利用绿豆植物废料合成绿色氧化铈纳米颗粒用于绿豆种子萌发

IF 3.9 Q2 NANOSCIENCE & NANOTECHNOLOGY
Nor Monica Ahmad, Nor’ Aishah Hasan
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引用次数: 0

摘要

利用生物方法合成氧化铈纳米颗粒(CeO2)以减少化学合成的有害影响已引起人们的广泛关注。本研究以土芋叶提取物为原料,采用溶胶-凝胶法制备CeO2-NPs。根据Debye-Scherrer方程,x射线粉末衍射(XRD)证实CeO2-NPs的晶体结构为立方结构,尺寸为2.94 nm。透射电子显微镜(TEM)图像显示,CeO2-NPs呈球形,平均尺寸为2.04 nm,与XRD分析结果基本一致。能量色散x射线(EDX)测量显示出归因于Ce和氧的高强度峰,进一步证明了CeO2-NPs的产生。傅里叶变换红外光谱(FTIR)分析显示Ce-O拉伸的存在,表明CeO2-NPs的形成。由于在CeO2-NPs合成过程中负责还原和稳定的植物化学成分,在光谱中发现了O- h、C-O和C=O的官能团。紫外可见光谱在213 nm处出现吸光度峰。进一步研究了合成的NPs对绿豆种子萌发的影响,发现籽粒萌发率和生长速率对绿豆种子萌发的影响具有显著性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis of Green Cerium Oxide Nanoparticles Using Plant Waste from Colocasia esculenta for Seed Germination of Mung Bean (Vigna radiata)
Synthesis of cerium oxide (CeO2) nanoparticles (NPs) via biological approach has received a lot of interest to reduce the harmful effects of chemical synthesis. In the present study, Colocasia esculenta leaf extract facilitated the preparation of CeO2-NPs by using the sol-gel technique. The crystal structural of CeO2-NPs was proven by X-ray powder diffraction (XRD) investigation to be cubic with size of 2.94 nm according to Debye–Scherrer equation. As demonstrated in the transmission electron microscopy (TEM) image, CeO2-NPs have a spherical form with an average size of 2.04 nm which is almost consistent with a finding from XRD analysis. Energy dispersive X-ray (EDX) measurements exhibited high-intensity peaks attributed to Ce and oxygen and further proved the creation of CeO2-NPs. The Fourier transform infrared spectroscopy (FTIR) analysis revealed the presence of Ce-O stretching, indicating the formation of CeO2-NPs. Functional groups of O-H, C-O, and C=O peaks were found in a spectrum due to the phytochemical components that were responsible for reducing and stabilizing during the synthesis process of CeO2-NPs. The examined UV-visible spectra exhibited the absorbance peak at 213 nm. The synthesized NPs produced in this study were further investigated for mung bean seed germination, whereby the influence of grain germination and growth rate demonstrated the significant finding.
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来源期刊
Journal of Nanotechnology
Journal of Nanotechnology NANOSCIENCE & NANOTECHNOLOGY-
CiteScore
5.50
自引率
2.40%
发文量
25
审稿时长
13 weeks
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