Nur Karima, Noval Kurniawati, B. Fachri, I. Rahmawati, B. Palupi, M. Mahfud, Ditta Kharisma Yolanda, A. Rahmawati, Badril Azhar, M. Muharja
{"title":"白莲花挥发油提取工艺优化无溶剂微波萃取法提取茶叶","authors":"Nur Karima, Noval Kurniawati, B. Fachri, I. Rahmawati, B. Palupi, M. Mahfud, Ditta Kharisma Yolanda, A. Rahmawati, Badril Azhar, M. Muharja","doi":"10.33795/jtkl.v6i2.339","DOIUrl":null,"url":null,"abstract":"Beluntas (Pluchea Indica L.) yang biasa digunakan sebagai astringent dan antipiretik memiliki potensi yang tinggi sebagai bahan baku produksi minyak atsiri. Tujuan dari penelitian ini adalah untuk mengoptimalkan solvent-free microwave extraction (SFME) dari daun beluntas menggunakan response surface metodology (RSM). Desain Box-Behnken dengan variasi waktu ekstraksi (60-120 menit), rasio bahan/labu distilat (0,06-0,1 g/ml), dan daya pemanas (150-450 Watt) digunakan untuk mengoptimalkan produksi minyak atsiri. Faktor rasio bahan/penyuling memiliki pengaruh signifikan paling tinggi terhadap rendemen minyak atsiri (P<0,05). Rendemen minyak atsiri meningkat seiring dengan meningkatnya daya pemanasan minyak dan waktu ekstraksi, dan sebaliknya. Di sisi lain, peningkatan rasio bahan/labu distilat memberikan dampak negatif terhadap rendemen minyak atsiri. Hasil minyak atsiri maksimum menggunakan metode SFME sebesar 0,2728 b/b% diperoleh untuk kondisi optimal waktu ekstraksi 90 menit, daya pemanasan 450 W, dan rasio bahan/labu distilat 0,06.Beluntas (Pluchea Indica L.) which commonly used as astringent and antipyretic has a high potential for the feedstock of essential oil production. The objective of this work is to optimize solvent-free microwave extraction (SFME) of Beluntas leaves by using response surface methodology (RSM). Box-Behnken Design with the variations of extraction time (60-120 min), feed/distiller ratio (0.06-0.1 g/ml), and heating power (150-450 W) was utilized to optimize essential oil yield. The feed/distiller ratio factor had the highest significant effect on the essential oil yield (P<0.05). Essential oil yield increased as the increase of oil heating power and time extraction, and vice versa. On the other hand, the increase in the feed/distiller ratio gave a negative impact on the essential oil yield. The maximum essential oil yield using SFME method of 0.2728 b/b% was obtained for the optimized condition of extraction time of 90 min, microwave heating power of 450 W, and feed/distiller ratio of 0.06.","PeriodicalId":52562,"journal":{"name":"Jurnal Teknik Kimia dan Lingkungan","volume":" ","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2022-10-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"1","resultStr":"{\"title\":\"Optimization of Essential Oil Extraction of Beluntas (Pluchea Indica L.) Leaves by Using Solvent-Free Microwave Extraction\",\"authors\":\"Nur Karima, Noval Kurniawati, B. 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Di sisi lain, peningkatan rasio bahan/labu distilat memberikan dampak negatif terhadap rendemen minyak atsiri. Hasil minyak atsiri maksimum menggunakan metode SFME sebesar 0,2728 b/b% diperoleh untuk kondisi optimal waktu ekstraksi 90 menit, daya pemanasan 450 W, dan rasio bahan/labu distilat 0,06.Beluntas (Pluchea Indica L.) which commonly used as astringent and antipyretic has a high potential for the feedstock of essential oil production. The objective of this work is to optimize solvent-free microwave extraction (SFME) of Beluntas leaves by using response surface methodology (RSM). Box-Behnken Design with the variations of extraction time (60-120 min), feed/distiller ratio (0.06-0.1 g/ml), and heating power (150-450 W) was utilized to optimize essential oil yield. The feed/distiller ratio factor had the highest significant effect on the essential oil yield (P<0.05). Essential oil yield increased as the increase of oil heating power and time extraction, and vice versa. 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Optimization of Essential Oil Extraction of Beluntas (Pluchea Indica L.) Leaves by Using Solvent-Free Microwave Extraction
Beluntas (Pluchea Indica L.) yang biasa digunakan sebagai astringent dan antipiretik memiliki potensi yang tinggi sebagai bahan baku produksi minyak atsiri. Tujuan dari penelitian ini adalah untuk mengoptimalkan solvent-free microwave extraction (SFME) dari daun beluntas menggunakan response surface metodology (RSM). Desain Box-Behnken dengan variasi waktu ekstraksi (60-120 menit), rasio bahan/labu distilat (0,06-0,1 g/ml), dan daya pemanas (150-450 Watt) digunakan untuk mengoptimalkan produksi minyak atsiri. Faktor rasio bahan/penyuling memiliki pengaruh signifikan paling tinggi terhadap rendemen minyak atsiri (P<0,05). Rendemen minyak atsiri meningkat seiring dengan meningkatnya daya pemanasan minyak dan waktu ekstraksi, dan sebaliknya. Di sisi lain, peningkatan rasio bahan/labu distilat memberikan dampak negatif terhadap rendemen minyak atsiri. Hasil minyak atsiri maksimum menggunakan metode SFME sebesar 0,2728 b/b% diperoleh untuk kondisi optimal waktu ekstraksi 90 menit, daya pemanasan 450 W, dan rasio bahan/labu distilat 0,06.Beluntas (Pluchea Indica L.) which commonly used as astringent and antipyretic has a high potential for the feedstock of essential oil production. The objective of this work is to optimize solvent-free microwave extraction (SFME) of Beluntas leaves by using response surface methodology (RSM). Box-Behnken Design with the variations of extraction time (60-120 min), feed/distiller ratio (0.06-0.1 g/ml), and heating power (150-450 W) was utilized to optimize essential oil yield. The feed/distiller ratio factor had the highest significant effect on the essential oil yield (P<0.05). Essential oil yield increased as the increase of oil heating power and time extraction, and vice versa. On the other hand, the increase in the feed/distiller ratio gave a negative impact on the essential oil yield. The maximum essential oil yield using SFME method of 0.2728 b/b% was obtained for the optimized condition of extraction time of 90 min, microwave heating power of 450 W, and feed/distiller ratio of 0.06.
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