热处理化学镀Ni-YSZ陶瓷涂层显微硬度参数优化

Q3 Engineering

Journal of Achievements in Materials and Manufacturing Engineering Pub Date : 2022-05-01 DOI:10.5604/01.3001.0016.0293

N. Bahiyah Baba, A. S. Ghazali, A. A. Abdul Rahman, S. Sharif

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引用次数: 0

摘要

讨论了化学镀Ni-YSZ陶瓷涂层热处理显微硬度的参数优化。热处理是提高化学镀镍层力学性能的一种方法，通过控制热处理参数可以提高化学镀镍层的力学性能。通过27次全阶乘3x3实验设计进行参数优化。在Minitab20中使用统计工具ANOVA对3个水平下的处理温度、处理时间和陶瓷粒度参数进行了评估。采用化学共沉积镍的方法在高速钢基体上沉积Ni-YSZ金属陶瓷涂层。温度和时间分别在300-400℃和0-2小时范围内变化。显微硬度测量使用维氏显微硬度计(岛津)根据ISO 6507-4进行。采用剑桥立体扫描90扫描电子显微镜(SEM)和能量色散x射线分析(EDXA)对其表面特征进行了分析。利用Minitab20软件中的方差分析(ANOVA)对Ni-YSZ陶瓷涂层获得高显微硬度的最佳条件进行了评价。结果表明，在处理温度为400℃时对高显微硬度影响最大，其次是处理时间为2小时。陶瓷粒度对获得高显微硬度的影响不大，但对处理温度和处理时间的相互作用有影响。本文只讨论了不同热处理参数对Ni-YSZ金属陶瓷涂层硬度性能影响的显微硬度优化条件。所得到的优化条件仅适用于化学镍溶液和处理方法相似的Ni-YSZ陶瓷镀层。本工作的价值在于利用实验三水平全析因设计对Ni-YSZ化学陶瓷涂层进行热处理参数优化，以获得较高的显微硬度。

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Parametric optimisation of microhardness on heat-treated electroless Ni-YSZ cermet coating

The paper discusses the parametric optimisation of the electroless Ni-YSZ cermet coating microhardness upon heat treatment. Heat treatment is a process to increase the mechanical properties of the electroless nickel coating and it can be enhanced by manipulating its parameters. Parametric optimisation is conducted by the design of experiment full factorial 3x3 with 27 runs. Treating temperature, treating time and ceramic particle size parameters at 3-level are evaluated using statistical tool ANOVA in Minitab20. Ni-YSZ cermet coating is deposited onto a high-speed steel substrate using the electroless nickel co-deposition method. The temperature and time were varied in a range of 300-400oC and 0-2 hours respectively. The microhardness measurements were carried out using a Vickers microhardness tester (Shimadzu) according to ISO 6507-4. The surface characterisation was analysed using Cambridge Stereoscan 90 Scanning Electron Microscope (SEM) coupled with Energy Dispersive X-ray Analysis (EDXA). The optimum condition in obtaining high microhardness on Ni-YSZ cermet coating is evaluated by statistical tool ANOVA in Minitab20 software. It is found that the most significant parameter for high microhardness is at the treating temperature of 400oC followed by treating time at 2 hours using nano-sized YSZ particles. The ceramic particle size is found not a significant parameter in obtaining a high microhardness, however it has effect on interaction between treating temperature and treating time. The paper only limits to the optimisation condition of microhardness on Ni-YSZ cermet coating hardness property by varying heat treatment parameters. The optimisation condition obtained might only applicable to the electroless Ni-YSZ cermet coating with similar electroless nickel solution and treatments. The value of this work is the heat treatment parametric optimisation to obtain high microhardness on electroless Ni-YSZ cermet coating by using the design of experiment 3-level full factorial.

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来源期刊

Journal of Achievements in Materials and Manufacturing Engineering Engineering-Industrial and Manufacturing Engineering

CiteScore

2.10

自引率

0.00%

发文量

期刊介绍： The Journal of Achievements in Materials and Manufacturing Engineering has been published by the Association for Computational Materials Science and Surface Engineering in collaboration with the World Academy of Materials and Manufacturing Engineering WAMME and the Section Metallic Materials of the Committee of Materials Science of the Polish Academy of Sciences as a monthly. It has 12 points which was received during the evaluation by the Ministry of Science and Higher Education journals and ICV 2017:100 on the ICI Journals Master list announced by the Index Copernicus. It is a continuation of "Proceedings on Achievements in Mechanical and Materials Engineering" published in 1992-2005. Scope: Materials[...] Properties[...] Methodology of Research[...] Analysis and Modelling[...] Manufacturing and Processingv Biomedical and Dental Engineering and Materials[...] Cleaner Production[...] Industrial Mangement and Organisation [...] Education and Research Trends[...]