M. Scapin, M. C. Tessari-Zampieri, S. Guilhen, M. Cotrim
{"title":"x射线荧光光谱法:废物分析的一种替代技术","authors":"M. Scapin, M. C. Tessari-Zampieri, S. Guilhen, M. Cotrim","doi":"10.15392/2319-0612.2023.2144","DOIUrl":null,"url":null,"abstract":"This study aims to develop reliable analytical methodology that is, cost-effective, and requires minimal sample quantity to quantify uranium content in nuclear waste and others. The Energy Dispersive X-ray Fluorescence Spectrometry (EDXRF) technique was used, and a rigorous comparison was made between the fundamental parameters (FP) method and the empirical (EMP) method. Statistical evaluation of results demonstrated that the FP method showed a satisfactory level of confidence for precision and limit of quantification.","PeriodicalId":9203,"journal":{"name":"Brazilian Journal of Radiation Sciences","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2023-05-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"X-ray fluorescence spectrometry: An alternative technique for analysis of waste\",\"authors\":\"M. Scapin, M. C. Tessari-Zampieri, S. Guilhen, M. Cotrim\",\"doi\":\"10.15392/2319-0612.2023.2144\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"This study aims to develop reliable analytical methodology that is, cost-effective, and requires minimal sample quantity to quantify uranium content in nuclear waste and others. The Energy Dispersive X-ray Fluorescence Spectrometry (EDXRF) technique was used, and a rigorous comparison was made between the fundamental parameters (FP) method and the empirical (EMP) method. Statistical evaluation of results demonstrated that the FP method showed a satisfactory level of confidence for precision and limit of quantification.\",\"PeriodicalId\":9203,\"journal\":{\"name\":\"Brazilian Journal of Radiation Sciences\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-05-22\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Brazilian Journal of Radiation Sciences\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.15392/2319-0612.2023.2144\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Brazilian Journal of Radiation Sciences","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.15392/2319-0612.2023.2144","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
X-ray fluorescence spectrometry: An alternative technique for analysis of waste
This study aims to develop reliable analytical methodology that is, cost-effective, and requires minimal sample quantity to quantify uranium content in nuclear waste and others. The Energy Dispersive X-ray Fluorescence Spectrometry (EDXRF) technique was used, and a rigorous comparison was made between the fundamental parameters (FP) method and the empirical (EMP) method. Statistical evaluation of results demonstrated that the FP method showed a satisfactory level of confidence for precision and limit of quantification.