树脂粘结简化二硅酸锂玻璃陶瓷修复体的疲劳失效载荷:陶瓷调理方法的影响。

João Paulo Mendes Tribst, J. Monteiro, A. B. Venturini, G. Pereira, M. Bottino, R. Melo, L. Valandro
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引用次数: 19

摘要

目的评价不同陶瓷表面调理方法对粘接胶结简化二硅酸锂玻璃陶瓷修复体疲劳破坏载荷的影响。材料与方法陶瓷(IPS e.max CAD, Ivoclar Vivadent) (Ø = 10 mm;厚度= 1.2 mm)和环氧树脂(Ø = 10 mm;厚度= 2.3 mm)的圆盘。陶瓷结合表面处理如下:不蚀刻,只使用mps -硅烷底漆(MN);用10%氢氟酸(HF)蚀刻20 s,然后涂底漆(HF + MN);HF +通用多模粘合剂应用(HF + SU);用一步蚀刻底漆(ME&P)蚀刻;HF +底漆+常规粘合剂(HF + MN + PAB)。环氧树脂圆盘用10% HF蚀刻20 s,然后涂上一层粘合剂(Multilink Primer a +B)。用复合水泥(Multilink N, Ivoclar Vivadent)对陶瓷/环氧树脂盘进行胶结。平均疲劳破坏载荷采用阶梯法确定(20 Hz频率下10万次循环;初始载荷= 1435 N;结果me&p组的疲劳失效载荷最大,HF腐蚀组次之,而MN组的疲劳失效载荷最小。所有的样品都呈现放射状裂纹,这些裂纹是由条件陶瓷表面(界面)的缺陷引起的。结论采用一步自蚀刻陶瓷底漆同时进行理化调理,促进了玻璃陶瓷修复体的最佳疲劳性能。这可能表明,由于表面变化比氢氟酸蚀刻产生的表面变化更小,因此一步处理减少了陶瓷表面的缺陷数量,改善了疲劳性能。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Fatigue Failure Load of Resin-bonded Simplified Lithium Disilicate Glass-Ceramic Restorations: Effect of Ceramic Conditioning Methods.
PURPOSE To evaluate the influence of different ceramic surface conditioning methods on the fatigue failure load of adhesively cemented simplified lithium-disilicate glass-ceramic restorations. MATERIALS AND METHODS Ceramic (IPS e.max CAD, Ivoclar Vivadent) (Ø = 10 mm; thickness = 1.2 mm) and epoxy resin (Ø = 10 mm; thickness = 2.3 mm) disks were produced. The ceramic bonding surfaces were treated as follows: no etching and MPS-silane primer application only (MN); etching with 10% hydrofluoric acid (HF) for 20 s followed by primer application (HF + MN); HF + universal multimode adhesive application (HF + SU); etching with a one-step etching primer (ME&P); HF + primer + conventional adhesive (HF + MN + PAB). The epoxy resin disks were etched with 10% HF for 20 s followed by a coat of bonding agent (Multilink Primer A+B). Pairs of ceramic/epoxy resin disks were cemented with composite cement (Multilink N, Ivoclar Vivadent). The mean fatigue failure load was determined by the staircase method (100,000 cycles at 20 Hz frequency; initial load = 1435 N; step size = 72 N). RESULTS ME&P had the highest fatigue failure load, followed by HF etched groups, while the non-etched condition (MN group) had the lowest. All samples presented radial cracks originating from defects at the conditioned ceramic surface (interface). CONCLUSION The simultaneous physicochemical conditioning with one-step self-etching ceramic primer promoted the best fatigue behavior results of the glass-ceramic restorations. It might indicate that this one-step conditioning reduces the number of flaws at the ceramic surface due to the slighter surface alterations than those produced by hydrofluoric acid etching, improving the fatigue behavior.
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