Evaluation of depth of dislocation visibility in SEM electron channeling contrast imaging in Ti-6Al-4V alloy using serial sectioning method

IF 1.8 4区 工程技术
Microscopy Pub Date : 2021-06-01 DOI:10.1093/jmicro/dfaa060
Shigeto Yamasaki;Misaki Deguchi;Masatoshi Mitsuhara;Hideharu Nakashima;Yutaro Ota;Keiji Kubushiro
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引用次数: 0

Abstract

In this study, we conducted a quantitative evaluation of dislocation density by scanning electron microscopy electron channeling contrast imaging for α grains of a Ti-6Al-4V alloy deformed at room temperature. The depth of visibility of dislocations is experimentally measured as 140 to 160 nm by a serial sectioning observation. This result is compared with the theoretical value and applied to evaluate dislocation density. These factors confirm that the theoretically calculated value of the depth of visibility, at 5 to 6 times the extinction distance, is valid for the hexagonal close-packed Ti alloy.
用连续切片法评价Ti-6Al-4V合金SEM电子沟道对比成像中位错可见度的深度
在本研究中,我们通过扫描电子显微镜电子沟道对比成像对室温下变形的Ti-6Al-4V合金的α晶粒的位错密度进行了定量评估。位错的可见深度通过连续切片观察实验测量为140至160nm。将该结果与理论值进行了比较,并应用于位错密度的评价。这些因素证实,在消光距离的5到6倍处,可视深度的理论计算值对于六方紧密堆积的Ti合金是有效的。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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来源期刊
Microscopy
Microscopy 工程技术-显微镜技术
自引率
11.10%
发文量
0
审稿时长
>12 weeks
期刊介绍: Microscopy, previously Journal of Electron Microscopy, promotes research combined with any type of microscopy techniques, applied in life and material sciences. Microscopy is the official journal of the Japanese Society of Microscopy.
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