阿拉伯联合酋长国进口枣椰果中农药残留监测

N. M. A. El-Mageed, I. Abu-Abdoun, Kaltham A. H. Kayaf, Abdulla S. Janaan
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引用次数: 1

摘要

对2020年期间从阿拉伯联合酋长国(阿联酋)进口的枣椰果中采集的代表性样品中农药残留情况进行了调查,以确保监管当局遵守标准规范和要求,维护消费者的健康和安全,并改善食品安全。采用多反应监测(MRM)模式的液相色谱-串联质谱(LC-ESI (+)-MS/MS)和改进的快速、简便、廉价、有效、坚固、安全(QuEChERS)方法,建立了一种准确、快速、可靠的同时测定230份进口日期样品中农药多残留的方法。根据欧盟SANCO指南(SANTE/12682/2019)对分析方法的性能进行了验证,该指南用于监测农药多重残留,以检查是否符合现有法规,特别是欧共体法规。测定了230份样品中343种化合物的残留水平。结果表明,红枣样品中残留在最大残留限量(MRL)以上的样品占4.34%,在最大残留限量内的样品占7.39%。230份样品中未检出残留,占88.26%。根据阿联酋、食品法典委员会和欧洲法规,在测试的343种农药中,有11种农药超过了检测限度。这项工作的主要目的,是让关注食物安全的市民和商号,了解商务部在保证进口食物中残留除害剂的质素方面的能力。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Monitoring of Pesticide Residues in Imported Datepalm Fruits in United Arab Emirates
The occurrence of pesticide residues in representative samples collected from imported dates palm fruits during 2020 to United Arab Emirates (UAE) was investigated to ensure compliance with the standard specifications and requirements by the regulatory and supervisory authorities, maintain the health and safety of consumers and improve food safety. An accurate, rapid, and reliable method for the simultaneous determination of pesticide multi-residues in 230 samples imported dates by liquid chromatography coupled with tandem mass spectrometry (LC–ESI (+)-MS/MS) operating in multiple reaction monitoring (MRM) mode and modified quick, easy, cheap, effective, rugged, safe (QuEChERS) method was used. The performance of the analytical method was validated in accordance with EU SANCO guidelines (SANTE/12682/2019) for monitoring pesticide multi-residues to check compliance with existing regulations, especially for European Community. Residues level of 343 compounds were determined in 230 samples. Results indicated that the percentage of samples with residues above the maximum residue levels (MRL) was 4.34% in dates samples, whereas samples with residues within MRL were 7.39% in dates samples. A total of 230 samples of 88.26% were free from detectable residues. Out of the 343 pesticides tested, 11 pesticides were found above the limit of detection, according to UAE, Codex, and European regulations. The main purpose of this work is to inform citizens and traders who have concerns about food safety on the capability of the MOCCAE on quality assurance regarding pesticide residue in imported food.
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