{"title":"金属固体样品等离子体喷射火焰发射光谱分析。1、氮气等离子体火焰的应用","authors":"K. Hirokawa, H. Gotō","doi":"10.1246/BCSJ.42.693","DOIUrl":null,"url":null,"abstract":"A small plasma jet burner for direct excitation of metal solid samples was developed. The optimum operating conditions are as follows; d.c. arc current about 15 A, flow rate of nitrogen tangentially introduced gas about 1.5–2 l/min, and that of atomizer gas about 3.5–4 l/min. The limit of detection of some elements were determined with solution samples. Satisfactory-calibration curves were also obtained for analyses of alloying elements in some solid form alloys.","PeriodicalId":21586,"journal":{"name":"Science reports of the Research Institutes, Tohoku University. Ser. A, Physics, chemistry and metallurgy","volume":"92 1","pages":"176"},"PeriodicalIF":0.0000,"publicationDate":"1969-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"6","resultStr":"{\"title\":\"Emission Spectrographic Analysis of Metal Solid Samples with Plasma Jet Flame. I. : Application of Nitrogen Plasma Flame\",\"authors\":\"K. Hirokawa, H. Gotō\",\"doi\":\"10.1246/BCSJ.42.693\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A small plasma jet burner for direct excitation of metal solid samples was developed. The optimum operating conditions are as follows; d.c. arc current about 15 A, flow rate of nitrogen tangentially introduced gas about 1.5–2 l/min, and that of atomizer gas about 3.5–4 l/min. The limit of detection of some elements were determined with solution samples. Satisfactory-calibration curves were also obtained for analyses of alloying elements in some solid form alloys.\",\"PeriodicalId\":21586,\"journal\":{\"name\":\"Science reports of the Research Institutes, Tohoku University. Ser. A, Physics, chemistry and metallurgy\",\"volume\":\"92 1\",\"pages\":\"176\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1969-03-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"6\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Science reports of the Research Institutes, Tohoku University. Ser. A, Physics, chemistry and metallurgy\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1246/BCSJ.42.693\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Science reports of the Research Institutes, Tohoku University. Ser. A, Physics, chemistry and metallurgy","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1246/BCSJ.42.693","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Emission Spectrographic Analysis of Metal Solid Samples with Plasma Jet Flame. I. : Application of Nitrogen Plasma Flame
A small plasma jet burner for direct excitation of metal solid samples was developed. The optimum operating conditions are as follows; d.c. arc current about 15 A, flow rate of nitrogen tangentially introduced gas about 1.5–2 l/min, and that of atomizer gas about 3.5–4 l/min. The limit of detection of some elements were determined with solution samples. Satisfactory-calibration curves were also obtained for analyses of alloying elements in some solid form alloys.