溶剂和催化剂用量对羊尾草高聚物聚合的影响研究

N. H. Airun, Zukhrufi Zukhrufi, F. I. Fajarwati
{"title":"溶剂和催化剂用量对羊尾草高聚物聚合的影响研究","authors":"N. H. Airun, Zukhrufi Zukhrufi, F. I. Fajarwati","doi":"10.20885/ijcr.vol5.iss2.art2","DOIUrl":null,"url":null,"abstract":"Aricryl synthesis was carried out by feeding technique. The monomers used were styrene, isobutyl acrylate, 2-HEMA and acrylamide powder. The catalysts used were AIBN (Azobisisobutyronitrile) and Perbutyl O98. The synthesis results were then devided by 2 for resin batch G-0915 A was diluted in > 63% mixture of n-butanol and methanol, while for G-0915 B was carried out dilution in > 63% toluene. the results obtained were compared based on the influence of the solvent using the parameters of viscosity, NV/total solid, AV (Acid Value), color and OH value. It was found that the best solvent according to specifications is toluene solvent with a viscosity of Z2-15. The Aricryl batch G-0915 was compared with Aricryl batch G-0903 based on the influence of the quantity of catalyst. The results showed that the increasing quantity of catalyst affects the aging process. Aging duration for Aricryl batch G-0903 was 11 hours, while for Arycril batch G-0915 was 8 hours.","PeriodicalId":33936,"journal":{"name":"Indonesian Journal of Chemical Research","volume":"21 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2020-11-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"STUDY OF THE EFFECT OF SOLVENT AND QUANTITY OF CATALYST ON ARICRYL POLYMERIZATION AT PT. ARISTEK HIGHPOLYMER BEKASI\",\"authors\":\"N. H. Airun, Zukhrufi Zukhrufi, F. I. Fajarwati\",\"doi\":\"10.20885/ijcr.vol5.iss2.art2\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Aricryl synthesis was carried out by feeding technique. The monomers used were styrene, isobutyl acrylate, 2-HEMA and acrylamide powder. The catalysts used were AIBN (Azobisisobutyronitrile) and Perbutyl O98. The synthesis results were then devided by 2 for resin batch G-0915 A was diluted in > 63% mixture of n-butanol and methanol, while for G-0915 B was carried out dilution in > 63% toluene. the results obtained were compared based on the influence of the solvent using the parameters of viscosity, NV/total solid, AV (Acid Value), color and OH value. It was found that the best solvent according to specifications is toluene solvent with a viscosity of Z2-15. The Aricryl batch G-0915 was compared with Aricryl batch G-0903 based on the influence of the quantity of catalyst. The results showed that the increasing quantity of catalyst affects the aging process. Aging duration for Aricryl batch G-0903 was 11 hours, while for Arycril batch G-0915 was 8 hours.\",\"PeriodicalId\":33936,\"journal\":{\"name\":\"Indonesian Journal of Chemical Research\",\"volume\":\"21 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2020-11-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Indonesian Journal of Chemical Research\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.20885/ijcr.vol5.iss2.art2\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Indonesian Journal of Chemical Research","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.20885/ijcr.vol5.iss2.art2","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

采用进料法合成芳基。所使用的单体有苯乙烯、丙烯酸异丁酯、2-HEMA和丙烯酰胺粉末。催化剂为AIBN(偶氮二异丁腈)和过丁基O98。树脂批G-0915 A在> 63%的正丁醇和甲醇混合物中稀释,G-0915 B在> 63%的甲苯中稀释,合成结果除以2。通过粘度、NV/total solid、AV (Acid Value)、颜色、OH值等参数,比较了溶剂对所得结果的影响。结果表明,符合规格要求的最佳溶剂为粘度为Z2-15的甲苯溶剂。根据催化剂用量的影响,对G-0915和G-0903两批aricyl进行了比较。结果表明,催化剂用量的增加会影响其老化过程。芳烯醇G-0903批次的老化时间为11小时,而芳烯醇G-0915批次的老化时间为8小时。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
STUDY OF THE EFFECT OF SOLVENT AND QUANTITY OF CATALYST ON ARICRYL POLYMERIZATION AT PT. ARISTEK HIGHPOLYMER BEKASI
Aricryl synthesis was carried out by feeding technique. The monomers used were styrene, isobutyl acrylate, 2-HEMA and acrylamide powder. The catalysts used were AIBN (Azobisisobutyronitrile) and Perbutyl O98. The synthesis results were then devided by 2 for resin batch G-0915 A was diluted in > 63% mixture of n-butanol and methanol, while for G-0915 B was carried out dilution in > 63% toluene. the results obtained were compared based on the influence of the solvent using the parameters of viscosity, NV/total solid, AV (Acid Value), color and OH value. It was found that the best solvent according to specifications is toluene solvent with a viscosity of Z2-15. The Aricryl batch G-0915 was compared with Aricryl batch G-0903 based on the influence of the quantity of catalyst. The results showed that the increasing quantity of catalyst affects the aging process. Aging duration for Aricryl batch G-0903 was 11 hours, while for Arycril batch G-0915 was 8 hours.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
39
审稿时长
4 weeks
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信