{"title":"水热合成钛酸铋","authors":"A. V. Prasada Rao, S. Komarneni","doi":"10.1109/ISAF.1996.598177","DOIUrl":null,"url":null,"abstract":"Bismuth titanate powder was synthesized at 240/spl deg/C by hydrothermal method using bismuth and titanium coprecipitated hydrous oxides. Microstructural investigation of resultant powder revealed aggregates of about 5-10 /spl mu/m. Pelletized samples derived from the above powder when heat treated at 1050/spl deg/C for 2 hrs showed 93.3% theoretical density. Fractured surface of sintered pellet showed large platelets of the order of 10-20 /spl mu/m indicating extensive grain growth.","PeriodicalId":14772,"journal":{"name":"ISAF '96. Proceedings of the Tenth IEEE International Symposium on Applications of Ferroelectrics","volume":"36 1","pages":"923-925 vol.2"},"PeriodicalIF":0.0000,"publicationDate":"1996-08-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Hydrothermal synthesis of bismuth titanate\",\"authors\":\"A. V. Prasada Rao, S. Komarneni\",\"doi\":\"10.1109/ISAF.1996.598177\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Bismuth titanate powder was synthesized at 240/spl deg/C by hydrothermal method using bismuth and titanium coprecipitated hydrous oxides. Microstructural investigation of resultant powder revealed aggregates of about 5-10 /spl mu/m. Pelletized samples derived from the above powder when heat treated at 1050/spl deg/C for 2 hrs showed 93.3% theoretical density. Fractured surface of sintered pellet showed large platelets of the order of 10-20 /spl mu/m indicating extensive grain growth.\",\"PeriodicalId\":14772,\"journal\":{\"name\":\"ISAF '96. Proceedings of the Tenth IEEE International Symposium on Applications of Ferroelectrics\",\"volume\":\"36 1\",\"pages\":\"923-925 vol.2\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1996-08-18\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"ISAF '96. Proceedings of the Tenth IEEE International Symposium on Applications of Ferroelectrics\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1109/ISAF.1996.598177\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"ISAF '96. Proceedings of the Tenth IEEE International Symposium on Applications of Ferroelectrics","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1109/ISAF.1996.598177","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Bismuth titanate powder was synthesized at 240/spl deg/C by hydrothermal method using bismuth and titanium coprecipitated hydrous oxides. Microstructural investigation of resultant powder revealed aggregates of about 5-10 /spl mu/m. Pelletized samples derived from the above powder when heat treated at 1050/spl deg/C for 2 hrs showed 93.3% theoretical density. Fractured surface of sintered pellet showed large platelets of the order of 10-20 /spl mu/m indicating extensive grain growth.