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Formation for a Quinoline Using a Stable Vinamidinium Salt

有机合成与工艺文献分享 2024-11-16 09:00

文章摘要

本文介绍了Takeda研究小组开发的一种实用合成方法，用于制备3-formylquinoline 12。该方法利用稳定的vinamidinium盐与苯胺衍生物11反应，通过三步化学转化实现：Schiff碱形成、苯胺邻位环化和在喹啉3-位引入醛基。研究小组通过开发新型的2-亚甲基氨基甲基vinamidinium三卤化物作为稳定的非吸湿性盐，成功实现了24.3公斤喹啉12的放大合成。

Formation for a Quinoline Using a Stable Vinamidinium Salt

查看文献： Synthesis of a stable triformylmethane synthon and its scalable application to 7-acylamino-3-formylquinoline syntheses
查看期刊： Tetrahedron

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