新型层状纳米硼酸锌的合成

2013 International Conference on Materials for Renewable Energy and Environment Pub Date : 2013-08-01 DOI:10.1109/ICMREE.2013.6893742

Pingqiang Gao, Wenhua Song, Feng Ding, Xing Wang

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引用次数: 1

摘要

在硼酸钠(Na2B4O7.10H2O)和硝酸硼酸锌(Zn(NO3)2·6H2O)的水溶液中，通过一步沉淀法成功合成了新型片状纳米硼酸锌4ZnOB2O3H2O。利用x射线衍射(XRD)、场发射扫描电镜(FESEM)、傅里叶变换红外光谱(FTIR)对样品进行表征，发现新材料具有片层状结构，粒径在100 ~ 200 nm左右，片层尺寸均匀，分散良好。

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Synthesis of a new lamellar nano zinc borate

A new lamellar nano zinc borate 4ZnOB₂O₃H₂O were successfully synthesized via one-step precipitation reaction in aqueous solution of sodium borate (Na₂B₄O₇.10H₂O) and zinc borate nitrate(Zn(NO₃)₂·6H₂O). The characterizations of the as-obtained samples were studied by X-ray diffraction(XRD), Field-emission scanning electron microscopy (FESEM), Fourier transform infrared spectrum (FTIR), It had been found that the new material have a lamellar shape with the particle size of around 100-200 nm, and it seems that the lamellar are size-homogeneous and well dispersed.

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2013 International Conference on Materials for Renewable Energy and Environment

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