共沉淀纳米粉体制备8mol%氧化钇稳定氧化锆(8YSZ)透明陶瓷及其微观结构演变

IF 3.8 3区 材料科学 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY
Penghui Chen , Qian Wang , Dianjun Hu , Danyang Zhu , Haohong Chen , Zhengfa Dai , Qiang Liu , Jiang Li
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引用次数: 0

摘要

以氨水为沉淀剂,采用共沉淀法合成了8YSZ前驱体。研究了煅烧温度对8YSZ纳米粉体相、形貌和分散性的影响。研究发现,在800°C下煅烧的8YSZ纳米粉体具有最佳的可烧结性,平均粒径为14.5 nm。然后通过在1250–1325°C下空气预烧结,然后在1550°C下HIP后处理制备8YSZ陶瓷。研究了预烧结温度对8YSZ陶瓷显微结构和光学透明性的影响。研究发现,在1300°C下预烧结的8YSZ陶瓷具有合适的微观结构。与我们以前的工作相比,共沉淀粉末制备的8YSZ透明陶瓷的HIP后处理温度成功降低了200°C。厚度为1.0mm的8YSZ陶瓷在800nm处的线内透射率达到65.7%,平均晶粒尺寸为25μm。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Fabrication and microstructure evolution of 8 mol% yttria-stabilized zirconia (8YSZ) transparent ceramics from co-precipitated nanopowders

8YSZ precursor was synthesized by the co-precipitation method using ammonia as the precipitant. The influences of calcination temperature on the phase, morphology and dispersity of 8YSZ nanopowders were investigated. It was found that the 8YSZ nanopowders calcined at 800 °C had the best sinterability with the mean particle size of 14.5 nm. 8YSZ ceramics were then fabricated by air pre-sintering at 1250–1325 °C followed by HIP post-treatment at 1550 °C. The influences of pre-sintering temperature on the microstructure and optical transparency of 8YSZ ceramics were studied. It was found that the 8YSZ ceramics pre-sintered at 1300 °C had a suitable microstructure. The HIP post-treatment temperature was successfully reduced by 200 °C for the 8YSZ transparent ceramics from co-precipitated powders compare with our previous works. In-line transmittance of the 8YSZ ceramics (1.0 mm in thickness) reached 65.7% at 800 nm and the average grain size was 25 μm.

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来源期刊
Optical Materials
Optical Materials 工程技术-材料科学:综合
CiteScore
6.60
自引率
12.80%
发文量
1265
审稿时长
38 days
期刊介绍: Optical Materials has an open access mirror journal Optical Materials: X, sharing the same aims and scope, editorial team, submission system and rigorous peer review. The purpose of Optical Materials is to provide a means of communication and technology transfer between researchers who are interested in materials for potential device applications. The journal publishes original papers and review articles on the design, synthesis, characterisation and applications of optical materials. OPTICAL MATERIALS focuses on: • Optical Properties of Material Systems; • The Materials Aspects of Optical Phenomena; • The Materials Aspects of Devices and Applications. Authors can submit separate research elements describing their data to Data in Brief and methods to Methods X.
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