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Solid-State Decomposition of Primary Sodium Alkoxides in Air

有机合成与工艺文献分享 2025-09-16 08:31
文章摘要
背景：固体钠甲醇盐和钠乙醇盐在有机合成中广泛应用，但存储不当可能导致分解。研究目的：探究钠甲醇盐在空气中长期存储后的分解行为及其对催化反应的影响，并与钾、锂盐稳定性对比。结论：钠甲醇盐在空气中存储20个月后剩余率低于35%，主要降解产物为碳酸钠而非氢氧化钠，降解由与二氧化碳反应引起，干燥氮气环境可防止分解，钾盐和锂盐则表现出更高稳定性。
Solid-State Decomposition of Primary Sodium Alkoxides in Air
查看文献： An Under-Appreciated Source of Reproducibility Issues in Cross-Coupling: Solid-State Decomposition of Primary Sodium Alkoxides in Air
查看期刊： ACS Catalysis
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