{"title":"由30纳米大小的羟基磷灰石颗粒基粉末制备的多孔陶瓷的机械性能，用于潜在的硬组织工程应用","authors":"G. Poinern, R. Brundavanam, X. Le, D. Fawcett","doi":"10.5923/J.AJBE.20120206.07","DOIUrl":null,"url":null,"abstract":"In this paper, synthesised nanometre sized hydroxyapatite (nano-HAP) powders composed of spherical 30 ± 5 nm particles were compacted and sintered at temperatures ranging from 650 to 1250℃ to form ceramics of varying porosity and mechanical strength. The size, crystalline structure and morphology of both the synthesised nano-HAP particle powders and the compacted and sintered ceramics were investigated using both X-ray diffraction (XRD) and Field Emission Scanning Electron Microscopy (FESEM). Further characterisation techniques such as Brunauer-Emmett-Teller (BET) particle surface area, porosity, bulk density, Vickers hardness and yield strength at various sintering temperatures were tested on sintered pellets and evaluated.","PeriodicalId":7620,"journal":{"name":"American Journal of Biomedical Engineering","volume":"32 1","pages":"278-286"},"PeriodicalIF":0.0000,"publicationDate":"2013-01-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"25","resultStr":"{\"title\":\"The mechanical properties of a porous ceramic derived from a 30 nm sized particle based powder of hydroxyapatite for potential hard tissue engineering applications\",\"authors\":\"G. Poinern, R. Brundavanam, X. Le, D. Fawcett\",\"doi\":\"10.5923/J.AJBE.20120206.07\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this paper, synthesised nanometre sized hydroxyapatite (nano-HAP) powders composed of spherical 30 ± 5 nm particles were compacted and sintered at temperatures ranging from 650 to 1250℃ to form ceramics of varying porosity and mechanical strength. The size, crystalline structure and morphology of both the synthesised nano-HAP particle powders and the compacted and sintered ceramics were investigated using both X-ray diffraction (XRD) and Field Emission Scanning Electron Microscopy (FESEM). Further characterisation techniques such as Brunauer-Emmett-Teller (BET) particle surface area, porosity, bulk density, Vickers hardness and yield strength at various sintering temperatures were tested on sintered pellets and evaluated.\",\"PeriodicalId\":7620,\"journal\":{\"name\":\"American Journal of Biomedical Engineering\",\"volume\":\"32 1\",\"pages\":\"278-286\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2013-01-07\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"25\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"American Journal of Biomedical Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.5923/J.AJBE.20120206.07\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"American Journal of Biomedical Engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5923/J.AJBE.20120206.07","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
The mechanical properties of a porous ceramic derived from a 30 nm sized particle based powder of hydroxyapatite for potential hard tissue engineering applications
In this paper, synthesised nanometre sized hydroxyapatite (nano-HAP) powders composed of spherical 30 ± 5 nm particles were compacted and sintered at temperatures ranging from 650 to 1250℃ to form ceramics of varying porosity and mechanical strength. The size, crystalline structure and morphology of both the synthesised nano-HAP particle powders and the compacted and sintered ceramics were investigated using both X-ray diffraction (XRD) and Field Emission Scanning Electron Microscopy (FESEM). Further characterisation techniques such as Brunauer-Emmett-Teller (BET) particle surface area, porosity, bulk density, Vickers hardness and yield strength at various sintering temperatures were tested on sintered pellets and evaluated.
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