甘蔗渣基活性炭的合成与表征:氯化锌浸渍率的影响

S. Joshi, Bishnu K.C.
{"title":"甘蔗渣基活性炭的合成与表征:氯化锌浸渍率的影响","authors":"S. Joshi, Bishnu K.C.","doi":"10.3126/jncs.v41i1.30490","DOIUrl":null,"url":null,"abstract":"Series of activated carbons (ACs) have been prepared from sugarcane bagasse powder by ZnCl2 activation at various impregnation ratios of ZnCl2 to Sugarcane bagasse powder of 0.25:1, 0.5:1, 1:1 and 2:1 by weight. Characteristics of the activated carbons (ACs) were determined by iodine number, methylene blue number, surface area, scanning electron microscopy (SEM) and x-ray diffraction. Iodine number (IN) indicated that, microporosity of the AC were increased with increasing impregnation ratio ZnCl2 to Sugarcane bagasse upto 1:1 then started to decrease. However, mesoporosity as well as surface area was increased progressively. The maximum value of iodine number (868 mg/g) was achieved in the AC prepared at impregnation ratio of ZnCl2 to Sugarcane bagasse of 1:1. SEM micrographs also show the presence of well developed pores on its surface of AC-1. The broad peaks in the XRD patterns indicated that, all the ACs is amorphous materials. From results, it is concluded that ZnCl2 concentration used in impregnation is effective for development of porosity and surface area of the AC prepared from sugarcane bagasse.","PeriodicalId":16483,"journal":{"name":"Journal of Nepal Chemical Society","volume":"75 1","pages":"74-79"},"PeriodicalIF":0.0000,"publicationDate":"2020-08-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Synthesis and Characterization of Sugarcane Bagasse Based Activated Carbon: Effect of Impregnation Ratio of ZnCl2\",\"authors\":\"S. Joshi, Bishnu K.C.\",\"doi\":\"10.3126/jncs.v41i1.30490\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Series of activated carbons (ACs) have been prepared from sugarcane bagasse powder by ZnCl2 activation at various impregnation ratios of ZnCl2 to Sugarcane bagasse powder of 0.25:1, 0.5:1, 1:1 and 2:1 by weight. Characteristics of the activated carbons (ACs) were determined by iodine number, methylene blue number, surface area, scanning electron microscopy (SEM) and x-ray diffraction. Iodine number (IN) indicated that, microporosity of the AC were increased with increasing impregnation ratio ZnCl2 to Sugarcane bagasse upto 1:1 then started to decrease. However, mesoporosity as well as surface area was increased progressively. The maximum value of iodine number (868 mg/g) was achieved in the AC prepared at impregnation ratio of ZnCl2 to Sugarcane bagasse of 1:1. SEM micrographs also show the presence of well developed pores on its surface of AC-1. The broad peaks in the XRD patterns indicated that, all the ACs is amorphous materials. From results, it is concluded that ZnCl2 concentration used in impregnation is effective for development of porosity and surface area of the AC prepared from sugarcane bagasse.\",\"PeriodicalId\":16483,\"journal\":{\"name\":\"Journal of Nepal Chemical Society\",\"volume\":\"75 1\",\"pages\":\"74-79\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2020-08-05\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Journal of Nepal Chemical Society\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.3126/jncs.v41i1.30490\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Nepal Chemical Society","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.3126/jncs.v41i1.30490","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3

摘要

以蔗渣粉为原料,在ZnCl2与蔗渣粉的浸渍比为0.25:1、0.5:1、1:1和2:1的条件下,采用ZnCl2活化制得系列活性炭。采用碘值、亚甲基蓝值、比表面积、扫描电镜和x射线衍射等方法对活性炭进行了表征。碘值(IN)表明,随着ZnCl2与蔗渣浸渍比的增加,蔗渣的微孔隙率逐渐增加,至1:1后开始降低。介孔率和比表面积逐渐增大。在氯化锌与甘蔗渣浸渍比为1:1的条件下制备的活性炭,碘值达到最大值(868 mg/g)。SEM显微图也显示AC-1表面存在发育良好的孔隙。XRD谱图的宽峰分析表明,活性炭均为非晶材料。实验结果表明,ZnCl2浸渍对蔗渣活性炭的孔隙率和比表面积的发展是有效的。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Characterization of Sugarcane Bagasse Based Activated Carbon: Effect of Impregnation Ratio of ZnCl2
Series of activated carbons (ACs) have been prepared from sugarcane bagasse powder by ZnCl2 activation at various impregnation ratios of ZnCl2 to Sugarcane bagasse powder of 0.25:1, 0.5:1, 1:1 and 2:1 by weight. Characteristics of the activated carbons (ACs) were determined by iodine number, methylene blue number, surface area, scanning electron microscopy (SEM) and x-ray diffraction. Iodine number (IN) indicated that, microporosity of the AC were increased with increasing impregnation ratio ZnCl2 to Sugarcane bagasse upto 1:1 then started to decrease. However, mesoporosity as well as surface area was increased progressively. The maximum value of iodine number (868 mg/g) was achieved in the AC prepared at impregnation ratio of ZnCl2 to Sugarcane bagasse of 1:1. SEM micrographs also show the presence of well developed pores on its surface of AC-1. The broad peaks in the XRD patterns indicated that, all the ACs is amorphous materials. From results, it is concluded that ZnCl2 concentration used in impregnation is effective for development of porosity and surface area of the AC prepared from sugarcane bagasse.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信