富果木的GC-MS/FT-IR筛选

S. Okereke, U. Arunsi, C. Nosiri
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引用次数: 5

摘要

采用傅里叶变换红外光谱(FTIR)和气相色谱-质谱(GC-MS)联用技术对青木果实中的官能团和植物成分进行了鉴定。采用Perkin Elmer分光光度计进行FTIR分析,并对其特征峰进行检测。采用气相色谱-质谱法筛选植物化学成分,化合物检测采用NIST 2.0版本2005文库。气相色谱-质谱分析结果显示不同的峰,测定了15种植物化学成分的存在。植物成分占比为β-依兰烯(2.85%)、1,6-环十二烯、1-甲基-5-亚甲基-8-(1-亚甲基)-、[s-(E,E)]- (1.71%);(-)- spathulenol(1.23%),反式- z -α-双abolene环氧化物(1.68%);正十六酸(2.90%);Manoyl oxide (2.51%);亚油酸(8.14%);油酸(3.13%);Cis-Z -α-Bisabolene (1.34%);Pimara-7 15-diene-3-one (8.86%);1-Heptatricotanol (2.07%);Kaur-1b-ene (6.59%);β-海松酸(36.39%);doconconent(1.66%)和androstanan -17- 1,3 -乙基-3-羟基- (5a)-(17.48%)。傅里叶红外光谱研究的结果揭示了芳烃、醇类、酚类、羧酸类、醚类、芳烃类、芳酮类、烯烃类、饱和醛类和酚类的存在。本研究对埃塞俄比亚木杉果实提取物进行了气相色谱-质谱和红外光谱分析,这些提取物含有多种生物活性成分,在民族医学中具有治疗感染和疾病的作用。关键词:傅里叶变换红外光谱(FTIR),气相色谱-质谱(GC-MS),植物化学,埃塞俄比亚木
本文章由计算机程序翻译,如有差异,请以英文原文为准。
GC-MS/FT-IR screening of Xylopia aethiopica (Dunal) A. Rich Fruit
The present study was aimed at identifying the functional groups and phyto-constituents present in Xylopia aethiopica (Dunal) A Rich fruit using Fourier Transform Infrared Spectrometry (FTIR) and Gas chromatography-mass spectroscopy (GC-MS), spectroscopy. FTIR method was performed using Perkin Elmer Spectrophotometer and the characteristic peaks were detected. The phytochemical constituents were screened by GC-MS method and the compound detection employed the NIST Ver. 2.0 year 2005 library. The results of the GC-MS analysis showed different peaks determining the presence of 15 phytochemical compounds in the fruit extract of A. aetiopica. The phyto-constituents with their percentage areas include β-Ylangene(2.85%), 1,6-Cyclodecadiene, 1-methyl-5-methylene-8- (1-methylene)-, [s-(E,E)]- (1.71%); (-)-Spathulenol (1.23%);Trans-Z-α-Bisabolene epoxide (1.68%); n-Hexadecanoic acid (2.90%); Manoyl oxide (2.51%); Linoleic acid (8.14%); Oleic acid (3.13%); Cis-Z-α-Bisabolene (1.34%); Pimara-7,15-diene-3-one (8.86%); 1-Heptatricotanol (2.07%); Kaur-1b-ene (6.59%); β-Pimaric acid (36.39%); Doconexent (1.66%) and Androstan-17-one, 3-ethyl-3-hydroxyl-, (5a)- (17.48%). The result of the FTIR spectroscopic studies revealed the presence of arenes, alcohols, phenols, carboxylic acids, ethers, aromatics, aryl ketone, alkenes, saturated aldehyde and phenols. The findings of the study revealed that the GC-MS and FTIR spectral analyses of Xylopia aethiopica (Dunal) A. Rich fruit extract composed of various bioactive compounds which have are used in ethnomedicine to treat and cure infections and diseases.   Key words: Fourier Transform Infrared Spectrometry (FTIR), Gas chromatography-mass spectroscopy (GC-MS), phytochemical, Xylopia aethiopica.
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