIF":0.0,"publicationDate":"2018-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"41505462","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
The effects of chemical components in the bath solution on mechanical properties of the electroplated coating on diamond tools 镀液中化学成分对金刚石工具电镀镀层力学性能的影响
International Journal of Nanomanufacturing Pub Date : 2018-05-09 DOI: 10.1504/IJNM.2018.10012672
Q. Chen, Cui Zhongming, He Qingshan, J. Wang, C. Feng
{"title":"The effects of chemical components in the bath solution on mechanical properties of the electroplated coating on diamond tools","authors":"Q. Chen, Cui Zhongming, He Qingshan, J. Wang, C. Feng","doi":"10.1504/IJNM.2018.10012672","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10012672","url":null,"abstract":"The bath compositions are critical to mechanical performance of the coating layer for electroplated diamond tools. In this paper, the effects of different chemical components in bath solution on mechanical properties including tensile strength and hardness of the electroplated coating were investigated by orthogonal experiments. The influences of different chemical components including nickel sulphate, cobalt sulphate and sodium chloride on mechanical properties of the electroplated coating were analysed. The results showed that increasing the component of nickel sulphate caused an unstable situation on tensile strength and hardness of the electroplated coating. However, hardness of the electroplated coating could be improved by increasing the component of cobalt sulphate. The concentration of sodium chloride had no obvious effect on mechanical properties of the electroplated coating layer. The experimental results revealed that the optimised bath compositions were at 270 g/L nickel sulphate, 20 g/L cobalt sulphate, and 10 g/L sodium chloride.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"131"},"PeriodicalIF":0.0,"publicationDate":"2018-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47688082","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Experimental research on pulse laser assisted micro turning of ZrO2 ceramic 脉冲激光辅助ZrO2陶瓷微车削的实验研究
International Journal of Nanomanufacturing Pub Date : 2018-05-09 DOI: 10.1504/IJNM.2018.10012676
Xiuqing Hao, Hao Yan, Jinjin Han, Chenjiao Yao, N. He
{"title":"Experimental research on pulse laser assisted micro turning of ZrO2 ceramic","authors":"Xiuqing Hao, Hao Yan, Jinjin Han, Chenjiao Yao, N. He","doi":"10.1504/IJNM.2018.10012676","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10012676","url":null,"abstract":"ZrO2 ceramic materials have outstanding propertied, like high wear resistance, good corrosion resistance, low thermal conductivity, etc., and has been widely applied in modern industry. However, ZrO2 ceramic is one of the difficult-to-machine materials, which would lead to rapid tool wear and poor surface quality. Micro turning combined with pulse laser, as a new kind of process in machining ZrO2 ceramic, is studied in this paper. And a comparative research between micro turning with and without pulse laser assisted of ZrO2 ceramic has been conducted. The results revealed that under the same machining parameters, both the cutting force and machined surface roughness obtained in pulse laser assisted micro turning was smaller than that in micro turning without pulse laser, and the pulse laser could effectively reduce the tool wear. The work carried out in this paper would be helpful to the further research on the pulse laser assisted micro machining of ZrO2 ceramic.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"165"},"PeriodicalIF":0.0,"publicationDate":"2018-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"43997437","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Research on energy consumption and energy efficiency of machine tools: a comprehensive survey 机床能耗与能效研究:综合调查
International Journal of Nanomanufacturing Pub Date : 2018-05-09 DOI: 10.1504/IJNM.2018.091579
L. C. Moreira, Weidong Li, M. Fitzpatrick, Xin Lu, Xiaoxia Li
