Rubiya Rashid , Sajad Mohd Wani , Shaziya Manzoor , F.A. Masoodi , Mohd Masarat Dar
{"title":"超声波辅助天然深共熔溶剂萃取苹果渣中生物活性化合物的绿色提取:优化、比较和生物活性","authors":"Rubiya Rashid , Sajad Mohd Wani , Shaziya Manzoor , F.A. Masoodi , Mohd Masarat Dar","doi":"10.1016/j.foodchem.2022.133871","DOIUrl":null,"url":null,"abstract":"<div><p>Natural deep eutectic solvents (NADES) coupled with ultrasound assisted extraction (UAE) was evaluated as extraction techniques for bioactive compounds from apple pomace. Seven natural deep eutectic solvents (NADES) with different molar ratios were explored as green extraction solvents to evaluate extraction efficiency in terms of total flavonoid content (TFC), total phenolic content (TPC), lipid peroxidation inhibition (LBI) and antioxidant potential. The solvents which performed better than conventional solvent were DES1 (Choline chloride: glycerol (1:2)), DES2 (Choline chloride: lactic acid (1:3)) and DES5 ((Choline chloride: citric acid (1:1)). These solvents were further evaluated for optimisation of processing parameters in UAE-DES. The maximum TPC value was achieved using sonication time 40 min, water 30 %, solid/liquid ratio 1:30, temperature 40 °C, acoustic intensity 83.2 W/cm<strong><sup>2</sup></strong> and duty cycle 75 %. HPLC of optimised extract was utilised for quantification of polyphenol compounds showing quercetin as main compound followed by chlorogenic acid, gallic acid, phloretin, phloridizin and rutin.</p></div>","PeriodicalId":318,"journal":{"name":"Food Chemistry","volume":"398 ","pages":"Article 133871"},"PeriodicalIF":8.5000,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"37","resultStr":"{\"title\":\"Green extraction of bioactive compounds from apple pomace by ultrasound assisted natural deep eutectic solvent extraction: Optimisation, comparison and bioactivity\",\"authors\":\"Rubiya Rashid , Sajad Mohd Wani , Shaziya Manzoor , F.A. Masoodi , Mohd Masarat Dar\",\"doi\":\"10.1016/j.foodchem.2022.133871\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<div><p>Natural deep eutectic solvents (NADES) coupled with ultrasound assisted extraction (UAE) was evaluated as extraction techniques for bioactive compounds from apple pomace. Seven natural deep eutectic solvents (NADES) with different molar ratios were explored as green extraction solvents to evaluate extraction efficiency in terms of total flavonoid content (TFC), total phenolic content (TPC), lipid peroxidation inhibition (LBI) and antioxidant potential. The solvents which performed better than conventional solvent were DES1 (Choline chloride: glycerol (1:2)), DES2 (Choline chloride: lactic acid (1:3)) and DES5 ((Choline chloride: citric acid (1:1)). These solvents were further evaluated for optimisation of processing parameters in UAE-DES. The maximum TPC value was achieved using sonication time 40 min, water 30 %, solid/liquid ratio 1:30, temperature 40 °C, acoustic intensity 83.2 W/cm<strong><sup>2</sup></strong> and duty cycle 75 %. HPLC of optimised extract was utilised for quantification of polyphenol compounds showing quercetin as main compound followed by chlorogenic acid, gallic acid, phloretin, phloridizin and rutin.</p></div>\",\"PeriodicalId\":318,\"journal\":{\"name\":\"Food Chemistry\",\"volume\":\"398 \",\"pages\":\"Article 133871\"},\"PeriodicalIF\":8.5000,\"publicationDate\":\"2023-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"37\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Food Chemistry\",\"FirstCategoryId\":\"97\",\"ListUrlMain\":\"https://www.sciencedirect.com/science/article/pii/S0308814622018337\",\"RegionNum\":1,\"RegionCategory\":\"农林科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q1\",\"JCRName\":\"CHEMISTRY, APPLIED\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Food Chemistry","FirstCategoryId":"97","ListUrlMain":"https://www.sciencedirect.com/science/article/pii/S0308814622018337","RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"CHEMISTRY, APPLIED","Score":null,"Total":0}
Green extraction of bioactive compounds from apple pomace by ultrasound assisted natural deep eutectic solvent extraction: Optimisation, comparison and bioactivity
Natural deep eutectic solvents (NADES) coupled with ultrasound assisted extraction (UAE) was evaluated as extraction techniques for bioactive compounds from apple pomace. Seven natural deep eutectic solvents (NADES) with different molar ratios were explored as green extraction solvents to evaluate extraction efficiency in terms of total flavonoid content (TFC), total phenolic content (TPC), lipid peroxidation inhibition (LBI) and antioxidant potential. The solvents which performed better than conventional solvent were DES1 (Choline chloride: glycerol (1:2)), DES2 (Choline chloride: lactic acid (1:3)) and DES5 ((Choline chloride: citric acid (1:1)). These solvents were further evaluated for optimisation of processing parameters in UAE-DES. The maximum TPC value was achieved using sonication time 40 min, water 30 %, solid/liquid ratio 1:30, temperature 40 °C, acoustic intensity 83.2 W/cm2 and duty cycle 75 %. HPLC of optimised extract was utilised for quantification of polyphenol compounds showing quercetin as main compound followed by chlorogenic acid, gallic acid, phloretin, phloridizin and rutin.
期刊介绍：
Food Chemistry publishes original research papers dealing with the advancement of the chemistry and biochemistry of foods or the analytical methods/ approach used. All papers should focus on the novelty of the research carried out.
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