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Development of a Manufacturing Process for S-892216 (3)

有机合成与工艺文献分享 2025-09-10 11:02
文章摘要
背景：S-892216 (3) 的制造过程中存在化合物6的分离难题，包括溶解度低、易形成共溶剂化物及稳定性差等问题。研究目的：开发高效稳定的生产工艺，解决提取过程中的沉淀风险、复杂后处理及降解问题。结论：通过溶剂系统优化（采用磺酸烷/甲苯替代THF），实现了稳定甲苯溶剂化物的结晶控制，并在25-35°C条件下有效抑制降解，最终建立了工业可行的工艺流程。
Development of a Manufacturing Process for S-892216 (3)
查看文献： Development of a Manufacturing Process for S-892216 Part II: Improvements Toward Commercially Feasible Process
查看期刊： Organic Process Research & Development
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