{"title":"利用光电化学技术制备多孔硅的电阻响应研究真空压力传感","authors":"N. Dawood, M. Zayer, Muslim F. Jawad","doi":"10.53293/jasn.2021.3763.1041","DOIUrl":null,"url":null,"abstract":"*Corresponding Author: Noor S. Dawood as.18.06@grad.uotechnology.edu.iq Abstract The manufacturing of vacuum sensors is critical to several vacuumbased applications. Porous silicon (PSi) was chosen as the vacuum sensor due to the possibility of moving air particles settled inside the pores while being put in the vacuum. The characteristics of porous silicon sensing to the evacuation of gases during vacuum was inferred by changing in the electrical resistivity. This work depends on the change in the electrical resistance of the PSi layers that was prepared via photo-electrochemical technique on the n-type (100) oriented silicon wafer. The surface topography of porous silicon is necessary to understand the morphological properties. Therefore, structural and morphological characterization of PSi samples were studied and analyzed using the scanning electron microscope (SEM) and X-Ray Diffraction (XRD) pattern. The etching process was carried out with various etching times, hydrofluoric acid (HF) concentration, and constant current density. The results showed that the pore size is increased as the etching time increased. The etching time produced pores of different sizes. The electrical resistance values were calculated after placing the sample in the vacuum system, starting from atmospheric pressure down to 10torr. The electrical properties of PSi indicate that electrical resistance gradually decreases with increasing vacuum pressure.","PeriodicalId":15241,"journal":{"name":"Journal of Applied Sciences and Nanotechnology","volume":"40 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-02-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Study of the Vacuum Pressure Sensing from the Electrical Resistance Response of Porous Silicon Fabricated via Photo-Electrochemical Technique\",\"authors\":\"N. Dawood, M. Zayer, Muslim F. Jawad\",\"doi\":\"10.53293/jasn.2021.3763.1041\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"*Corresponding Author: Noor S. Dawood as.18.06@grad.uotechnology.edu.iq Abstract The manufacturing of vacuum sensors is critical to several vacuumbased applications. Porous silicon (PSi) was chosen as the vacuum sensor due to the possibility of moving air particles settled inside the pores while being put in the vacuum. The characteristics of porous silicon sensing to the evacuation of gases during vacuum was inferred by changing in the electrical resistivity. This work depends on the change in the electrical resistance of the PSi layers that was prepared via photo-electrochemical technique on the n-type (100) oriented silicon wafer. The surface topography of porous silicon is necessary to understand the morphological properties. Therefore, structural and morphological characterization of PSi samples were studied and analyzed using the scanning electron microscope (SEM) and X-Ray Diffraction (XRD) pattern. The etching process was carried out with various etching times, hydrofluoric acid (HF) concentration, and constant current density. The results showed that the pore size is increased as the etching time increased. The etching time produced pores of different sizes. The electrical resistance values were calculated after placing the sample in the vacuum system, starting from atmospheric pressure down to 10torr. The electrical properties of PSi indicate that electrical resistance gradually decreases with increasing vacuum pressure.\",\"PeriodicalId\":15241,\"journal\":{\"name\":\"Journal of Applied Sciences and Nanotechnology\",\"volume\":\"40 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-02-27\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Applied Sciences and Nanotechnology\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.53293/jasn.2021.3763.1041\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Applied Sciences and Nanotechnology","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.53293/jasn.2021.3763.1041","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 1
摘要
*通讯作者:Noor S. Dawood as.18.06@grad.uotechnology.edu.iq摘要真空传感器的制造对于几种基于真空的应用至关重要。之所以选择多孔硅(PSi)作为真空传感器,是因为在真空状态下,孔隙内的空气颗粒可能会移动。通过电阻率的变化推断了多孔硅在真空过程中对气体释放的传感特性。这项工作依赖于通过光电化学技术在n型(100)取向硅片上制备的PSi层的电阻变化。多孔硅的表面形貌是了解其形态特性的必要条件。因此,采用扫描电镜(SEM)和x射线衍射(XRD)对PSi样品的结构和形态特征进行了研究和分析。在不同的蚀刻次数、氢氟酸(HF)浓度和恒流密度下进行了蚀刻过程。结果表明,随着刻蚀时间的延长,孔尺寸增大。蚀刻时间产生了不同大小的孔隙。将样品置于真空系统中,从大气压开始,直至10torr,计算电阻值。PSi的电学特性表明,电阻随真空压力的增大而逐渐减小。
Study of the Vacuum Pressure Sensing from the Electrical Resistance Response of Porous Silicon Fabricated via Photo-Electrochemical Technique
*Corresponding Author: Noor S. Dawood as.18.06@grad.uotechnology.edu.iq Abstract The manufacturing of vacuum sensors is critical to several vacuumbased applications. Porous silicon (PSi) was chosen as the vacuum sensor due to the possibility of moving air particles settled inside the pores while being put in the vacuum. The characteristics of porous silicon sensing to the evacuation of gases during vacuum was inferred by changing in the electrical resistivity. This work depends on the change in the electrical resistance of the PSi layers that was prepared via photo-electrochemical technique on the n-type (100) oriented silicon wafer. The surface topography of porous silicon is necessary to understand the morphological properties. Therefore, structural and morphological characterization of PSi samples were studied and analyzed using the scanning electron microscope (SEM) and X-Ray Diffraction (XRD) pattern. The etching process was carried out with various etching times, hydrofluoric acid (HF) concentration, and constant current density. The results showed that the pore size is increased as the etching time increased. The etching time produced pores of different sizes. The electrical resistance values were calculated after placing the sample in the vacuum system, starting from atmospheric pressure down to 10torr. The electrical properties of PSi indicate that electrical resistance gradually decreases with increasing vacuum pressure.