{"title":"用Box-Behnken设计方法评价硫酸浸出粘土中氧化铝的最优因素","authors":"Volkan Arslan","doi":"10.3103/S106782122202002X","DOIUrl":null,"url":null,"abstract":"<p>Calcination experiments were carried out using calcined clay and optimum calcination conditions were determined as 750°C and 60 min. The Box–Behnken design (BBD) was used to model, predict, and optimize the experimental parameters. The effective parameters and their interactions were explained with a mathematical model. The correlation coefficient (<i>R</i><sup>2</sup>) of the proposed model for the relationship between the yield of alumina extraction and experimental parameters was calculated as 0.9573 and it was determined that the predicted and actual values were in good agreement. The modeling results showed that the significance order of the parameters was leaching temperature > acid concentration > leaching time > acid/clay ratio. Finally, an extra optimization study was carried out to maximize the yield of alumina extraction and the yield was found to be 88.15% under the optimum conditions determined by the model (2.56 M acid concentration, 154.46 min leaching time, 89.77°C leaching temperature, and 53.21% acid/clay ratio).</p>","PeriodicalId":765,"journal":{"name":"Russian Journal of Non-Ferrous Metals","volume":null,"pages":null},"PeriodicalIF":0.6000,"publicationDate":"2022-04-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Optimal Factor Evaluation for the Extraction of Alumina from Clays by Sulfuric Acid Leaching Process Using Box–Behnken Design Methodology\",\"authors\":\"Volkan Arslan\",\"doi\":\"10.3103/S106782122202002X\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Calcination experiments were carried out using calcined clay and optimum calcination conditions were determined as 750°C and 60 min. The Box–Behnken design (BBD) was used to model, predict, and optimize the experimental parameters. The effective parameters and their interactions were explained with a mathematical model. The correlation coefficient (<i>R</i><sup>2</sup>) of the proposed model for the relationship between the yield of alumina extraction and experimental parameters was calculated as 0.9573 and it was determined that the predicted and actual values were in good agreement. The modeling results showed that the significance order of the parameters was leaching temperature > acid concentration > leaching time > acid/clay ratio. Finally, an extra optimization study was carried out to maximize the yield of alumina extraction and the yield was found to be 88.15% under the optimum conditions determined by the model (2.56 M acid concentration, 154.46 min leaching time, 89.77°C leaching temperature, and 53.21% acid/clay ratio).</p>\",\"PeriodicalId\":765,\"journal\":{\"name\":\"Russian Journal of Non-Ferrous Metals\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.6000,\"publicationDate\":\"2022-04-30\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"1\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Russian Journal of Non-Ferrous Metals\",\"FirstCategoryId\":\"88\",\"ListUrlMain\":\"https://link.springer.com/article/10.3103/S106782122202002X\",\"RegionNum\":4,\"RegionCategory\":\"材料科学\",\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"METALLURGY & METALLURGICAL ENGINEERING\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Russian Journal of Non-Ferrous Metals","FirstCategoryId":"88","ListUrlMain":"https://link.springer.com/article/10.3103/S106782122202002X","RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"METALLURGY & METALLURGICAL ENGINEERING","Score":null,"Total":0}
Optimal Factor Evaluation for the Extraction of Alumina from Clays by Sulfuric Acid Leaching Process Using Box–Behnken Design Methodology
Calcination experiments were carried out using calcined clay and optimum calcination conditions were determined as 750°C and 60 min. The Box–Behnken design (BBD) was used to model, predict, and optimize the experimental parameters. The effective parameters and their interactions were explained with a mathematical model. The correlation coefficient (R2) of the proposed model for the relationship between the yield of alumina extraction and experimental parameters was calculated as 0.9573 and it was determined that the predicted and actual values were in good agreement. The modeling results showed that the significance order of the parameters was leaching temperature > acid concentration > leaching time > acid/clay ratio. Finally, an extra optimization study was carried out to maximize the yield of alumina extraction and the yield was found to be 88.15% under the optimum conditions determined by the model (2.56 M acid concentration, 154.46 min leaching time, 89.77°C leaching temperature, and 53.21% acid/clay ratio).
期刊介绍:
Russian Journal of Non-Ferrous Metals is a journal the main goal of which is to achieve new knowledge in the following topics: extraction metallurgy, hydro- and pirometallurgy, casting, plastic deformation, metallography and heat treatment, powder metallurgy and composites, self-propagating high-temperature synthesis, surface engineering and advanced protected coatings, environments, and energy capacity in non-ferrous metallurgy.