最佳提取条件建模并鉴定胡椒Atsiri油的成分

Shintawati Shintawati, A. Analianasari, Zukryandry Zukryandry
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引用次数: 0

摘要

黑胡椒是一种具有辛辣味道和独特香气的香料,被称为香料之王。黑胡椒独特的香气来自于构成胡椒精油的挥发性化合物。黑胡椒精油具有抗菌特性,可以缓解呼吸道感染和肌肉紊乱。从蒸馏过程中获得辣椒精油受操作条件的影响。本研究的目的是利用气相色谱法(GCMS)对黑胡椒挥发油的成分进行鉴定,并对黑胡椒挥发油的工艺条件(原料粒度、溶剂比、蒸馏时间)进行优化。采用响应面法(RSM)确定最佳条件。结果表明,本实验黑胡椒精油的最高得率为5.14%。实验结果表明,料粒度为40目,溶剂比为0.12 (g ml-1),蒸馏时间为162 min,辣椒油得率为5.81%。GCMS测试结果表明,辣椒精油的主要成分为石竹烯、山香烯、柠檬烯、蒈烯和a-蒎烯。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Pemodelan Kondisi Optimum Ekstraksi dan Identifikasi Senyawa Penyusun Minyak Atsiri Lada Hitam
Black pepper is a spice with a spicy taste and a distinctive aroma that has become known as the King of Spices. The distinctive aroma of black pepper comes from the volatile compounds that make up the essential oil of pepper. Black pepper essential oil has antimicrobial properties that can relieve respiratory infections and relieve muscle disorders. The acquisition of pepper essential oil from the distillation process is influenced by operating conditions. The aim of this study was to identify the composition of black pepper essential oil compounds using GCMS and to optimize the operating conditions (material size, solvent ratio, and distillation time). The method used to determine the optimum condition is using the Response Surface Method (RSM). The results showed that the highest yield of black pepper essential oil from this experiment is 5.14%. The empirical model was also suitable for the experiment and the optimum conditions for producing the maximum pepper oil yield 5,81% were 40 mesh of material size, 0.12 (g.ml-1) of solvent ratio and 162 minutes of distillation time. GCMS test results showed that the main constituents of pepper essential oil are caryophyllene, ocimene, limonene, carene, and a-pinene.
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