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Crystal structure and magnetic properties of the diuranium tritelluride U2Te3 三碲化二铀U2Te3的晶体结构和磁性能
European Journal of Solid State and Inorganic Chemistry Pub Date : 1998-01-01 DOI: 10.1016/S0992-4361(98)80015-5
O. Tougait, M. Potel, J.C. Levet, H. Noël
{"title":"Crystal structure and magnetic properties of the diuranium tritelluride U2Te3","authors":"O. Tougait,&nbsp;M. Potel,&nbsp;J.C. Levet,&nbsp;H. Noël","doi":"10.1016/S0992-4361(98)80015-5","DOIUrl":"10.1016/S0992-4361(98)80015-5","url":null,"abstract":"<div><p>Single crystals of U<sub>2</sub>Te<sub>3</sub> were obtained by solid state reaction between the elements in stoichiometric proportions mixed with a small quantity of cesium chloride. U<sub>2</sub>Te<sub>3</sub> crystallizes in the orthorhombic system, space group Pnma (n<sup>o</sup> 62), with unit cell parameters a = 12.175(2)Å, b = 4.370(1)Å, c = 11.828(2)Å, and Z = 4. The structure was determined from single crystal X-ray diffraction data and refined to final residual factors R(F) = 0.030 and Rω(F) = 0.035 for 32 variable parameters and a unique data set of 1100 diffraction intensities [I &gt; 3σ(I)]. The U atoms are located on two 4c non equivalent crystallographic positions. U(1) has a 7-fold coordination of Te atoms with a coordination polyhedron deriving from an octahedron in which one apex is split into two positions, and U(2) has a monocapped trigonal prismatic coordination. U<sub>2</sub>Te<sub>3</sub> exhibits rather complex magnetic behaviour, with an onset of ferromagnetic order at T ∼ 110 K and spin reorientation below 105 K.</p></div>","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"35 1","pages":"Pages 67-76"},"PeriodicalIF":0.0,"publicationDate":"1998-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/S0992-4361(98)80015-5","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75327262","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 11
Li20 evaporation during the laser heated pedestal growth of LiTaO3 single-crystal fibers 激光加热LiTaO3单晶光纤支架生长过程中Li20的蒸发
European Journal of Solid State and Inorganic Chemistry Pub Date : 1998-01-01 DOI: 10.1016/S0992-4361(98)80010-6
R. Burlot, M. Ferriol, R. Moncorgé, G. Boulon
{"title":"Li20 evaporation during the laser heated pedestal growth of LiTaO3 single-crystal fibers","authors":"R. Burlot,&nbsp;M. Ferriol,&nbsp;R. Moncorgé,&nbsp;G. Boulon","doi":"10.1016/S0992-4361(98)80010-6","DOIUrl":"10.1016/S0992-4361(98)80010-6","url":null,"abstract":"<div><p>The growth of LiTaO<sub>3</sub> single-crystal fibers by the Laser Heated Pedestal Growth technique was performed using different pulling rates and growth atmosphere pressures. Fibers were produced with a diameter of about 800 μm and lengths between 20 and 50 mm. Due to the high melting point of LiTaO<sub>3</sub>, incongruent evaporation of lithium oxide took place during the growth. Its influence on the morphology of the crystals obtained was characterized by transmission optical microscopy and an estimate of the evaporation time constant of Li<sub>2</sub>O made.</p></div>","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"35 1","pages":"Pages 1-8"},"PeriodicalIF":0.0,"publicationDate":"1998-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.1016/S0992-4361(98)80010-6","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"82810215","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
Electrical Transport Properties of the Misfit Layer Compounds (SnS)1. 20TiS2 and (PbS)1.18TiS2 Misfit层化合物(SnS)的电输运性质20TiS2和(PbS)1.18TiS2
European Journal of Solid State and Inorganic Chemistry Pub Date : 1991-11-12 DOI: 10.1002/CHIN.199145021
G. Wiegers, R. Haange
{"title":"Electrical Transport Properties of the Misfit Layer Compounds (SnS)1. 20TiS2 and (PbS)1.18TiS2","authors":"G. Wiegers, R. Haange","doi":"10.1002/CHIN.199145021","DOIUrl":"https://doi.org/10.1002/CHIN.199145021","url":null,"abstract":"(SnS)1.20TiS2 and (PbS)1.18TiS2 are misfit layer compounds, built of alternate double layers SnS (PbS), actually a slightly distorted {001} slice of rocksalt type SnS (PbS), and sandwiches TiS2, slightly distorted compared to those of 1T-TiS2. The electrical transport properties, measured on single crystals for the in-plane resistivity (rho-ab), the resistivity along c (rho-c) and Hall coefficient (R(H)) and on powder compacts for the Seebeck coefficient (alpha) are metallic like those of 1T-TiS2 intercalated with an electron donating species. The rho-ab versus temperature curves are non-linear from 4 to 300 K. R(H) and alpha are negative for both compounds. The Hall coefficients at 300 K correspond with 0.20 +/- 0.04 e/Ti for (SnS)1.20TiS2 and 0.43 +/- 0.09 e/Ti for (PbS)1.18TiS2. The Seebeck coefficients point to 0.2 - 0.4 e/Ti.","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"58 24 1","pages":"1071-1078"},"PeriodicalIF":0.0,"publicationDate":"1991-11-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86544665","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 23
Barium titanate by the sol-gel process 溶胶-凝胶法制备钛酸钡
European Journal of Solid State and Inorganic Chemistry Pub Date : 1989-12-12 DOI: 10.1002/CHIN.198950336
A. Larbot, F. García, C. Guizard
