微乳液法原位合成NiO/ZnO核壳纳米颗粒

Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Pub Date : 2016-05-03 DOI:10.1080/15533174.2014.989595

D. Han, C. Wang, D. Li, Z. Cao

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引用次数: 10

摘要

在Triton X-100/正己醇/环己烷/水W/O微乳液体系中成功制备了NiO(核)/ZnO(壳)核-壳和纳米颗粒。确定了基本合成条件。首先在室温下合成Ni(OH)2/Zn(OH)2纳米颗粒，然后在500℃下煅烧得到NiO/ZnO纳米颗粒。采用透射电镜(TEM)和x射线衍射仪(XRD)对煅烧产物进行了研究。阐述了核壳型NiO/ZnO纳米颗粒的形成机理。

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NiO/ZnO Core-Shell Nanoparticles In Situ Synthesis Via Microemulsion Method

Nanoparticles of NiO(core)/ZnO(shell) core-shell and nanoparticles were successfully prepared in Triton X-100/n-hexanol/cyclohexane/water W/O microemulsion system. Basic synthesis conditions were determined. Ni(OH)2/Zn(OH)2 nanoparticles were first synthesized at room temperature then calcined at 500°C to form NiO/ZnO nanoparticles. The calcined products were studied by means of TEM, and XRD analyzers. The mechanism of the core shell NiO/ZnO nanoparticles formation is explained.

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来源期刊

Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry 工程技术-纳米科技

自引率

0.00%

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审稿时长

5 months