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Organocatalytic Conversion of Nucleosides to Furanoid Glycals

有机合成与工艺文献分享 2025-08-21 06:21

文章摘要

本文背景聚焦于核苷向呋喃糖烯的有机催化转化过程，特别是在胸苷转化中遇到的产率不稳定问题。研究目的旨在通过工艺优化和新型催化剂开发，提高反应效率和产率稳定性。结论表明，采用氨清除剂、氮气吹扫以及新型二硫代磷酸亚胺催化剂153的应用显著改善了反应性能，BSA作为硅基转移试剂的使用可彻底解决氨气生成相关问题，最终实现75-80%的测定产率。

Organocatalytic Conversion of Nucleosides to Furanoid Glycals

查看文献： Discovery and Development of an Unusual Organocatalyst for the Conversion of Thymidine to Furanoid Glycal
查看期刊： Organic Process Research & Development

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