{"title":"Barium titanate by the sol-gel process","authors":"A. Larbot, F. García, C. Guizard","doi":"10.1002/CHIN.198950336","DOIUrl":"https://doi.org/10.1002/CHIN.198950336","url":null,"abstract":"The Sol-Gel technique is used to prepare powder and densified ceramic of BaTiO 3 . The experimental conditions (precursors, hydrolysis, heat treatment) for the preparation of a powder, suitable for sintering onto a product of high dielectric constant and weak loss tangent, are studied. The characteristics of the ceramic as a fonction of the sintering temperature are also reported","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"50 1","pages":"327-337"},"PeriodicalIF":0.0,"publicationDate":"1989-12-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84204132","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 6
On trigonal weberites: structure refinements of Na2MnC1F7 and Na2MnGaF7 三角网:Na2MnC1F7和na2mnngaf7的结构改进
European Journal of Solid State and Inorganic Chemistry Pub Date : 1989-04-04 DOI: 10.1002/CHIN.198914008
G. Courbion, G. Férey, H. Holler, D. Babel
{"title":"On trigonal weberites: structure refinements of Na2MnC1F7 and Na2MnGaF7","authors":"G. Courbion, G. Férey, H. Holler, D. Babel","doi":"10.1002/CHIN.198914008","DOIUrl":"https://doi.org/10.1002/CHIN.198914008","url":null,"abstract":"","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"14 1","pages":"435-447"},"PeriodicalIF":0.0,"publicationDate":"1989-04-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87803144","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 12
Na2SiF6 and ordered trirutile-types: crystal and magnetic structure of α- and β-LiMnVF6 Na2SiF6和有序三元型:α-和β-LiMnVF6的晶体和磁性结构
European Journal of Solid State and Inorganic Chemistry Pub Date : 1989-03-28 DOI: 10.1002/CHIN.198913004
G. Courbion, C. Jacoboni, P. Wolfers
{"title":"Na2SiF6 and ordered trirutile-types: crystal and magnetic structure of α- and β-LiMnVF6","authors":"G. Courbion, C. Jacoboni, P. Wolfers","doi":"10.1002/CHIN.198913004","DOIUrl":"https://doi.org/10.1002/CHIN.198913004","url":null,"abstract":"","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"27 1","pages":"359-374"},"PeriodicalIF":0.0,"publicationDate":"1989-03-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83443358","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 5
Synthesis and study of sodium hydroxi-cuprate: Na2Cu (OH)4 and copper hydroxide: Cu(OH)2 氢氧化铜钠:Na2Cu (OH)4和氢氧化铜:Cu(OH)2的合成与研究
European Journal of Solid State and Inorganic Chemistry Pub Date : 1989-03-28 DOI: 10.1002/CHIN.198913003
Y. Cudennec, A. Lecerf, A. Riou, Y. Gérault
{"title":"Synthesis and study of sodium hydroxi-cuprate: Na2Cu (OH)4 and copper hydroxide: Cu(OH)2","authors":"Y. Cudennec, A. Lecerf, A. Riou, Y. Gérault","doi":"10.1002/CHIN.198913003","DOIUrl":"https://doi.org/10.1002/CHIN.198913003","url":null,"abstract":"","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"20 1","pages":"351-358"},"PeriodicalIF":0.0,"publicationDate":"1989-03-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"74380718","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
New lanthanide hydrogen phosphites LnH(PO3H)2 2H2O 新型镧系亚磷酸氢盐LnH(PO3H) 2H2O
European Journal of Solid State and Inorganic Chemistry Pub Date : 1989-03-21 DOI: 10.1002/CHIN.198912008
J. Durand, M. Loukili, N. Tijani, M. Rafiq, L. Cot
{"title":"New lanthanide hydrogen phosphites LnH(PO3H)2 2H2O","authors":"J. Durand, M. Loukili, N. Tijani, M. Rafiq, L. Cot","doi":"10.1002/CHIN.198912008","DOIUrl":"https://doi.org/10.1002/CHIN.198912008","url":null,"abstract":"","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"1 1","pages":"297-303"},"PeriodicalIF":0.0,"publicationDate":"1989-03-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80573716","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
The layered compounds AMv(PO4)2 (A=K, Rb, Cs and M=Sb, Nb, Ta) 层状化合物AMv(PO4)2 (A=K, Rb, Cs, M=Sb, Nb, Ta)
European Journal of Solid State and Inorganic Chemistry Pub Date : 1989-03-21 DOI: 10.1002/CHIN.198912005
S. Oyetola, A. Verbaere, Y. Piffard, M. Tournoux
{"title":"The layered compounds AMv(PO4)2 (A=K, Rb, Cs and M=Sb, Nb, Ta)","authors":"S. Oyetola, A. Verbaere, Y. Piffard, M. Tournoux","doi":"10.1002/CHIN.198912005","DOIUrl":"https://doi.org/10.1002/CHIN.198912005","url":null,"abstract":"","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"260 1","pages":"259-278"},"PeriodicalIF":0.0,"publicationDate":"1989-03-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"77675362","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 24
NMR Study of the intermetallic phase Li2Ga7 金属间相Li2Ga7的核磁共振研究
European Journal of Solid State and Inorganic Chemistry Pub Date : 1989-03-21 DOI: 10.1002/CHIN.198912018
M. Tillard-Charbonnel, C. Belin, M. Herzog-Cance
{"title":"NMR Study of the intermetallic phase Li2Ga7","authors":"M. Tillard-Charbonnel, C. Belin, M. Herzog-Cance","doi":"10.1002/CHIN.198912018","DOIUrl":"https://doi.org/10.1002/CHIN.198912018","url":null,"abstract":"","PeriodicalId":100507,"journal":{"name":"European Journal of Solid State and Inorganic Chemistry","volume":"45 1","pages":"329-340"},"PeriodicalIF":0.0,"publicationDate":"1989-03-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83649727","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
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