环形炉集成到DAC室,稳定和均匀的样品加热到2000k。

IF 1.7 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION
Muyun Han, Wenhui Liu, Min Cao, Weichao Li, Dawei Jiang, Yonghao Han, Chunxiao Gao
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引用次数: 0

摘要

金刚石砧细胞是研究材料在极端压力和温度下行为的强大工具,但实现有效和均匀的加热仍然具有挑战性。本研究介绍了一种金属-绝缘体-金属夹层结构的环形炉,采用钽(Ta)加热,钨(W)电极,云母陶瓷粉绝缘,可稳定均匀加热至2000 K。结合热电偶数据和有限元模拟的校准方法确保了精确的温度测量。实验验证表明,该炉保持了光谱测量的光学通道,并支持高压和高温条件下的原位电导率表征。这一进展为极端条件下的多物理场实验提供了一个强大的平台。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Ring type furnace integrated into DAC chamber for stable and uniform sample heating up to 2000 K.

The diamond anvil cell is a powerful tool for investigating material behavior under extreme pressure and temperature, but achieving efficient and uniform heating remains challenging. This study introduces a ring-type furnace integrated into a gasket with a metal-insulator-metal sandwich structure, using tantalum (Ta) for heating, tungsten (W) for electrodes, and mica-ceramic powder for insulation, enabling stable and uniform heating up to 2000 K. A calibration method combining thermocouple data and finite element simulations ensures accurate temperature measurement. Experimental validation shows that the furnace maintains optical access for spectroscopic measurements and supports in situ conductivity characterization under high-pressure and high-temperature conditions. This advancement provides a robust platform for multi-physics experiments under extreme conditions.

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来源期刊
Review of Scientific Instruments
Review of Scientific Instruments 工程技术-物理:应用
CiteScore
3.00
自引率
12.50%
发文量
758
审稿时长
2.6 months
期刊介绍: Review of Scientific Instruments, is committed to the publication of advances in scientific instruments, apparatuses, and techniques. RSI seeks to meet the needs of engineers and scientists in physics, chemistry, and the life sciences.
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