{"title":"Research on energy consumption and energy efficiency of machine tools: a comprehensive survey","authors":"L. C. Moreira, Weidong Li, M. Fitzpatrick, Xin Lu, Xiaoxia Li","doi":"10.1504/IJNM.2018.091579","DOIUrl":"https://doi.org/10.1504/IJNM.2018.091579","url":null,"abstract":"The increasing demand for energy, coupled with concerns over pollution and climate change, has led governments to establish policy frameworks to reduce CO2 emissions. Moreover, rises in energy price and increasingly greener customer behaviour are pushing the manufacturing industries to develop more sustainable processes. As a major source of energy consumption in manufacturing systems, machine tools have been the focus of sustainability research communities worldwide. This paper provides a survey of manufacturing industry's sustainability trends and presents a technology-foresight-based methodology for gathering key information on the research development in this topic. Furthermore, a correlation between real world aspects, such as legal, economic and environmental, and the development of research on energy consumption and efficiency of machine tools is provided. The results highlight the leading countries, institutions, authors and subject areas in this field. Research and development shows a high correlation with governmental actions, and appears to be of core importance to meet CO2 reduction targets.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"140-164"},"PeriodicalIF":0.0,"publicationDate":"2018-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1504/IJNM.2018.091579","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"45424585","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Axicon profile metrology using contact stylus method 使用触针法进行Axicon轮廓测量
International Journal of Nanomanufacturing Pub Date : 2018-05-09 DOI: 10.1504/IJNM.2018.10012674
Huimin Gao, Xiaodong Zhang, F. Fang
{"title":"Axicon profile metrology using contact stylus method","authors":"Huimin Gao, Xiaodong Zhang, F. Fang","doi":"10.1504/IJNM.2018.10012674","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10012674","url":null,"abstract":"Axicon lenses, characterised by their cone shape, have rotational symmetry. The generatrix of axicons is the surface profile going across the apex of the axicon and the cone angle of the axicon can be calculated from the generatrix. Axicons, widely used in optical alignment and Bessel-Gauss beam generation, require high accuracy in surface and cone angle metrology. However, current methods focus on measuring the cone angle with a stylus profiler, a process in which misalignment and displacement are common when measuring the generatrix. A method is proposed that multiple parallel measurement paths near the apex of the axicon will obtain the generatrix with the specific algorithm. In experiments, the axicon with a cone angle of about 90° was measured by the stylus profiler method (Taylor-Hobson PGI 3D) in the 0.5 mm, 0.4 mm and 0.3 mm distances, whose results show good agreement in the cone angle range and generatrix error. Experimental results prove the feasibility of the proposed method.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"177"},"PeriodicalIF":0.0,"publicationDate":"2018-05-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44511817","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Experimental investigation on the abrasive wear of AISI 52100 steel AISI 52100钢磨料磨损试验研究
International Journal of Nanomanufacturing Pub Date : 2018-01-11 DOI: 10.1504/IJNM.2018.10009995
Chen Zhixiang, W. Yao, J. Yuan, Zhongdian Cheng, W. Hang, Tianchen Zhao
{"title":"Experimental investigation on the abrasive wear of AISI 52100 steel","authors":"Chen Zhixiang, W. Yao, J. Yuan, Zhongdian Cheng, W. Hang, Tianchen Zhao","doi":"10.1504/IJNM.2018.10009995","DOIUrl":"https://doi.org/10.1504/IJNM.2018.10009995","url":null,"abstract":"AISI 52100 steel has been widely used in various types of bearings in machinery equipment due to its excellent mechanical properties and high availability. In the final manufacturing process of bearing parts usually involve lapping and polishing methods on the ultra-precision machining in order to achieve high accuracy of profile and fine surface quality. The essence of this process is abrasive wear of AISI 52100 steel material. Therefore, in order to improve the super finishing process of bearings super finishing, the experiment of abrasive wear of AISI 52100 steel materials were carried out in this paper. The effects of different abrasive diameter and pressure on the material removal amount of AISI 52100 steel were investigated; the abrasive correction coefficient K in Preston formula was computed and obtained. The result shows that reducing the abrasive diameter can increase the material removal rate and improve surface quality when other factors are maintained constant.","PeriodicalId":14170,"journal":{"name":"International Journal of Nanomanufacturing","volume":"14 1","pages":"65"},"PeriodicalIF":0.0,"publicationDate":"2018-01-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44147052","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
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