纳米颗粒分散液滴干燥后形成环状结块的检测方法

A. Kurokawa, K. Kumagai, Satoru Akai, N. Handa, Yoshikazu Sasaki, N. Kikuchi, S. Kitamura, H. Manabe
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引用次数: 0

摘要

本文描述了微电网表面纳米颗粒环状凝聚体的检测方法。纳米粒子的环状分布通常是通过自然干燥纳米粒子分散的水滴形成的。利用分散在水中的荧光NPs和荧光显微镜对其环状结构进行了鉴定。用这种方法,通过冷冻干燥样品制备观察到环形成的减少。通过与透射电镜图像的比较表明,该方法不仅可以进行环形检测,而且可以对颗粒密度均匀性进行评价。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Detection method for ring-shape agglomerations formed by drying nanoparticle-dispersed droplet
The detection method for the ring-shaped agglomerations of nanoparticles (NPs) on a microgrid surface is described. The ring distribution of NPs is typically formed by naturally drying the droplet of nanoparticle-dispersed water. Fluorescent (FL) NPs dispersed in water and an FL microscope were used for the identification of the ring formation. With this method, the reduction of the ring formation was observed by a freeze-drying specimen preparation. The comparison with the transmission electron microscope image showed that this method gives not only for ring-shape detection but also for the evaluation of the particle-density homogeneity.
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