A versatile steel belt casting equipment for in situ synchrotron radiation x-ray scattering measurement of polymer films.

IF 16.4 1区化学 Q1 CHEMISTRY, MULTIDISCIPLINARY

Accounts of Chemical Research Pub Date : 2024-09-01 DOI:10.1063/5.0219366

Shenghui Liu, Shichao Cheng, Yu Luo, Jianhe Zhu, Liangbao Liu, Hang Guo, Kunpeng Cui, Minfang An, Liangbin Li

{"title":"A versatile steel belt casting equipment for in situ synchrotron radiation x-ray scattering measurement of polymer films.","authors":"Shenghui Liu, Shichao Cheng, Yu Luo, Jianhe Zhu, Liangbao Liu, Hang Guo, Kunpeng Cui, Minfang An, Liangbin Li","doi":"10.1063/5.0219366","DOIUrl":null,"url":null,"abstract":"<p><p>A steel belt casting equipment, weighing approximately ∼6-7 tons and measuring ∼5 m in length, has been designed and developed for simulating the industrial processing of polymer films and being combined with synchrotron radiation in situ x-ray scattering measurements. Through modification of its modules, it is feasible to implement two distinct film casting modes, namely the wet and the dry casting processes. The speed of a steel belt can span from 0.5 to 8 m/min. The highest experimental temperature and drying wind speed are 300 °C and 6 m/s, respectively. All film casting parameters, such as extrusion speed, distance between die and steel belt, casting speed, temperature, and wind speed, can be adjusted independently. Especially, the control accuracy of the temperature and casting rate can reach ±0.1 °C and ±0.01 m/min, respectively. The feasibility of this equipment has been validated through in situ x-ray scattering tests at the BL10U1 industrial beamline of the Shanghai synchrotron radiation facility. With the assistance of this equipment, the understanding of the physical mechanism behind the film casting process should be improved so that the development of advanced functional polymer films.</p>","PeriodicalId":1,"journal":{"name":"Accounts of Chemical Research","volume":null,"pages":null},"PeriodicalIF":16.4000,"publicationDate":"2024-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Accounts of Chemical Research","FirstCategoryId":"5","ListUrlMain":"https://doi.org/10.1063/5.0219366","RegionNum":1,"RegionCategory":"化学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q1","JCRName":"CHEMISTRY, MULTIDISCIPLINARY","Score":null,"Total":0}

引用次数: 0

Abstract

A steel belt casting equipment, weighing approximately ∼6-7 tons and measuring ∼5 m in length, has been designed and developed for simulating the industrial processing of polymer films and being combined with synchrotron radiation in situ x-ray scattering measurements. Through modification of its modules, it is feasible to implement two distinct film casting modes, namely the wet and the dry casting processes. The speed of a steel belt can span from 0.5 to 8 m/min. The highest experimental temperature and drying wind speed are 300 °C and 6 m/s, respectively. All film casting parameters, such as extrusion speed, distance between die and steel belt, casting speed, temperature, and wind speed, can be adjusted independently. Especially, the control accuracy of the temperature and casting rate can reach ±0.1 °C and ±0.01 m/min, respectively. The feasibility of this equipment has been validated through in situ x-ray scattering tests at the BL10U1 industrial beamline of the Shanghai synchrotron radiation facility. With the assistance of this equipment, the understanding of the physical mechanism behind the film casting process should be improved so that the development of advanced functional polymer films.

查看原文本刊更多论文

用于现场同步辐射 X 射线散射测量聚合物薄膜的多功能钢带铸造设备。

为模拟聚合物薄膜的工业加工过程，并结合同步辐射原位 X 射线散射测量，设计和开发了一种钢带浇注设备，重约 6-7 吨，长约 5 米。通过修改模块，可以实现两种不同的薄膜浇铸模式，即湿法和干法浇铸工艺。钢带的速度可以从 0.5 米/分钟到 8 米/分钟不等。最高实验温度和干燥风速分别为 300 °C 和 6 m/s。所有薄膜浇铸参数，如挤压速度、模具与钢带之间的距离、浇铸速度、温度和风速，均可独立调节。特别是温度和浇注速度的控制精度分别可达 ±0.1 ℃ 和 ±0.01 米/分钟。通过在上海同步辐射设施 BL10U1 工业光束线进行原位 X 射线散射试验，验证了该设备的可行性。在该设备的帮助下，人们对薄膜浇铸过程背后的物理机理的认识将得到提高，从而促进先进功能聚合物薄膜的开发。

本文章由计算机程序翻译，如有差异，请以英文原文为准。

求助全文

约1分钟内获得全文求助全文

来源期刊

Accounts of Chemical Research 化学-化学综合

CiteScore

31.40

自引率

1.10%

发文量

312

审稿时长

2 months

期刊介绍： Accounts of Chemical Research presents short, concise and critical articles offering easy-to-read overviews of basic research and applications in all areas of chemistry and biochemistry. These short reviews focus on research from the author’s own laboratory and are designed to teach the reader about a research project. In addition, Accounts of Chemical Research publishes commentaries that give an informed opinion on a current research problem. Special Issues online are devoted to a single topic of unusual activity and significance. Accounts of Chemical Research replaces the traditional article abstract with an article "Conspectus." These entries synopsize the research affording the reader a closer look at the content and significance of an article. Through this provision of a more detailed description of the article contents, the Conspectus enhances the article's discoverability by search engines and the exposure for the research.