S. S. Kakati, T. M. Makandar, M. K. Rendale, S. N. Mathad
{"title":"柑橘柠檬介导的溶胶-凝胶自燃烧法绿色合成纳米钴掺杂Mg-Zn","authors":"S. S. Kakati, T. M. Makandar, M. K. Rendale, S. N. Mathad","doi":"10.3103/S1061386222030049","DOIUrl":null,"url":null,"abstract":"<p>Cobalt doped Mg–Zn ferrite (Mg<sub>(0.56)</sub>Co<sub>(0.14)</sub>Zn<sub>(0.30)</sub>Fe<sub>2</sub>O<sub>4</sub>) was synthesized by the modified sol–gel auto combustion method (MSG) in which lemon extracts were used as the source of energy. X-ray diffraction (XRD) technique was employed to confirm the formation of cubic spinel ferrite phase. The lattice parameter was evaluated to be 8.39 Å with an average crystallite size ranging from 41–51 nm. Dislocation density, mechanical properties, and hopping length were determined. Crystallite size and strain were evaluated using W–H plot and size–strain plot.</p>","PeriodicalId":595,"journal":{"name":"International Journal of Self-Propagating High-Temperature Synthesis","volume":null,"pages":null},"PeriodicalIF":0.5000,"publicationDate":"2022-09-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Green Synthesis Approach for Nanosized Cobalt Doped Mg–Zn through Citrus Lemon Mediated Sol–Gel Auto Combustion Method\",\"authors\":\"S. S. Kakati, T. M. Makandar, M. K. Rendale, S. N. Mathad\",\"doi\":\"10.3103/S1061386222030049\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"<p>Cobalt doped Mg–Zn ferrite (Mg<sub>(0.56)</sub>Co<sub>(0.14)</sub>Zn<sub>(0.30)</sub>Fe<sub>2</sub>O<sub>4</sub>) was synthesized by the modified sol–gel auto combustion method (MSG) in which lemon extracts were used as the source of energy. X-ray diffraction (XRD) technique was employed to confirm the formation of cubic spinel ferrite phase. The lattice parameter was evaluated to be 8.39 Å with an average crystallite size ranging from 41–51 nm. Dislocation density, mechanical properties, and hopping length were determined. Crystallite size and strain were evaluated using W–H plot and size–strain plot.</p>\",\"PeriodicalId\":595,\"journal\":{\"name\":\"International Journal of Self-Propagating High-Temperature Synthesis\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.5000,\"publicationDate\":\"2022-09-15\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Journal of Self-Propagating High-Temperature Synthesis\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://link.springer.com/article/10.3103/S1061386222030049\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q4\",\"JCRName\":\"MATERIALS SCIENCE, MULTIDISCIPLINARY\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Journal of Self-Propagating High-Temperature Synthesis","FirstCategoryId":"1085","ListUrlMain":"https://link.springer.com/article/10.3103/S1061386222030049","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q4","JCRName":"MATERIALS SCIENCE, MULTIDISCIPLINARY","Score":null,"Total":0}
Green Synthesis Approach for Nanosized Cobalt Doped Mg–Zn through Citrus Lemon Mediated Sol–Gel Auto Combustion Method
Cobalt doped Mg–Zn ferrite (Mg(0.56)Co(0.14)Zn(0.30)Fe2O4) was synthesized by the modified sol–gel auto combustion method (MSG) in which lemon extracts were used as the source of energy. X-ray diffraction (XRD) technique was employed to confirm the formation of cubic spinel ferrite phase. The lattice parameter was evaluated to be 8.39 Å with an average crystallite size ranging from 41–51 nm. Dislocation density, mechanical properties, and hopping length were determined. Crystallite size and strain were evaluated using W–H plot and size–strain plot.
期刊介绍:
International Journal of Self-Propagating High-Temperature Synthesis is an international journal covering a wide range of topics concerned with self-propagating high-temperature synthesis (SHS), the process for the production of advanced materials based on solid-state combustion utilizing internally generated chemical energy. Subjects range from the fundamentals of SHS processes, chemistry and technology of SHS products and advanced materials to problems concerned with related fields, such as the kinetics and thermodynamics of high-temperature chemical reactions, combustion theory, macroscopic kinetics of nonisothermic processes, etc. The journal is intended to provide a wide-ranging exchange of research results and a better understanding of developmental and innovative trends in SHS science and applications.