离子液体作为封盖剂的纯纳米颗粒和混合纳米颗粒的比较

N. Santhi, K. Rajathi, S. Sridhar
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引用次数: 3

摘要

离子液体是一种特殊的化合物,在现代科学的许多领域都有应用。由于离子液体具有高度可调性和无与伦比的性能,在合成、催化、萃取、电化学、分析、生物技术等领域发挥着重要作用。离子液体除了具有物理和化学性质外,其高生物活性也引起了生物化学家、生态学家和医学专业人士的极大关注。鉴于上述性质,采用咪唑离子液体溶剂合成纳米结构的纳米颗粒。本文通过简单的共沉淀、还原和共沉淀工艺,成功地合成了立方型纯Fe2O3、球形纯Ag(0)和六角形杂化AgFe2O3。通过IR、XRD、SEM、EDX和TEM等光谱分析对合成的纳米颗粒进行了详细表征。采用x射线衍射(XRD)、扫描电子显微镜(SEM)和透射电子显微镜(TEM)技术对颗粒的大小和形状进行了表征。用能量色散x射线分析(EDX)对产品的质量、数量和纯度进行了检测。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Comparison of Pure and Hybrid Nanoparticles using Ionic Liquid as a Capping agent
Ionic liquids are exceptional chemical compounds that are used in many areas of modern science. Due to their highly adjustable nature and incomparable properties, ionic liquids have become key players in the areas of synthesis, catalysis, extraction, electrochemistry, analysis, biotechnology, etc. In addition to the physical and chemical properties of ionic liquids, their high biological activity has attracted considerable attention from biochemists, ecologists and medical professionals. Due to the properties mentioned above, an imidazolium ionic liquid solvent was used for the synthesis of nanostructure nanoparticles. In the present work, cubic form of pure Fe2O3, spherical nature of pure Ag (0) and hexagonal shaped hybrid AgFe2O3 were successfully synthesized by a simple co-precipitation, reduction and co-precipitation processes. The synthesized nanoparticles were characterized in detail by spectral studies such as IR, XRD, SEM, EDX and TEM analysis. The size and shape of the particles were performed by X-ray Diffraction (XRD), Scanning Electron Microscope (SEM) techniques and Transmission Electron Microscope (TEM) techniques. Quality quantity and purity of the products was checked by Energy Dispersive X-Ray Analysis (EDX).
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