用Box-Behnken设计方法评价硫酸浸出粘土中氧化铝的最优因素

IF 0.6 4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING
Volkan Arslan
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引用次数: 1

摘要

采用煅烧粘土进行煅烧实验,确定最佳煅烧条件为750℃、60 min。采用Box-Behnken设计(BBD)对实验参数进行建模、预测和优化。用数学模型解释了有效参数及其相互作用。建立的氧化铝萃取率与实验参数关系模型的相关系数R2为0.9573,预测值与实际值吻合较好。建模结果表明,各参数的显著性顺序为浸出温度>酸浓度>浸出时间>酸/粘土比例。最后,为实现氧化铝提取率的最大化,进行了进一步的优化研究,在该模型确定的最佳条件下(酸浓度2.56 M,浸出时间154.46 min,浸出温度89.77℃,酸泥比53.21%),氧化铝提取率可达88.15%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。

Optimal Factor Evaluation for the Extraction of Alumina from Clays by Sulfuric Acid Leaching Process Using Box–Behnken Design Methodology

Optimal Factor Evaluation for the Extraction of Alumina from Clays by Sulfuric Acid Leaching Process Using Box–Behnken Design Methodology

Calcination experiments were carried out using calcined clay and optimum calcination conditions were determined as 750°C and 60 min. The Box–Behnken design (BBD) was used to model, predict, and optimize the experimental parameters. The effective parameters and their interactions were explained with a mathematical model. The correlation coefficient (R2) of the proposed model for the relationship between the yield of alumina extraction and experimental parameters was calculated as 0.9573 and it was determined that the predicted and actual values were in good agreement. The modeling results showed that the significance order of the parameters was leaching temperature > acid concentration > leaching time > acid/clay ratio. Finally, an extra optimization study was carried out to maximize the yield of alumina extraction and the yield was found to be 88.15% under the optimum conditions determined by the model (2.56 M acid concentration, 154.46 min leaching time, 89.77°C leaching temperature, and 53.21% acid/clay ratio).

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来源期刊
Russian Journal of Non-Ferrous Metals
Russian Journal of Non-Ferrous Metals METALLURGY & METALLURGICAL ENGINEERING-
CiteScore
1.90
自引率
12.50%
发文量
59
审稿时长
3 months
期刊介绍: Russian Journal of Non-Ferrous Metals is a journal the main goal of which is to achieve new knowledge in the following topics: extraction metallurgy, hydro- and pirometallurgy, casting, plastic deformation, metallography and heat treatment, powder metallurgy and composites, self-propagating high-temperature synthesis, surface engineering and advanced protected coatings, environments, and energy capacity in non-ferrous metallurgy.
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